Synchrotron X-ray topographic characterization of dislocations in 6H-SiC axial samples
•Different types of dislocations in axial 6H-SiC are revealed.•Different configurations of basal plane dislocations are investigated.•Different types of the threading dislocations are characterized. Wide bandgap semiconductor, 6H-SiC, is being applied in photoconductive semiconductor switches (PCSS)...
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Veröffentlicht in: | Journal of crystal growth 2022-02, Vol.579 (C), p.126459, Article 126459 |
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description | •Different types of dislocations in axial 6H-SiC are revealed.•Different configurations of basal plane dislocations are investigated.•Different types of the threading dislocations are characterized.
Wide bandgap semiconductor, 6H-SiC, is being applied in photoconductive semiconductor switches (PCSS) due to its semi-insulating properties. The behavior of the dislocations in 6H- SiC under the application of voltage and laser in such devices is of particular interest. In this study, synchrotron X-ray transmission topography, grazing incidence topography and rocking curve topography are applied to characterize the types and distribution of defects in (1 1 –2 0) oriented wafers. Threading edge dislocations (TED), threading screw dislocations (TSD), threading mixed dislocation (TMD) and basal plane dislocations (BPD) in 6H-SiC axial samples are revealed in the X-ray topographs. TEDs are observed to be more likely off c-axis compared to TSDs/TMDs. Contrast features of BPDs differ depending on their Burgers vectors and orientation with respect to wafer surface on rocking curve topographs and grazing incidence topographs. Applying ray tracing simulations, the configurations of BPDs can be determined, and the threading dislocations (TED, TSD and TMD) can be distinguished in grazing incidence topographs. The understanding of the nature and the distribution of these dislocations will help predict their propagation and movement under the application of voltage and laser, providing guidance for device fabrication. |
doi_str_mv | 10.1016/j.jcrysgro.2021.126459 |
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Wide bandgap semiconductor, 6H-SiC, is being applied in photoconductive semiconductor switches (PCSS) due to its semi-insulating properties. The behavior of the dislocations in 6H- SiC under the application of voltage and laser in such devices is of particular interest. In this study, synchrotron X-ray transmission topography, grazing incidence topography and rocking curve topography are applied to characterize the types and distribution of defects in (1 1 –2 0) oriented wafers. Threading edge dislocations (TED), threading screw dislocations (TSD), threading mixed dislocation (TMD) and basal plane dislocations (BPD) in 6H-SiC axial samples are revealed in the X-ray topographs. TEDs are observed to be more likely off c-axis compared to TSDs/TMDs. Contrast features of BPDs differ depending on their Burgers vectors and orientation with respect to wafer surface on rocking curve topographs and grazing incidence topographs. Applying ray tracing simulations, the configurations of BPDs can be determined, and the threading dislocations (TED, TSD and TMD) can be distinguished in grazing incidence topographs. The understanding of the nature and the distribution of these dislocations will help predict their propagation and movement under the application of voltage and laser, providing guidance for device fabrication.</description><identifier>ISSN: 0022-0248</identifier><identifier>EISSN: 1873-5002</identifier><identifier>DOI: 10.1016/j.jcrysgro.2021.126459</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>A1. Characterization ; A1. Defects ; A1. X-ray topography ; B1. Silicon carbide ; B2. Semiconducting materials ; Basal plane ; Edge dislocations ; Electric potential ; Grazing incidence ; Ray tracing ; Screw dislocations ; Silicon carbide ; Switches ; Synchrotron radiation ; Synchrotrons ; Threading dislocations ; Topography ; Voltage ; Wide bandgap semiconductors ; X ray topography</subject><ispartof>Journal of crystal growth, 2022-02, Vol.579 (C), p.126459, Article 126459</ispartof><rights>2021</rights><rights>Copyright Elsevier BV Feb 1, 2022</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c3309-589559ecfd7fec51f753f8b03e01bb58e6b67a10311378e9c2ebdb3b8bdecabd3</citedby><cites>FETCH-LOGICAL-c3309-589559ecfd7fec51f753f8b03e01bb58e6b67a10311378e9c2ebdb3b8bdecabd3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.jcrysgro.2021.126459$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>230,314,780,784,885,3548,27922,27923,45993</link.rule.ids><backlink>$$Uhttps://www.osti.gov/biblio/1868670$$D View this record in Osti.gov$$Hfree_for_read</backlink></links><search><creatorcontrib>Peng, Hongyu</creatorcontrib><creatorcontrib>Liu, Yafei</creatorcontrib><creatorcontrib>Chen, Zeyu</creatorcontrib><creatorcontrib>Cheng, Qianyu</creatorcontrib><creatorcontrib>Hu, Shanshan</creatorcontrib><creatorcontrib>Raghothamachar, Balaji</creatorcontrib><creatorcontrib>Dudley, Michael</creatorcontrib><creatorcontrib>Sampayan, Kristin</creatorcontrib><creatorcontrib>Sampayan, Stephen</creatorcontrib><title>Synchrotron X-ray topographic characterization of dislocations in 6H-SiC axial samples</title><title>Journal of crystal growth</title><description>•Different types of dislocations in axial 6H-SiC are revealed.•Different configurations of basal plane dislocations are investigated.•Different types of the threading dislocations are characterized.
Wide bandgap semiconductor, 6H-SiC, is being applied in photoconductive semiconductor switches (PCSS) due to its semi-insulating properties. The behavior of the dislocations in 6H- SiC under the application of voltage and laser in such devices is of particular interest. In this study, synchrotron X-ray transmission topography, grazing incidence topography and rocking curve topography are applied to characterize the types and distribution of defects in (1 1 –2 0) oriented wafers. Threading edge dislocations (TED), threading screw dislocations (TSD), threading mixed dislocation (TMD) and basal plane dislocations (BPD) in 6H-SiC axial samples are revealed in the X-ray topographs. TEDs are observed to be more likely off c-axis compared to TSDs/TMDs. Contrast features of BPDs differ depending on their Burgers vectors and orientation with respect to wafer surface on rocking curve topographs and grazing incidence topographs. Applying ray tracing simulations, the configurations of BPDs can be determined, and the threading dislocations (TED, TSD and TMD) can be distinguished in grazing incidence topographs. The understanding of the nature and the distribution of these dislocations will help predict their propagation and movement under the application of voltage and laser, providing guidance for device fabrication.</description><subject>A1. Characterization</subject><subject>A1. Defects</subject><subject>A1. X-ray topography</subject><subject>B1. Silicon carbide</subject><subject>B2. Semiconducting materials</subject><subject>Basal plane</subject><subject>Edge dislocations</subject><subject>Electric potential</subject><subject>Grazing incidence</subject><subject>Ray tracing</subject><subject>Screw dislocations</subject><subject>Silicon carbide</subject><subject>Switches</subject><subject>Synchrotron radiation</subject><subject>Synchrotrons</subject><subject>Threading dislocations</subject><subject>Topography</subject><subject>Voltage</subject><subject>Wide bandgap semiconductors</subject><subject>X ray topography</subject><issn>0022-0248</issn><issn>1873-5002</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2022</creationdate><recordtype>article</recordtype><recordid>eNqFkE9LxDAQxYMouK5-BSl67po0Jk1vyuI_EDysireQTKe7KWtTkyqun96s1bOHmWHg94Y3j5BjRmeMMnnWzloIm7gMflbQgs1YIc9FtUMmTJU8F5QWu2SSepHT4lztk4MYW0qTktEJeV5sOlgFPwTfZS95MJts8L1fBtOvHGSwMsHAgMF9mcElxDdZ7eLaw88aM9dl8jZfuHlmPp1ZZ9G89muMh2SvMeuIR79zSp6urx7nt_n9w83d_PI-B85plQtVCVEhNHXZIAjWlII3ylKOlFkrFEorS8MoZ4yXCiso0NaWW2VrBGNrPiUn410fB6cjuAFhBb7rEAbNlFSypAk6HaE--Ld3jINu_Xvoki9dSM5TiapMlBwpCD7GgI3ug3s1YaMZ1dugdav_gtbboPUYdBJejEJMj344DFsf2AHWLmxt1N79d-Ib9JaLJA</recordid><startdate>20220201</startdate><enddate>20220201</enddate><creator>Peng, Hongyu</creator><creator>Liu, Yafei</creator><creator>Chen, Zeyu</creator><creator>Cheng, Qianyu</creator><creator>Hu, Shanshan</creator><creator>Raghothamachar, Balaji</creator><creator>Dudley, Michael</creator><creator>Sampayan, Kristin</creator><creator>Sampayan, Stephen</creator><general>Elsevier B.V</general><general>Elsevier BV</general><general>Elsevier</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope><scope>OTOTI</scope></search><sort><creationdate>20220201</creationdate><title>Synchrotron X-ray topographic characterization of dislocations in 6H-SiC axial samples</title><author>Peng, Hongyu ; Liu, Yafei ; Chen, Zeyu ; Cheng, Qianyu ; Hu, Shanshan ; Raghothamachar, Balaji ; Dudley, Michael ; Sampayan, Kristin ; Sampayan, Stephen</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c3309-589559ecfd7fec51f753f8b03e01bb58e6b67a10311378e9c2ebdb3b8bdecabd3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2022</creationdate><topic>A1. Characterization</topic><topic>A1. Defects</topic><topic>A1. X-ray topography</topic><topic>B1. Silicon carbide</topic><topic>B2. Semiconducting materials</topic><topic>Basal plane</topic><topic>Edge dislocations</topic><topic>Electric potential</topic><topic>Grazing incidence</topic><topic>Ray tracing</topic><topic>Screw dislocations</topic><topic>Silicon carbide</topic><topic>Switches</topic><topic>Synchrotron radiation</topic><topic>Synchrotrons</topic><topic>Threading dislocations</topic><topic>Topography</topic><topic>Voltage</topic><topic>Wide bandgap semiconductors</topic><topic>X ray topography</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Peng, Hongyu</creatorcontrib><creatorcontrib>Liu, Yafei</creatorcontrib><creatorcontrib>Chen, Zeyu</creatorcontrib><creatorcontrib>Cheng, Qianyu</creatorcontrib><creatorcontrib>Hu, Shanshan</creatorcontrib><creatorcontrib>Raghothamachar, Balaji</creatorcontrib><creatorcontrib>Dudley, Michael</creatorcontrib><creatorcontrib>Sampayan, Kristin</creatorcontrib><creatorcontrib>Sampayan, Stephen</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>OSTI.GOV</collection><jtitle>Journal of crystal growth</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Peng, Hongyu</au><au>Liu, Yafei</au><au>Chen, Zeyu</au><au>Cheng, Qianyu</au><au>Hu, Shanshan</au><au>Raghothamachar, Balaji</au><au>Dudley, Michael</au><au>Sampayan, Kristin</au><au>Sampayan, Stephen</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synchrotron X-ray topographic characterization of dislocations in 6H-SiC axial samples</atitle><jtitle>Journal of crystal growth</jtitle><date>2022-02-01</date><risdate>2022</risdate><volume>579</volume><issue>C</issue><spage>126459</spage><pages>126459-</pages><artnum>126459</artnum><issn>0022-0248</issn><eissn>1873-5002</eissn><abstract>•Different types of dislocations in axial 6H-SiC are revealed.•Different configurations of basal plane dislocations are investigated.•Different types of the threading dislocations are characterized.
Wide bandgap semiconductor, 6H-SiC, is being applied in photoconductive semiconductor switches (PCSS) due to its semi-insulating properties. The behavior of the dislocations in 6H- SiC under the application of voltage and laser in such devices is of particular interest. In this study, synchrotron X-ray transmission topography, grazing incidence topography and rocking curve topography are applied to characterize the types and distribution of defects in (1 1 –2 0) oriented wafers. Threading edge dislocations (TED), threading screw dislocations (TSD), threading mixed dislocation (TMD) and basal plane dislocations (BPD) in 6H-SiC axial samples are revealed in the X-ray topographs. TEDs are observed to be more likely off c-axis compared to TSDs/TMDs. Contrast features of BPDs differ depending on their Burgers vectors and orientation with respect to wafer surface on rocking curve topographs and grazing incidence topographs. Applying ray tracing simulations, the configurations of BPDs can be determined, and the threading dislocations (TED, TSD and TMD) can be distinguished in grazing incidence topographs. The understanding of the nature and the distribution of these dislocations will help predict their propagation and movement under the application of voltage and laser, providing guidance for device fabrication.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><doi>10.1016/j.jcrysgro.2021.126459</doi><oa>free_for_read</oa></addata></record> |
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subjects | A1. Characterization A1. Defects A1. X-ray topography B1. Silicon carbide B2. Semiconducting materials Basal plane Edge dislocations Electric potential Grazing incidence Ray tracing Screw dislocations Silicon carbide Switches Synchrotron radiation Synchrotrons Threading dislocations Topography Voltage Wide bandgap semiconductors X ray topography |
title | Synchrotron X-ray topographic characterization of dislocations in 6H-SiC axial samples |
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