Direct in situ observation of ZnO nucleation and growth via transmission X-ray microscopy
The nucleation and growth of a nanostructure controls its size and morphology, and ultimately its functional properties. Hence it is crucial to investigate growth mechanisms under relevant growth conditions at the nanometer length scale. Here we image the nucleation and growth of electrodeposited Zn...
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Veröffentlicht in: | Nanoscale 2016-01, Vol.8 (4), p.1849-1853 |
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creator | Tay, S E R Goode, A E Nelson Weker, J Cruickshank, A A Heutz, S Porter, A E Ryan, M P Toney, M F |
description | The nucleation and growth of a nanostructure controls its size and morphology, and ultimately its functional properties. Hence it is crucial to investigate growth mechanisms under relevant growth conditions at the nanometer length scale. Here we image the nucleation and growth of electrodeposited ZnO nanostructures in situ, using a transmission X-ray microscope and specially designed electrochemical cell. We show that this imaging technique leads to new insights into the nucleation and growth mechanisms in electrodeposited ZnO including direct, in situ observations of instantaneous versus delayed nucleation. |
doi_str_mv | 10.1039/c5nr07019h |
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We show that this imaging technique leads to new insights into the nucleation and growth mechanisms in electrodeposited ZnO including direct, in situ observations of instantaneous versus delayed nucleation.</description><subject>Electrochemical cells</subject><subject>Image transmission</subject><subject>Microscopes</subject><subject>Nanostructure</subject><subject>Nucleation</subject><subject>X-ray microscopy</subject><subject>X-rays</subject><subject>Zinc oxide</subject><issn>2040-3364</issn><issn>2040-3372</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2016</creationdate><recordtype>article</recordtype><recordid>eNo9kFtLxDAQhYMo3l_8ARJ8EqE6ado0eZT1soIoiIL6UtJp6kZ2kzVJlf33dl31aYY5H4c5h5ADBqcMuDrD0gWogKnJGtnOoYCM8ypf_99FsUV2YnwHEIoLvkm2clFxWUC1TV4ubDCYqHU02tRT30QTPnWy3lHf0Vd3T12PU7O6aNfSt-C_0oR-Wk1T0C7ObIxL7TkLekFnFoOP6OeLPbLR6Wk0-79zlzxdXT6Oxtnt_fXN6Pw2Qy55yppKFFwrmZedlly0OeOogAF0ZVc1gIWSKCvMIUfVGllio5VSrCiLtpWiRb5Ljla-PiZbR7TJ4AS9c0OsmuWlUJIP0PEKmgf_0ZuY6uFtNNOpdsb3sWYSJCjBKjGgJyt0GSQG09XzYGc6LGoG9bLvelTePfz0PR7gw1_fvpmZ9h_9K5h_A6lGerQ</recordid><startdate>20160101</startdate><enddate>20160101</enddate><creator>Tay, S E R</creator><creator>Goode, A E</creator><creator>Nelson Weker, J</creator><creator>Cruickshank, A A</creator><creator>Heutz, S</creator><creator>Porter, A E</creator><creator>Ryan, M P</creator><creator>Toney, M F</creator><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>F28</scope><scope>FR3</scope><scope>JG9</scope><scope>L7M</scope><scope>OTOTI</scope></search><sort><creationdate>20160101</creationdate><title>Direct in situ observation of ZnO nucleation and growth via transmission X-ray microscopy</title><author>Tay, S E R ; Goode, A E ; Nelson Weker, J ; Cruickshank, A A ; Heutz, S ; Porter, A E ; Ryan, M P ; Toney, M F</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c383t-b7643a9825fa836d213c90100f5f7b0c498c87c202c9de85cba9991454dd86dc3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2016</creationdate><topic>Electrochemical cells</topic><topic>Image transmission</topic><topic>Microscopes</topic><topic>Nanostructure</topic><topic>Nucleation</topic><topic>X-ray microscopy</topic><topic>X-rays</topic><topic>Zinc oxide</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Tay, S E R</creatorcontrib><creatorcontrib>Goode, A E</creatorcontrib><creatorcontrib>Nelson Weker, J</creatorcontrib><creatorcontrib>Cruickshank, A A</creatorcontrib><creatorcontrib>Heutz, S</creatorcontrib><creatorcontrib>Porter, A E</creatorcontrib><creatorcontrib>Ryan, M P</creatorcontrib><creatorcontrib>Toney, M F</creatorcontrib><creatorcontrib>SLAC National Accelerator Lab., Menlo Park, CA (United States)</creatorcontrib><collection>PubMed</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>ANTE: Abstracts in New Technology & Engineering</collection><collection>Engineering Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>OSTI.GOV</collection><jtitle>Nanoscale</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Tay, S E R</au><au>Goode, A E</au><au>Nelson Weker, J</au><au>Cruickshank, A A</au><au>Heutz, S</au><au>Porter, A E</au><au>Ryan, M P</au><au>Toney, M F</au><aucorp>SLAC National Accelerator Lab., Menlo Park, CA (United States)</aucorp><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Direct in situ observation of ZnO nucleation and growth via transmission X-ray microscopy</atitle><jtitle>Nanoscale</jtitle><addtitle>Nanoscale</addtitle><date>2016-01-01</date><risdate>2016</risdate><volume>8</volume><issue>4</issue><spage>1849</spage><epage>1853</epage><pages>1849-1853</pages><issn>2040-3364</issn><eissn>2040-3372</eissn><abstract>The nucleation and growth of a nanostructure controls its size and morphology, and ultimately its functional properties. 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subjects | Electrochemical cells Image transmission Microscopes Nanostructure Nucleation X-ray microscopy X-rays Zinc oxide |
title | Direct in situ observation of ZnO nucleation and growth via transmission X-ray microscopy |
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