Raman and infrared spectra of plutonium (IV) oxalate and its thermal degradation products

For over 80 years, plutonium dioxide has been routinely produced via thermal decomposition of hydrated plutonium(IV) oxalate. Despite the longstanding utility of this process, the chemical structures of starting materials and intermediates produced during this thermal conversion remain ill-defined....

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Veröffentlicht in:	Journal of nuclear materials 2022-04, Vol.562, p.153574, Article 153574
Hauptverfasser:	Christian, Jonathan H., Foley, Bryan J., Ciprian, Elodia, Dick, Don D., Said, Meena, Darvin, Jason, Hixon, Amy E., Villa-Aleman, Eliel
Format:	Artikel
Sprache:	eng
Schlagworte:	Calcination Chemical compounds Computer applications Decomposition Degradation products Dioxides Infrared spectra Intermediates Mathematical models Non proliferation Nuclear forensics Nuclear fuels Oxalic acid Oxycarbides Plutonium Plutonium dioxide Plutonium oxalate RADIATION CHEMISTRY, RADIOCHEMISTRY, AND NUCLEAR CHEMISTRY Scanning electron microscopy Spectral bands Thermal decomposition Thermal degradation Vibrational spectra X ray powder diffraction X-ray diffraction
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