XRD and {sup 119}Sn Moessbauer spectroscopy characterization of SnSe obtained from a simple chemical route
Crystalline tin selenide semiconductor was synthesized by a chemical route. Selenium powder reacted with potassium boronhydride, giving a soluble selenium species potassium seleniumhydride. The reaction of potassium seleniumhydride with tin chloride produced crystalline tin selenide, which was chara...
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| Veröffentlicht in: | Materials research bulletin 2005-09, Vol.40 (9) |
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| container_title | Materials research bulletin |
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| creator | Bernardes-Silva, Ana Claudia Mesquita, A.F. Moura de Neto, E. Porto, A.O. Ardisson, J.D. Lima, G.M. de Lameiras, F.S. |
| description | Crystalline tin selenide semiconductor was synthesized by a chemical route. Selenium powder reacted with potassium boronhydride, giving a soluble selenium species potassium seleniumhydride. The reaction of potassium seleniumhydride with tin chloride produced crystalline tin selenide, which was characterized by X-ray diffraction, {sup 119}Sn Moessbauer spectroscopy and scanning electronic microscopy. The material was thermally treated, in nitrogen flow, at 300 and 600 deg. C for 2 h and the particle size evolution was studied by X-ray diffraction. The X-ray diffraction and {sup 119}Sn Moessbauer results showed that a mixture of tin oxides and orthorhombic tin selenide was obtained. |
| doi_str_mv | 10.1016/j.materresbull.2005.04.021 |
| format | Article |
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Selenium powder reacted with potassium boronhydride, giving a soluble selenium species potassium seleniumhydride. The reaction of potassium seleniumhydride with tin chloride produced crystalline tin selenide, which was characterized by X-ray diffraction, {sup 119}Sn Moessbauer spectroscopy and scanning electronic microscopy. The material was thermally treated, in nitrogen flow, at 300 and 600 deg. C for 2 h and the particle size evolution was studied by X-ray diffraction. The X-ray diffraction and {sup 119}Sn Moessbauer results showed that a mixture of tin oxides and orthorhombic tin selenide was obtained.</description><identifier>ISSN: 0025-5408</identifier><identifier>EISSN: 1873-4227</identifier><identifier>DOI: 10.1016/j.materresbull.2005.04.021</identifier><language>eng</language><publisher>United States</publisher><subject>MATERIALS SCIENCE ; MICROSCOPY ; MOESSBAUER EFFECT ; ORTHORHOMBIC LATTICES ; PARTICLE SIZE ; POTASSIUM ; SELENIUM ; SEMICONDUCTOR MATERIALS ; TIN 119 ; TIN CHLORIDES ; TIN OXIDES ; X-RAY DIFFRACTION</subject><ispartof>Materials research bulletin, 2005-09, Vol.40 (9)</ispartof><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>230,314,780,784,885,27924,27925</link.rule.ids><backlink>$$Uhttps://www.osti.gov/biblio/20891587$$D View this record in Osti.gov$$Hfree_for_read</backlink></links><search><creatorcontrib>Bernardes-Silva, Ana Claudia</creatorcontrib><creatorcontrib>Mesquita, A.F.</creatorcontrib><creatorcontrib>Moura de Neto, E.</creatorcontrib><creatorcontrib>Porto, A.O.</creatorcontrib><creatorcontrib>Ardisson, J.D.</creatorcontrib><creatorcontrib>Lima, G.M. de</creatorcontrib><creatorcontrib>Lameiras, F.S.</creatorcontrib><title>XRD and {sup 119}Sn Moessbauer spectroscopy characterization of SnSe obtained from a simple chemical route</title><title>Materials research bulletin</title><description>Crystalline tin selenide semiconductor was synthesized by a chemical route. Selenium powder reacted with potassium boronhydride, giving a soluble selenium species potassium seleniumhydride. The reaction of potassium seleniumhydride with tin chloride produced crystalline tin selenide, which was characterized by X-ray diffraction, {sup 119}Sn Moessbauer spectroscopy and scanning electronic microscopy. The material was thermally treated, in nitrogen flow, at 300 and 600 deg. C for 2 h and the particle size evolution was studied by X-ray diffraction. The X-ray diffraction and {sup 119}Sn Moessbauer results showed that a mixture of tin oxides and orthorhombic tin selenide was obtained.</description><subject>MATERIALS SCIENCE</subject><subject>MICROSCOPY</subject><subject>MOESSBAUER EFFECT</subject><subject>ORTHORHOMBIC LATTICES</subject><subject>PARTICLE SIZE</subject><subject>POTASSIUM</subject><subject>SELENIUM</subject><subject>SEMICONDUCTOR MATERIALS</subject><subject>TIN 119</subject><subject>TIN CHLORIDES</subject><subject>TIN OXIDES</subject><subject>X-RAY DIFFRACTION</subject><issn>0025-5408</issn><issn>1873-4227</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2005</creationdate><recordtype>article</recordtype><recordid>eNqNj7tOxDAQAC0EEoHjH1ZQx6xNQnI1D9FcQyiuOzm-jc6RY0depwDEv5OCD6CaZqTRCHGrUCpUj_ejnEymlIj7xXupEWuJlUStzkSh2uahrLRuzkWBqOuyrrC9FFfMIyJWbdMUYty_P4MJR_jmZQaltj9dgF0k5t4slIBnsjlFtnH-BHsyydi1575MdjFAHKALHUHss3GBjjCkOIEBdtPsafVpctZ4SHHJtBEXg_FMN3-8FnevLx9Pb2Xk7A5sXSZ7sjGEtXjQ2G5VvQ78z_oFfABTpw</recordid><startdate>20050901</startdate><enddate>20050901</enddate><creator>Bernardes-Silva, Ana Claudia</creator><creator>Mesquita, A.F.</creator><creator>Moura de Neto, E.</creator><creator>Porto, A.O.</creator><creator>Ardisson, J.D.</creator><creator>Lima, G.M. de</creator><creator>Lameiras, F.S.</creator><scope>OTOTI</scope></search><sort><creationdate>20050901</creationdate><title>XRD and {sup 119}Sn Moessbauer spectroscopy characterization of SnSe obtained from a simple chemical route</title><author>Bernardes-Silva, Ana Claudia ; Mesquita, A.F. ; Moura de Neto, E. ; Porto, A.O. ; Ardisson, J.D. ; Lima, G.M. de ; Lameiras, F.S.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-osti_scitechconnect_208915873</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2005</creationdate><topic>MATERIALS SCIENCE</topic><topic>MICROSCOPY</topic><topic>MOESSBAUER EFFECT</topic><topic>ORTHORHOMBIC LATTICES</topic><topic>PARTICLE SIZE</topic><topic>POTASSIUM</topic><topic>SELENIUM</topic><topic>SEMICONDUCTOR MATERIALS</topic><topic>TIN 119</topic><topic>TIN CHLORIDES</topic><topic>TIN OXIDES</topic><topic>X-RAY DIFFRACTION</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Bernardes-Silva, Ana Claudia</creatorcontrib><creatorcontrib>Mesquita, A.F.</creatorcontrib><creatorcontrib>Moura de Neto, E.</creatorcontrib><creatorcontrib>Porto, A.O.</creatorcontrib><creatorcontrib>Ardisson, J.D.</creatorcontrib><creatorcontrib>Lima, G.M. de</creatorcontrib><creatorcontrib>Lameiras, F.S.</creatorcontrib><collection>OSTI.GOV</collection><jtitle>Materials research bulletin</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Bernardes-Silva, Ana Claudia</au><au>Mesquita, A.F.</au><au>Moura de Neto, E.</au><au>Porto, A.O.</au><au>Ardisson, J.D.</au><au>Lima, G.M. de</au><au>Lameiras, F.S.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>XRD and {sup 119}Sn Moessbauer spectroscopy characterization of SnSe obtained from a simple chemical route</atitle><jtitle>Materials research bulletin</jtitle><date>2005-09-01</date><risdate>2005</risdate><volume>40</volume><issue>9</issue><issn>0025-5408</issn><eissn>1873-4227</eissn><abstract>Crystalline tin selenide semiconductor was synthesized by a chemical route. Selenium powder reacted with potassium boronhydride, giving a soluble selenium species potassium seleniumhydride. The reaction of potassium seleniumhydride with tin chloride produced crystalline tin selenide, which was characterized by X-ray diffraction, {sup 119}Sn Moessbauer spectroscopy and scanning electronic microscopy. The material was thermally treated, in nitrogen flow, at 300 and 600 deg. C for 2 h and the particle size evolution was studied by X-ray diffraction. The X-ray diffraction and {sup 119}Sn Moessbauer results showed that a mixture of tin oxides and orthorhombic tin selenide was obtained.</abstract><cop>United States</cop><doi>10.1016/j.materresbull.2005.04.021</doi></addata></record> |
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| ispartof | Materials research bulletin, 2005-09, Vol.40 (9) |
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| subjects | MATERIALS SCIENCE MICROSCOPY MOESSBAUER EFFECT ORTHORHOMBIC LATTICES PARTICLE SIZE POTASSIUM SELENIUM SEMICONDUCTOR MATERIALS TIN 119 TIN CHLORIDES TIN OXIDES X-RAY DIFFRACTION |
| title | XRD and {sup 119}Sn Moessbauer spectroscopy characterization of SnSe obtained from a simple chemical route |
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