Structures of the reduced niobium oxides Nb{sub 12}O{sub 29} and Nb{sub 22}O{sub 54}

The crystal structure of Nb{sub 22}O{sub 54} is reported for the first time, and the structure of orthorhombic Nb{sub 12}O{sub 29} is reexamined, resolving previous ambiguities. Single crystal X-ray and electron diffraction were employed. These compounds were found to crystallize in the space groups...

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Veröffentlicht in:	Journal of solid state chemistry 2007-10, Vol.180 (10)
Hauptverfasser:	McQueen, T., Xu, Q., Andersen, E.N., Zandbergen, H.W., Cava, R.J.
Format:	Artikel
Sprache:	eng
Schlagworte:	BOND LENGTHS ELECTRON DIFFRACTION INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY MAGNETIC MOMENTS MONOCRYSTALS NIOBIUM NIOBIUM OXIDES ORTHORHOMBIC LATTICES SHEAR SPACE GROUPS X RADIATION X-RAY DIFFRACTION
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