Microstructure Development of 308L Stainless Steel During Additive Manufacturing
In situ high-energy X-ray diffraction measurements were completed during deposition of 308L stainless steel wire onto a 304L stainless steel substrate. Attempts were made to extract microstructural features such as phase fraction and internal stress, as well as temperature evolution immediately foll...
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Veröffentlicht in: | Metallurgical and materials transactions. A, Physical metallurgy and materials science Physical metallurgy and materials science, 2019-05, Vol.50 (5), p.2538-2553 |
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creator | Brown, D. W. Losko, A. Carpenter, J. S. Cooley, J. C. Clausen, B. Dahal, J. Kenesei, P. Park, J.-S. |
description | In situ
high-energy X-ray diffraction measurements were completed during deposition of 308L stainless steel wire onto a 304L stainless steel substrate. Attempts were made to extract microstructural features such as phase fraction and internal stress, as well as temperature evolution immediately following the deposition. The limited data that could be collected during deposition and rapid solidification are critically examined. High-energy X-rays coupled with relatively slow detectors were utilized to enable determination of orientation-dependent lattice parameters accurately enough to comment on phase strain evolution between austenite and ferrite. Information about the hydrostatic and deviatoric stress states of the constituent phases was determined on time scales that are relevant to their development. However, the time resolution of the technique was insufficient to monitor phase evolution during the solid–solid phase transformation and, more so, during solidification. Moreover, the accurate and absolute determination of inherently statistical parameters, such as phase fraction, depends critically on the ability to sample a statistically significant numbers of grains in the microstructure. |
doi_str_mv | 10.1007/s11661-019-05169-1 |
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high-energy X-ray diffraction measurements were completed during deposition of 308L stainless steel wire onto a 304L stainless steel substrate. Attempts were made to extract microstructural features such as phase fraction and internal stress, as well as temperature evolution immediately following the deposition. The limited data that could be collected during deposition and rapid solidification are critically examined. High-energy X-rays coupled with relatively slow detectors were utilized to enable determination of orientation-dependent lattice parameters accurately enough to comment on phase strain evolution between austenite and ferrite. Information about the hydrostatic and deviatoric stress states of the constituent phases was determined on time scales that are relevant to their development. However, the time resolution of the technique was insufficient to monitor phase evolution during the solid–solid phase transformation and, more so, during solidification. Moreover, the accurate and absolute determination of inherently statistical parameters, such as phase fraction, depends critically on the ability to sample a statistically significant numbers of grains in the microstructure.</description><identifier>ISSN: 1073-5623</identifier><identifier>EISSN: 1543-1940</identifier><identifier>DOI: 10.1007/s11661-019-05169-1</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>additive manufacture ; Additive manufacturing ; Austenitic stainless steels ; Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Deposition ; ENGINEERING ; Evolution ; Feature extraction ; Iron constituents ; Lattice parameters ; MATERIALS SCIENCE ; Metallic Materials ; Microstructure ; Nanotechnology ; Phase transitions ; Rapid solidification ; Residual stress ; Solid phases ; Stainless steel ; Structural Materials ; Substrates ; Surfaces and Interfaces ; Temperature ; Thin Films ; X-ray diffraction</subject><ispartof>Metallurgical and materials transactions. A, Physical metallurgy and materials science, 2019-05, Vol.50 (5), p.2538-2553</ispartof><rights>The Minerals, Metals & Materials Society and ASM International 2019</rights><rights>Metallurgical and Materials Transactions A is a copyright of Springer, (2019). All Rights Reserved.</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c390t-774e05d04eb1053d86e9cc9f37c2c360663f5d94c26d1f51a828b35fa05fb8e13</citedby><cites>FETCH-LOGICAL-c390t-774e05d04eb1053d86e9cc9f37c2c360663f5d94c26d1f51a828b35fa05fb8e13</cites><orcidid>000000018821043X ; 000000033906846X ; 000000015307356X ; 0000000345658212 ; 0000000226492352</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s11661-019-05169-1$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s11661-019-05169-1$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>230,314,776,780,881,27901,27902,41464,42533,51294</link.rule.ids><backlink>$$Uhttps://www.osti.gov/servlets/purl/1511613$$D View this record in Osti.gov$$Hfree_for_read</backlink></links><search><creatorcontrib>Brown, D. W.</creatorcontrib><creatorcontrib>Losko, A.</creatorcontrib><creatorcontrib>Carpenter, J. S.</creatorcontrib><creatorcontrib>Cooley, J. C.</creatorcontrib><creatorcontrib>Clausen, B.</creatorcontrib><creatorcontrib>Dahal, J.</creatorcontrib><creatorcontrib>Kenesei, P.</creatorcontrib><creatorcontrib>Park, J.-S.</creatorcontrib><creatorcontrib>Los Alamos National Lab. (LANL), Los Alamos, NM (United States)</creatorcontrib><creatorcontrib>Argonne National Lab. (ANL), Argonne, IL (United States)</creatorcontrib><title>Microstructure Development of 308L Stainless Steel During Additive Manufacturing</title><title>Metallurgical and materials transactions. A, Physical metallurgy and materials science</title><addtitle>Metall Mater Trans A</addtitle><description>In situ
high-energy X-ray diffraction measurements were completed during deposition of 308L stainless steel wire onto a 304L stainless steel substrate. Attempts were made to extract microstructural features such as phase fraction and internal stress, as well as temperature evolution immediately following the deposition. The limited data that could be collected during deposition and rapid solidification are critically examined. High-energy X-rays coupled with relatively slow detectors were utilized to enable determination of orientation-dependent lattice parameters accurately enough to comment on phase strain evolution between austenite and ferrite. Information about the hydrostatic and deviatoric stress states of the constituent phases was determined on time scales that are relevant to their development. However, the time resolution of the technique was insufficient to monitor phase evolution during the solid–solid phase transformation and, more so, during solidification. Moreover, the accurate and absolute determination of inherently statistical parameters, such as phase fraction, depends critically on the ability to sample a statistically significant numbers of grains in the microstructure.</description><subject>additive manufacture</subject><subject>Additive manufacturing</subject><subject>Austenitic stainless steels</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>Deposition</subject><subject>ENGINEERING</subject><subject>Evolution</subject><subject>Feature extraction</subject><subject>Iron constituents</subject><subject>Lattice parameters</subject><subject>MATERIALS SCIENCE</subject><subject>Metallic Materials</subject><subject>Microstructure</subject><subject>Nanotechnology</subject><subject>Phase transitions</subject><subject>Rapid solidification</subject><subject>Residual stress</subject><subject>Solid phases</subject><subject>Stainless steel</subject><subject>Structural Materials</subject><subject>Substrates</subject><subject>Surfaces and Interfaces</subject><subject>Temperature</subject><subject>Thin Films</subject><subject>X-ray diffraction</subject><issn>1073-5623</issn><issn>1543-1940</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2019</creationdate><recordtype>article</recordtype><sourceid>8G5</sourceid><sourceid>BENPR</sourceid><sourceid>GUQSH</sourceid><sourceid>M2O</sourceid><recordid>eNp9kE1LxDAQhosouK7-AU9Fz9WZpknb47J-wi4K6jl004lm6bY1SRf896ZW8OZphuF5J5Mnis4RrhAgv3aIQmACWCbAUZQJHkQz5BlLsMzgMPSQs4SLlB1HJ85tAQLKxCx6XhtlO-ftoPxgKb6hPTVdv6PWx52OGRSr-MVXpm3IudARNfHNYE37Hi_q2nizp3hdtYOuxnwYn0ZHumocnf3WefR2d_u6fEhWT_ePy8UqUawEn-R5RsBryGiDwFldCCqVKjXLVaqYACGY5nWZqVTUqDlWRVpsGNcVcL0pCNk8upj2huONdMp4Uh-qa1tSXiIPPpAF6HKCett9DuS83HaDbcNdMsUyeEJW8EClEzWacJa07K3ZVfZLIshRr5z0yuBM_uiV4_tsCrl-_DbZv9X_pL4BH6x8Kg</recordid><startdate>20190501</startdate><enddate>20190501</enddate><creator>Brown, D. 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C.</creator><creator>Clausen, B.</creator><creator>Dahal, J.</creator><creator>Kenesei, P.</creator><creator>Park, J.-S.</creator><general>Springer US</general><general>Springer Nature B.V</general><general>ASM International</general><scope>AAYXX</scope><scope>CITATION</scope><scope>3V.</scope><scope>4T-</scope><scope>4U-</scope><scope>7SR</scope><scope>7XB</scope><scope>88I</scope><scope>8AF</scope><scope>8AO</scope><scope>8BQ</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>8FK</scope><scope>8G5</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>GNUQQ</scope><scope>GUQSH</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>L6V</scope><scope>M2O</scope><scope>M2P</scope><scope>M7S</scope><scope>MBDVC</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>PTHSS</scope><scope>Q9U</scope><scope>S0X</scope><scope>OIOZB</scope><scope>OTOTI</scope><orcidid>https://orcid.org/000000018821043X</orcidid><orcidid>https://orcid.org/000000033906846X</orcidid><orcidid>https://orcid.org/000000015307356X</orcidid><orcidid>https://orcid.org/0000000345658212</orcidid><orcidid>https://orcid.org/0000000226492352</orcidid></search><sort><creationdate>20190501</creationdate><title>Microstructure Development of 308L Stainless Steel During Additive Manufacturing</title><author>Brown, D. W. ; Losko, A. ; Carpenter, J. S. ; Cooley, J. C. ; Clausen, B. ; Dahal, J. ; Kenesei, P. ; Park, J.-S.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c390t-774e05d04eb1053d86e9cc9f37c2c360663f5d94c26d1f51a828b35fa05fb8e13</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2019</creationdate><topic>additive manufacture</topic><topic>Additive manufacturing</topic><topic>Austenitic stainless steels</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry and Materials Science</topic><topic>Deposition</topic><topic>ENGINEERING</topic><topic>Evolution</topic><topic>Feature extraction</topic><topic>Iron constituents</topic><topic>Lattice parameters</topic><topic>MATERIALS SCIENCE</topic><topic>Metallic Materials</topic><topic>Microstructure</topic><topic>Nanotechnology</topic><topic>Phase transitions</topic><topic>Rapid solidification</topic><topic>Residual stress</topic><topic>Solid phases</topic><topic>Stainless steel</topic><topic>Structural Materials</topic><topic>Substrates</topic><topic>Surfaces and Interfaces</topic><topic>Temperature</topic><topic>Thin Films</topic><topic>X-ray diffraction</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Brown, D. W.</creatorcontrib><creatorcontrib>Losko, A.</creatorcontrib><creatorcontrib>Carpenter, J. S.</creatorcontrib><creatorcontrib>Cooley, J. C.</creatorcontrib><creatorcontrib>Clausen, B.</creatorcontrib><creatorcontrib>Dahal, J.</creatorcontrib><creatorcontrib>Kenesei, P.</creatorcontrib><creatorcontrib>Park, J.-S.</creatorcontrib><creatorcontrib>Los Alamos National Lab. (LANL), Los Alamos, NM (United States)</creatorcontrib><creatorcontrib>Argonne National Lab. 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A, Physical metallurgy and materials science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Brown, D. W.</au><au>Losko, A.</au><au>Carpenter, J. S.</au><au>Cooley, J. C.</au><au>Clausen, B.</au><au>Dahal, J.</au><au>Kenesei, P.</au><au>Park, J.-S.</au><aucorp>Los Alamos National Lab. (LANL), Los Alamos, NM (United States)</aucorp><aucorp>Argonne National Lab. (ANL), Argonne, IL (United States)</aucorp><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Microstructure Development of 308L Stainless Steel During Additive Manufacturing</atitle><jtitle>Metallurgical and materials transactions. A, Physical metallurgy and materials science</jtitle><stitle>Metall Mater Trans A</stitle><date>2019-05-01</date><risdate>2019</risdate><volume>50</volume><issue>5</issue><spage>2538</spage><epage>2553</epage><pages>2538-2553</pages><issn>1073-5623</issn><eissn>1543-1940</eissn><abstract>In situ
high-energy X-ray diffraction measurements were completed during deposition of 308L stainless steel wire onto a 304L stainless steel substrate. Attempts were made to extract microstructural features such as phase fraction and internal stress, as well as temperature evolution immediately following the deposition. The limited data that could be collected during deposition and rapid solidification are critically examined. High-energy X-rays coupled with relatively slow detectors were utilized to enable determination of orientation-dependent lattice parameters accurately enough to comment on phase strain evolution between austenite and ferrite. Information about the hydrostatic and deviatoric stress states of the constituent phases was determined on time scales that are relevant to their development. However, the time resolution of the technique was insufficient to monitor phase evolution during the solid–solid phase transformation and, more so, during solidification. Moreover, the accurate and absolute determination of inherently statistical parameters, such as phase fraction, depends critically on the ability to sample a statistically significant numbers of grains in the microstructure.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s11661-019-05169-1</doi><tpages>16</tpages><orcidid>https://orcid.org/000000018821043X</orcidid><orcidid>https://orcid.org/000000033906846X</orcidid><orcidid>https://orcid.org/000000015307356X</orcidid><orcidid>https://orcid.org/0000000345658212</orcidid><orcidid>https://orcid.org/0000000226492352</orcidid><oa>free_for_read</oa></addata></record> |
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subjects | additive manufacture Additive manufacturing Austenitic stainless steels Characterization and Evaluation of Materials Chemistry and Materials Science Deposition ENGINEERING Evolution Feature extraction Iron constituents Lattice parameters MATERIALS SCIENCE Metallic Materials Microstructure Nanotechnology Phase transitions Rapid solidification Residual stress Solid phases Stainless steel Structural Materials Substrates Surfaces and Interfaces Temperature Thin Films X-ray diffraction |
title | Microstructure Development of 308L Stainless Steel During Additive Manufacturing |
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