Direct in situ observation of ZnO nucleation and growth via transmission X-ray microscopy

The nucleation and growth of a nanostructure controls its size and morphology, and ultimately its functional properties. Hence it is crucial to investigate growth mechanisms under relevant growth conditions at the nanometer length scale. Here we image the nucleation and growth of electrodeposited Zn...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Nanoscale 2016-01, Vol.8 (4), p.1849-1853
Hauptverfasser: Tay, S E R, Goode, A E, Nelson Weker, J, Cruickshank, A A, Heutz, S, Porter, A E, Ryan, M P, Toney, M F
Format: Artikel
Sprache:eng
Schlagworte:
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
container_end_page 1853
container_issue 4
container_start_page 1849
container_title Nanoscale
container_volume 8
creator Tay, S E R
Goode, A E
Nelson Weker, J
Cruickshank, A A
Heutz, S
Porter, A E
Ryan, M P
Toney, M F
description The nucleation and growth of a nanostructure controls its size and morphology, and ultimately its functional properties. Hence it is crucial to investigate growth mechanisms under relevant growth conditions at the nanometer length scale. Here we image the nucleation and growth of electrodeposited ZnO nanostructures in situ, using a transmission X-ray microscope and specially designed electrochemical cell. We show that this imaging technique leads to new insights into the nucleation and growth mechanisms in electrodeposited ZnO including direct, in situ observations of instantaneous versus delayed nucleation.
doi_str_mv 10.1039/c5nr07019h
format Article
fullrecord <record><control><sourceid>proquest_osti_</sourceid><recordid>TN_cdi_osti_scitechconnect_1256983</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>1808096176</sourcerecordid><originalsourceid>FETCH-LOGICAL-c383t-b7643a9825fa836d213c90100f5f7b0c498c87c202c9de85cba9991454dd86dc3</originalsourceid><addsrcrecordid>eNo9kFtLxDAQhYMo3l_8ARJ8EqE6ado0eZT1soIoiIL6UtJp6kZ2kzVJlf33dl31aYY5H4c5h5ADBqcMuDrD0gWogKnJGtnOoYCM8ypf_99FsUV2YnwHEIoLvkm2clFxWUC1TV4ubDCYqHU02tRT30QTPnWy3lHf0Vd3T12PU7O6aNfSt-C_0oR-Wk1T0C7ObIxL7TkLekFnFoOP6OeLPbLR6Wk0-79zlzxdXT6Oxtnt_fXN6Pw2Qy55yppKFFwrmZedlly0OeOogAF0ZVc1gIWSKCvMIUfVGllio5VSrCiLtpWiRb5Ljla-PiZbR7TJ4AS9c0OsmuWlUJIP0PEKmgf_0ZuY6uFtNNOpdsb3sWYSJCjBKjGgJyt0GSQG09XzYGc6LGoG9bLvelTePfz0PR7gw1_fvpmZ9h_9K5h_A6lGerQ</addsrcrecordid><sourcetype>Open Access Repository</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>1808096176</pqid></control><display><type>article</type><title>Direct in situ observation of ZnO nucleation and growth via transmission X-ray microscopy</title><source>Royal Society Of Chemistry Journals</source><source>Alma/SFX Local Collection</source><creator>Tay, S E R ; Goode, A E ; Nelson Weker, J ; Cruickshank, A A ; Heutz, S ; Porter, A E ; Ryan, M P ; Toney, M F</creator><creatorcontrib>Tay, S E R ; Goode, A E ; Nelson Weker, J ; Cruickshank, A A ; Heutz, S ; Porter, A E ; Ryan, M P ; Toney, M F ; SLAC National Accelerator Lab., Menlo Park, CA (United States)</creatorcontrib><description>The nucleation and growth of a nanostructure controls its size and morphology, and ultimately its functional properties. Hence it is crucial to investigate growth mechanisms under relevant growth conditions at the nanometer length scale. Here we image the nucleation and growth of electrodeposited ZnO nanostructures in situ, using a transmission X-ray microscope and specially designed electrochemical cell. We show that this imaging technique leads to new insights into the nucleation and growth mechanisms in electrodeposited ZnO including direct, in situ observations of instantaneous versus delayed nucleation.</description><identifier>ISSN: 2040-3364</identifier><identifier>EISSN: 2040-3372</identifier><identifier>DOI: 10.1039/c5nr07019h</identifier><identifier>PMID: 26738407</identifier><language>eng</language><publisher>England</publisher><subject>Electrochemical cells ; Image transmission ; Microscopes ; Nanostructure ; Nucleation ; X-ray microscopy ; X-rays ; Zinc oxide</subject><ispartof>Nanoscale, 2016-01, Vol.8 (4), p.1849-1853</ispartof><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c383t-b7643a9825fa836d213c90100f5f7b0c498c87c202c9de85cba9991454dd86dc3</citedby><cites>FETCH-LOGICAL-c383t-b7643a9825fa836d213c90100f5f7b0c498c87c202c9de85cba9991454dd86dc3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>230,315,781,785,886,27926,27927</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/26738407$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink><backlink>$$Uhttps://www.osti.gov/biblio/1256983$$D View this record in Osti.gov$$Hfree_for_read</backlink></links><search><creatorcontrib>Tay, S E R</creatorcontrib><creatorcontrib>Goode, A E</creatorcontrib><creatorcontrib>Nelson Weker, J</creatorcontrib><creatorcontrib>Cruickshank, A A</creatorcontrib><creatorcontrib>Heutz, S</creatorcontrib><creatorcontrib>Porter, A E</creatorcontrib><creatorcontrib>Ryan, M P</creatorcontrib><creatorcontrib>Toney, M F</creatorcontrib><creatorcontrib>SLAC National Accelerator Lab., Menlo Park, CA (United States)</creatorcontrib><title>Direct in situ observation of ZnO nucleation and growth via transmission X-ray microscopy</title><title>Nanoscale</title><addtitle>Nanoscale</addtitle><description>The nucleation and growth of a nanostructure controls its size and morphology, and ultimately its functional properties. Hence it is crucial to investigate growth mechanisms under relevant growth conditions at the nanometer length scale. Here we image the nucleation and growth of electrodeposited ZnO nanostructures in situ, using a transmission X-ray microscope and specially designed electrochemical cell. We show that this imaging technique leads to new insights into the nucleation and growth mechanisms in electrodeposited ZnO including direct, in situ observations of instantaneous versus delayed nucleation.</description><subject>Electrochemical cells</subject><subject>Image transmission</subject><subject>Microscopes</subject><subject>Nanostructure</subject><subject>Nucleation</subject><subject>X-ray microscopy</subject><subject>X-rays</subject><subject>Zinc oxide</subject><issn>2040-3364</issn><issn>2040-3372</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2016</creationdate><recordtype>article</recordtype><recordid>eNo9kFtLxDAQhYMo3l_8ARJ8EqE6ado0eZT1soIoiIL6UtJp6kZ2kzVJlf33dl31aYY5H4c5h5ADBqcMuDrD0gWogKnJGtnOoYCM8ypf_99FsUV2YnwHEIoLvkm2clFxWUC1TV4ubDCYqHU02tRT30QTPnWy3lHf0Vd3T12PU7O6aNfSt-C_0oR-Wk1T0C7ObIxL7TkLekFnFoOP6OeLPbLR6Wk0-79zlzxdXT6Oxtnt_fXN6Pw2Qy55yppKFFwrmZedlly0OeOogAF0ZVc1gIWSKCvMIUfVGllio5VSrCiLtpWiRb5Ljla-PiZbR7TJ4AS9c0OsmuWlUJIP0PEKmgf_0ZuY6uFtNNOpdsb3sWYSJCjBKjGgJyt0GSQG09XzYGc6LGoG9bLvelTePfz0PR7gw1_fvpmZ9h_9K5h_A6lGerQ</recordid><startdate>20160101</startdate><enddate>20160101</enddate><creator>Tay, S E R</creator><creator>Goode, A E</creator><creator>Nelson Weker, J</creator><creator>Cruickshank, A A</creator><creator>Heutz, S</creator><creator>Porter, A E</creator><creator>Ryan, M P</creator><creator>Toney, M F</creator><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>F28</scope><scope>FR3</scope><scope>JG9</scope><scope>L7M</scope><scope>OTOTI</scope></search><sort><creationdate>20160101</creationdate><title>Direct in situ observation of ZnO nucleation and growth via transmission X-ray microscopy</title><author>Tay, S E R ; Goode, A E ; Nelson Weker, J ; Cruickshank, A A ; Heutz, S ; Porter, A E ; Ryan, M P ; Toney, M F</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c383t-b7643a9825fa836d213c90100f5f7b0c498c87c202c9de85cba9991454dd86dc3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2016</creationdate><topic>Electrochemical cells</topic><topic>Image transmission</topic><topic>Microscopes</topic><topic>Nanostructure</topic><topic>Nucleation</topic><topic>X-ray microscopy</topic><topic>X-rays</topic><topic>Zinc oxide</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Tay, S E R</creatorcontrib><creatorcontrib>Goode, A E</creatorcontrib><creatorcontrib>Nelson Weker, J</creatorcontrib><creatorcontrib>Cruickshank, A A</creatorcontrib><creatorcontrib>Heutz, S</creatorcontrib><creatorcontrib>Porter, A E</creatorcontrib><creatorcontrib>Ryan, M P</creatorcontrib><creatorcontrib>Toney, M F</creatorcontrib><creatorcontrib>SLAC National Accelerator Lab., Menlo Park, CA (United States)</creatorcontrib><collection>PubMed</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>ANTE: Abstracts in New Technology &amp; Engineering</collection><collection>Engineering Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>OSTI.GOV</collection><jtitle>Nanoscale</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Tay, S E R</au><au>Goode, A E</au><au>Nelson Weker, J</au><au>Cruickshank, A A</au><au>Heutz, S</au><au>Porter, A E</au><au>Ryan, M P</au><au>Toney, M F</au><aucorp>SLAC National Accelerator Lab., Menlo Park, CA (United States)</aucorp><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Direct in situ observation of ZnO nucleation and growth via transmission X-ray microscopy</atitle><jtitle>Nanoscale</jtitle><addtitle>Nanoscale</addtitle><date>2016-01-01</date><risdate>2016</risdate><volume>8</volume><issue>4</issue><spage>1849</spage><epage>1853</epage><pages>1849-1853</pages><issn>2040-3364</issn><eissn>2040-3372</eissn><abstract>The nucleation and growth of a nanostructure controls its size and morphology, and ultimately its functional properties. Hence it is crucial to investigate growth mechanisms under relevant growth conditions at the nanometer length scale. Here we image the nucleation and growth of electrodeposited ZnO nanostructures in situ, using a transmission X-ray microscope and specially designed electrochemical cell. We show that this imaging technique leads to new insights into the nucleation and growth mechanisms in electrodeposited ZnO including direct, in situ observations of instantaneous versus delayed nucleation.</abstract><cop>England</cop><pmid>26738407</pmid><doi>10.1039/c5nr07019h</doi><tpages>5</tpages><oa>free_for_read</oa></addata></record>
fulltext fulltext
identifier ISSN: 2040-3364
ispartof Nanoscale, 2016-01, Vol.8 (4), p.1849-1853
issn 2040-3364
2040-3372
language eng
recordid cdi_osti_scitechconnect_1256983
source Royal Society Of Chemistry Journals; Alma/SFX Local Collection
subjects Electrochemical cells
Image transmission
Microscopes
Nanostructure
Nucleation
X-ray microscopy
X-rays
Zinc oxide
title Direct in situ observation of ZnO nucleation and growth via transmission X-ray microscopy
url https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2024-12-17T19%3A21%3A42IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_osti_&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Direct%20in%20situ%20observation%20of%20ZnO%20nucleation%20and%20growth%20via%20transmission%20X-ray%20microscopy&rft.jtitle=Nanoscale&rft.au=Tay,%20S%20E%20R&rft.aucorp=SLAC%20National%20Accelerator%20Lab.,%20Menlo%20Park,%20CA%20(United%20States)&rft.date=2016-01-01&rft.volume=8&rft.issue=4&rft.spage=1849&rft.epage=1853&rft.pages=1849-1853&rft.issn=2040-3364&rft.eissn=2040-3372&rft_id=info:doi/10.1039/c5nr07019h&rft_dat=%3Cproquest_osti_%3E1808096176%3C/proquest_osti_%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=1808096176&rft_id=info:pmid/26738407&rfr_iscdi=true