Synchrotron X-ray topographic characterization of dislocations in 6H-SiC axial samples

•Different types of dislocations in axial 6H-SiC are revealed.•Different configurations of basal plane dislocations are investigated.•Different types of the threading dislocations are characterized. Wide bandgap semiconductor, 6H-SiC, is being applied in photoconductive semiconductor switches (PCSS)...

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Veröffentlicht in:Journal of crystal growth 2022-02, Vol.579 (C), p.126459, Article 126459
Hauptverfasser: Peng, Hongyu, Liu, Yafei, Chen, Zeyu, Cheng, Qianyu, Hu, Shanshan, Raghothamachar, Balaji, Dudley, Michael, Sampayan, Kristin, Sampayan, Stephen
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container_issue C
container_start_page 126459
container_title Journal of crystal growth
container_volume 579
creator Peng, Hongyu
Liu, Yafei
Chen, Zeyu
Cheng, Qianyu
Hu, Shanshan
Raghothamachar, Balaji
Dudley, Michael
Sampayan, Kristin
Sampayan, Stephen
description •Different types of dislocations in axial 6H-SiC are revealed.•Different configurations of basal plane dislocations are investigated.•Different types of the threading dislocations are characterized. Wide bandgap semiconductor, 6H-SiC, is being applied in photoconductive semiconductor switches (PCSS) due to its semi-insulating properties. The behavior of the dislocations in 6H- SiC under the application of voltage and laser in such devices is of particular interest. In this study, synchrotron X-ray transmission topography, grazing incidence topography and rocking curve topography are applied to characterize the types and distribution of defects in (1 1 –2 0) oriented wafers. Threading edge dislocations (TED), threading screw dislocations (TSD), threading mixed dislocation (TMD) and basal plane dislocations (BPD) in 6H-SiC axial samples are revealed in the X-ray topographs. TEDs are observed to be more likely off c-axis compared to TSDs/TMDs. Contrast features of BPDs differ depending on their Burgers vectors and orientation with respect to wafer surface on rocking curve topographs and grazing incidence topographs. Applying ray tracing simulations, the configurations of BPDs can be determined, and the threading dislocations (TED, TSD and TMD) can be distinguished in grazing incidence topographs. The understanding of the nature and the distribution of these dislocations will help predict their propagation and movement under the application of voltage and laser, providing guidance for device fabrication.
doi_str_mv 10.1016/j.jcrysgro.2021.126459
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Wide bandgap semiconductor, 6H-SiC, is being applied in photoconductive semiconductor switches (PCSS) due to its semi-insulating properties. The behavior of the dislocations in 6H- SiC under the application of voltage and laser in such devices is of particular interest. In this study, synchrotron X-ray transmission topography, grazing incidence topography and rocking curve topography are applied to characterize the types and distribution of defects in (1 1 –2 0) oriented wafers. Threading edge dislocations (TED), threading screw dislocations (TSD), threading mixed dislocation (TMD) and basal plane dislocations (BPD) in 6H-SiC axial samples are revealed in the X-ray topographs. TEDs are observed to be more likely off c-axis compared to TSDs/TMDs. Contrast features of BPDs differ depending on their Burgers vectors and orientation with respect to wafer surface on rocking curve topographs and grazing incidence topographs. Applying ray tracing simulations, the configurations of BPDs can be determined, and the threading dislocations (TED, TSD and TMD) can be distinguished in grazing incidence topographs. The understanding of the nature and the distribution of these dislocations will help predict their propagation and movement under the application of voltage and laser, providing guidance for device fabrication.</description><identifier>ISSN: 0022-0248</identifier><identifier>EISSN: 1873-5002</identifier><identifier>DOI: 10.1016/j.jcrysgro.2021.126459</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>A1. Characterization ; A1. Defects ; A1. X-ray topography ; B1. Silicon carbide ; B2. 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Semiconducting materials</subject><subject>Basal plane</subject><subject>Edge dislocations</subject><subject>Electric potential</subject><subject>Grazing incidence</subject><subject>Ray tracing</subject><subject>Screw dislocations</subject><subject>Silicon carbide</subject><subject>Switches</subject><subject>Synchrotron radiation</subject><subject>Synchrotrons</subject><subject>Threading dislocations</subject><subject>Topography</subject><subject>Voltage</subject><subject>Wide bandgap semiconductors</subject><subject>X ray topography</subject><issn>0022-0248</issn><issn>1873-5002</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2022</creationdate><recordtype>article</recordtype><recordid>eNqFkE9LxDAQxYMouK5-BSl67po0Jk1vyuI_EDysireQTKe7KWtTkyqun96s1bOHmWHg94Y3j5BjRmeMMnnWzloIm7gMflbQgs1YIc9FtUMmTJU8F5QWu2SSepHT4lztk4MYW0qTktEJeV5sOlgFPwTfZS95MJts8L1fBtOvHGSwMsHAgMF9mcElxDdZ7eLaw88aM9dl8jZfuHlmPp1ZZ9G89muMh2SvMeuIR79zSp6urx7nt_n9w83d_PI-B85plQtVCVEhNHXZIAjWlII3ylKOlFkrFEorS8MoZ4yXCiso0NaWW2VrBGNrPiUn410fB6cjuAFhBb7rEAbNlFSypAk6HaE--Ld3jINu_Xvoki9dSM5TiapMlBwpCD7GgI3ug3s1YaMZ1dugdav_gtbboPUYdBJejEJMj344DFsf2AHWLmxt1N79d-Ib9JaLJA</recordid><startdate>20220201</startdate><enddate>20220201</enddate><creator>Peng, Hongyu</creator><creator>Liu, Yafei</creator><creator>Chen, Zeyu</creator><creator>Cheng, Qianyu</creator><creator>Hu, Shanshan</creator><creator>Raghothamachar, Balaji</creator><creator>Dudley, Michael</creator><creator>Sampayan, Kristin</creator><creator>Sampayan, Stephen</creator><general>Elsevier B.V</general><general>Elsevier BV</general><general>Elsevier</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope><scope>OTOTI</scope></search><sort><creationdate>20220201</creationdate><title>Synchrotron X-ray topographic characterization of dislocations in 6H-SiC axial samples</title><author>Peng, Hongyu ; Liu, Yafei ; Chen, Zeyu ; Cheng, Qianyu ; Hu, Shanshan ; Raghothamachar, Balaji ; Dudley, Michael ; Sampayan, Kristin ; Sampayan, Stephen</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c3309-589559ecfd7fec51f753f8b03e01bb58e6b67a10311378e9c2ebdb3b8bdecabd3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2022</creationdate><topic>A1. Characterization</topic><topic>A1. Defects</topic><topic>A1. X-ray topography</topic><topic>B1. Silicon carbide</topic><topic>B2. Semiconducting materials</topic><topic>Basal plane</topic><topic>Edge dislocations</topic><topic>Electric potential</topic><topic>Grazing incidence</topic><topic>Ray tracing</topic><topic>Screw dislocations</topic><topic>Silicon carbide</topic><topic>Switches</topic><topic>Synchrotron radiation</topic><topic>Synchrotrons</topic><topic>Threading dislocations</topic><topic>Topography</topic><topic>Voltage</topic><topic>Wide bandgap semiconductors</topic><topic>X ray topography</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Peng, Hongyu</creatorcontrib><creatorcontrib>Liu, Yafei</creatorcontrib><creatorcontrib>Chen, Zeyu</creatorcontrib><creatorcontrib>Cheng, Qianyu</creatorcontrib><creatorcontrib>Hu, Shanshan</creatorcontrib><creatorcontrib>Raghothamachar, Balaji</creatorcontrib><creatorcontrib>Dudley, Michael</creatorcontrib><creatorcontrib>Sampayan, Kristin</creatorcontrib><creatorcontrib>Sampayan, Stephen</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>OSTI.GOV</collection><jtitle>Journal of crystal growth</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Peng, Hongyu</au><au>Liu, Yafei</au><au>Chen, Zeyu</au><au>Cheng, Qianyu</au><au>Hu, Shanshan</au><au>Raghothamachar, Balaji</au><au>Dudley, Michael</au><au>Sampayan, Kristin</au><au>Sampayan, Stephen</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synchrotron X-ray topographic characterization of dislocations in 6H-SiC axial samples</atitle><jtitle>Journal of crystal growth</jtitle><date>2022-02-01</date><risdate>2022</risdate><volume>579</volume><issue>C</issue><spage>126459</spage><pages>126459-</pages><artnum>126459</artnum><issn>0022-0248</issn><eissn>1873-5002</eissn><abstract>•Different types of dislocations in axial 6H-SiC are revealed.•Different configurations of basal plane dislocations are investigated.•Different types of the threading dislocations are characterized. 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subjects A1. Characterization
A1. Defects
A1. X-ray topography
B1. Silicon carbide
B2. Semiconducting materials
Basal plane
Edge dislocations
Electric potential
Grazing incidence
Ray tracing
Screw dislocations
Silicon carbide
Switches
Synchrotron radiation
Synchrotrons
Threading dislocations
Topography
Voltage
Wide bandgap semiconductors
X ray topography
title Synchrotron X-ray topographic characterization of dislocations in 6H-SiC axial samples
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