Size-controlled synthesis, microstructure and magnetic properties of Ni nanoparticles
Ni nanoparticles with different mean diameters of 15–83 nm were synthesized by solution reduction process. The size of Ni nanoparticles can be controlled by varying the concentration of NiCl 2·6H 2O and synthesis temperature. The samples were characterized by scanning electron microscopy (SEM), tran...
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| Veröffentlicht in: | Materials research bulletin 2008-12, Vol.43 (12), p.3529-3536 |
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| container_title | Materials research bulletin |
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| creator | Wang, Huazhi Kou, Xinli Zhang, Lei Li, Jiangong |
| description | Ni nanoparticles with different mean diameters of 15–83
nm were synthesized by solution reduction process. The size of Ni nanoparticles can be controlled by varying the concentration of NiCl
2·6H
2O and synthesis temperature. The samples were characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), infrared spectroscopy (IR) and X-ray photoelectron spectroscopy (XPS). Results show that the synthesized particles are single-phased Ni with a face-centered cubic crystal structure. Magnetic measurements indicate that Ni nanoparticles are ferromagnetic. The lattice constants and coercivities of the samples are size-dependent. |
| doi_str_mv | 10.1016/j.materresbull.2008.01.012 |
| format | Article |
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nm were synthesized by solution reduction process. The size of Ni nanoparticles can be controlled by varying the concentration of NiCl
2·6H
2O and synthesis temperature. The samples were characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), infrared spectroscopy (IR) and X-ray photoelectron spectroscopy (XPS). Results show that the synthesized particles are single-phased Ni with a face-centered cubic crystal structure. Magnetic measurements indicate that Ni nanoparticles are ferromagnetic. The lattice constants and coercivities of the samples are size-dependent.</description><identifier>ISSN: 0025-5408</identifier><identifier>EISSN: 1873-4227</identifier><identifier>DOI: 10.1016/j.materresbull.2008.01.012</identifier><language>eng</language><publisher>United States: Elsevier Ltd</publisher><subject>A. Nanostructures ; ABSORPTION SPECTROSCOPY ; COERCIVE FORCE ; D. Magnetic properties ; D. Microstructure ; FCC LATTICES ; INFRARED SPECTRA ; LATTICE PARAMETERS ; MAGNETIC PROPERTIES ; MATERIALS SCIENCE ; MICROSTRUCTURE ; NANOSTRUCTURES ; NICKEL ; PARTICLES ; SCANNING ELECTRON MICROSCOPY ; SYNTHESIS ; TRANSMISSION ELECTRON MICROSCOPY ; X-RAY DIFFRACTION ; X-RAY PHOTOELECTRON SPECTROSCOPY</subject><ispartof>Materials research bulletin, 2008-12, Vol.43 (12), p.3529-3536</ispartof><rights>2008 Elsevier Ltd</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c418t-3a82e0f0cae9aab1f640cf5603b7ab78ad29200dac47a977b70142757fc5b203</citedby><cites>FETCH-LOGICAL-c418t-3a82e0f0cae9aab1f640cf5603b7ab78ad29200dac47a977b70142757fc5b203</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.materresbull.2008.01.012$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>230,315,781,785,886,3551,27928,27929,45999</link.rule.ids><backlink>$$Uhttps://www.osti.gov/biblio/21195040$$D View this record in Osti.gov$$Hfree_for_read</backlink></links><search><creatorcontrib>Wang, Huazhi</creatorcontrib><creatorcontrib>Kou, Xinli</creatorcontrib><creatorcontrib>Zhang, Lei</creatorcontrib><creatorcontrib>Li, Jiangong</creatorcontrib><title>Size-controlled synthesis, microstructure and magnetic properties of Ni nanoparticles</title><title>Materials research bulletin</title><description>Ni nanoparticles with different mean diameters of 15–83
nm were synthesized by solution reduction process. The size of Ni nanoparticles can be controlled by varying the concentration of NiCl
2·6H
2O and synthesis temperature. The samples were characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), infrared spectroscopy (IR) and X-ray photoelectron spectroscopy (XPS). Results show that the synthesized particles are single-phased Ni with a face-centered cubic crystal structure. Magnetic measurements indicate that Ni nanoparticles are ferromagnetic. The lattice constants and coercivities of the samples are size-dependent.</description><subject>A. Nanostructures</subject><subject>ABSORPTION SPECTROSCOPY</subject><subject>COERCIVE FORCE</subject><subject>D. Magnetic properties</subject><subject>D. Microstructure</subject><subject>FCC LATTICES</subject><subject>INFRARED SPECTRA</subject><subject>LATTICE PARAMETERS</subject><subject>MAGNETIC PROPERTIES</subject><subject>MATERIALS SCIENCE</subject><subject>MICROSTRUCTURE</subject><subject>NANOSTRUCTURES</subject><subject>NICKEL</subject><subject>PARTICLES</subject><subject>SCANNING ELECTRON MICROSCOPY</subject><subject>SYNTHESIS</subject><subject>TRANSMISSION ELECTRON MICROSCOPY</subject><subject>X-RAY DIFFRACTION</subject><subject>X-RAY PHOTOELECTRON SPECTROSCOPY</subject><issn>0025-5408</issn><issn>1873-4227</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2008</creationdate><recordtype>article</recordtype><recordid>eNqNUE1LxDAQDaLguvofil5tnaTppvUm6ycsenA9hzSdulnatCRZYf31pqwHj8LAwPA-5j1CLilkFOjiZpv1KqBz6Otd12UMoMyAxmFHZEZLkaecMXFMZgCsSAsO5Sk5834LALwUYkY-3s03pnqwwQ1dh03i9zZs0Bt_nfRGu8EHt9Nh5zBRtkl69WkxGJ2MbhjRBYM-Gdrk1SRW2WFU8aI79OfkpFWdx4vfPSfrx4f18jldvT29LO9Wqea0DGmuSobQglZYKVXTdsFBt8UC8lqoWpSqYVWM1CjNhaqEqAVQzkQhWl3UDPI5uTrIxi-N9NoE1JuYxaIOklFaFcAn1O0BNaXxDls5OtMrt5cU5NSi3Mq_LcqpRQk0Dovk-wMZY4wvg26yQauxMW5yaQbzH5kfhE6EVg</recordid><startdate>20081201</startdate><enddate>20081201</enddate><creator>Wang, Huazhi</creator><creator>Kou, Xinli</creator><creator>Zhang, Lei</creator><creator>Li, Jiangong</creator><general>Elsevier Ltd</general><scope>AAYXX</scope><scope>CITATION</scope><scope>OTOTI</scope></search><sort><creationdate>20081201</creationdate><title>Size-controlled synthesis, microstructure and magnetic properties of Ni nanoparticles</title><author>Wang, Huazhi ; Kou, Xinli ; Zhang, Lei ; Li, Jiangong</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c418t-3a82e0f0cae9aab1f640cf5603b7ab78ad29200dac47a977b70142757fc5b203</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2008</creationdate><topic>A. Nanostructures</topic><topic>ABSORPTION SPECTROSCOPY</topic><topic>COERCIVE FORCE</topic><topic>D. Magnetic properties</topic><topic>D. Microstructure</topic><topic>FCC LATTICES</topic><topic>INFRARED SPECTRA</topic><topic>LATTICE PARAMETERS</topic><topic>MAGNETIC PROPERTIES</topic><topic>MATERIALS SCIENCE</topic><topic>MICROSTRUCTURE</topic><topic>NANOSTRUCTURES</topic><topic>NICKEL</topic><topic>PARTICLES</topic><topic>SCANNING ELECTRON MICROSCOPY</topic><topic>SYNTHESIS</topic><topic>TRANSMISSION ELECTRON MICROSCOPY</topic><topic>X-RAY DIFFRACTION</topic><topic>X-RAY PHOTOELECTRON SPECTROSCOPY</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Wang, Huazhi</creatorcontrib><creatorcontrib>Kou, Xinli</creatorcontrib><creatorcontrib>Zhang, Lei</creatorcontrib><creatorcontrib>Li, Jiangong</creatorcontrib><collection>CrossRef</collection><collection>OSTI.GOV</collection><jtitle>Materials research bulletin</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Wang, Huazhi</au><au>Kou, Xinli</au><au>Zhang, Lei</au><au>Li, Jiangong</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Size-controlled synthesis, microstructure and magnetic properties of Ni nanoparticles</atitle><jtitle>Materials research bulletin</jtitle><date>2008-12-01</date><risdate>2008</risdate><volume>43</volume><issue>12</issue><spage>3529</spage><epage>3536</epage><pages>3529-3536</pages><issn>0025-5408</issn><eissn>1873-4227</eissn><abstract>Ni nanoparticles with different mean diameters of 15–83
nm were synthesized by solution reduction process. The size of Ni nanoparticles can be controlled by varying the concentration of NiCl
2·6H
2O and synthesis temperature. The samples were characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), infrared spectroscopy (IR) and X-ray photoelectron spectroscopy (XPS). Results show that the synthesized particles are single-phased Ni with a face-centered cubic crystal structure. Magnetic measurements indicate that Ni nanoparticles are ferromagnetic. The lattice constants and coercivities of the samples are size-dependent.</abstract><cop>United States</cop><pub>Elsevier Ltd</pub><doi>10.1016/j.materresbull.2008.01.012</doi><tpages>8</tpages></addata></record> |
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| source | Access via ScienceDirect (Elsevier) |
| subjects | A. Nanostructures ABSORPTION SPECTROSCOPY COERCIVE FORCE D. Magnetic properties D. Microstructure FCC LATTICES INFRARED SPECTRA LATTICE PARAMETERS MAGNETIC PROPERTIES MATERIALS SCIENCE MICROSTRUCTURE NANOSTRUCTURES NICKEL PARTICLES SCANNING ELECTRON MICROSCOPY SYNTHESIS TRANSMISSION ELECTRON MICROSCOPY X-RAY DIFFRACTION X-RAY PHOTOELECTRON SPECTROSCOPY |
| title | Size-controlled synthesis, microstructure and magnetic properties of Ni nanoparticles |
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