Hydrothermal synthesis and characterization of two new bicapped Keggin heteropoly tungstovanadated derivatives

Two new heteropoly tungstovanadate derivatives, [Fe(phen) 3] 2[W 10.5V 4.5O 42]·3H 2O (1) and [Fe(phen) 3] 2[W 10V 5O 42].6H 2O (2) (phen=1,10′-phenanthroline), have been synthesized under hydrothermal conditions by using different starting materials, and characterized by elemental analysis, IR, ESR...

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Veröffentlicht in:	Journal of solid state chemistry 2006-01, Vol.179 (1), p.122-129
Hauptverfasser:	Liu, Ya-Bing, Duan, Li-Mei, Yang, Xiao-Mei, Xu, Ji-Qing, Zhang, Qing-Bin, Lu, Yu-Kun, Liu, Jian
Format:	Artikel
Sprache:	eng
Schlagworte:	Bicapped Keggin structure Condensed matter: structure, mechanical and thermal properties Cross-disciplinary physics: materials science rheology ELECTRON SPIN RESONANCE Exact sciences and technology Growth from solutions HYDROTHERMAL SYNTHESIS Inorganic compounds INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY Materials science Methods of crystal growth physics of crystal growth Miscellaneous MONOCLINIC LATTICES MONOCRYSTALS Physics Polyoxometalates Property characterization SPACE GROUPS Structure of solids and liquids crystallography Structure of specific crystalline solids THERMAL GRAVIMETRIC ANALYSIS TUNGSTEN COMPOUNDS VANADATES X-RAY DIFFRACTION X-RAY PHOTOELECTRON SPECTROSCOPY
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