Solidification and loss of hydrostaticity in liquid media used for pressure measurements
We carried out a study of the pressure dependence of the solidification temperature in nine pressure transmitting media that are liquid at ambient temperature, under pressures up to 2.3 GPa. These fluids are 1:1 isopentane/n-pentane, 4:6 light mineral oil/n-pentane, 1:1 isoamyl alcohol/n-pentane, 4:...
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creator | Torikachvili, M S Kim, S K Colombier, E Bud'ko, S L Canfield, P C |
description | We carried out a study of the pressure dependence of the solidification temperature in nine pressure transmitting media that are liquid at ambient temperature, under pressures up to 2.3 GPa. These fluids are 1:1 isopentane/n-pentane, 4:6 light mineral oil/n-pentane, 1:1 isoamyl alcohol/n-pentane, 4:1 methanol/ethanol, 1:1 FC72/FC84 (Fluorinert), Daphne 7373, isopentane, and Dow Corning PMX silicone oils 200 and 60,000 cS. We relied on the high sensitivity of the electrical resistivity of Ba(Fe(1-x)Ru(x))2As2 single crystals to the freezing of the pressure media and cross-checked with corresponding anomalies observed in the resistance of the manganin coil that served as the ambient temperature resistive manometer. In addition to establishing the temperature-pressure line separating the liquid (hydrostatic) and frozen (non-hydrostatic) phases, these data permit rough estimates of the freezing pressure of these media at ambient temperature. This pressure establishes the extreme limit for the medium to be considered hydrostatic. For higher applied pressures, the medium has to be treated as non-hydrostatic. |
doi_str_mv | 10.1063/1.4937478 |
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These fluids are 1:1 isopentane/n-pentane, 4:6 light mineral oil/n-pentane, 1:1 isoamyl alcohol/n-pentane, 4:1 methanol/ethanol, 1:1 FC72/FC84 (Fluorinert), Daphne 7373, isopentane, and Dow Corning PMX silicone oils 200 and 60,000 cS. We relied on the high sensitivity of the electrical resistivity of Ba(Fe(1-x)Ru(x))2As2 single crystals to the freezing of the pressure media and cross-checked with corresponding anomalies observed in the resistance of the manganin coil that served as the ambient temperature resistive manometer. In addition to establishing the temperature-pressure line separating the liquid (hydrostatic) and frozen (non-hydrostatic) phases, these data permit rough estimates of the freezing pressure of these media at ambient temperature. This pressure establishes the extreme limit for the medium to be considered hydrostatic. For higher applied pressures, the medium has to be treated as non-hydrostatic.</description><identifier>ISSN: 0034-6748</identifier><identifier>EISSN: 1089-7623</identifier><identifier>DOI: 10.1063/1.4937478</identifier><identifier>PMID: 26724044</identifier><language>eng</language><publisher>United States: American Institute of Physics</publisher><subject>Ambient temperature ; electrical resistivity ; Ethanol ; Freezing ; glass transitions ; high pressure ; hydrostatics ; Manganin ; Mineral oils ; OTHER INSTRUMENTATION ; Pressure dependence ; Scientific apparatus & instruments ; Single crystals ; Solidification ; Temperature dependence</subject><ispartof>Review of scientific instruments, 2015-12, Vol.86 (12), p.123904-123904</ispartof><rights>2015 AIP Publishing LLC.</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c441t-2bba4a8e5fd659ea342c92d6f527b2e65ad1ca854a5b27b9e8bf04b3b91154d83</citedby><cites>FETCH-LOGICAL-c441t-2bba4a8e5fd659ea342c92d6f527b2e65ad1ca854a5b27b9e8bf04b3b91154d83</cites><orcidid>0000-0003-1651-3655 ; 0000000316513655</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>230,314,777,781,882,27905,27906</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/26724044$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink><backlink>$$Uhttps://www.osti.gov/servlets/purl/1249336$$D View this record in Osti.gov$$Hfree_for_read</backlink></links><search><creatorcontrib>Torikachvili, M S</creatorcontrib><creatorcontrib>Kim, S K</creatorcontrib><creatorcontrib>Colombier, E</creatorcontrib><creatorcontrib>Bud'ko, S L</creatorcontrib><creatorcontrib>Canfield, P C</creatorcontrib><creatorcontrib>Ames Laboratory (AMES), Ames, IA (United States)</creatorcontrib><title>Solidification and loss of hydrostaticity in liquid media used for pressure measurements</title><title>Review of scientific instruments</title><addtitle>Rev Sci Instrum</addtitle><description>We carried out a study of the pressure dependence of the solidification temperature in nine pressure transmitting media that are liquid at ambient temperature, under pressures up to 2.3 GPa. These fluids are 1:1 isopentane/n-pentane, 4:6 light mineral oil/n-pentane, 1:1 isoamyl alcohol/n-pentane, 4:1 methanol/ethanol, 1:1 FC72/FC84 (Fluorinert), Daphne 7373, isopentane, and Dow Corning PMX silicone oils 200 and 60,000 cS. We relied on the high sensitivity of the electrical resistivity of Ba(Fe(1-x)Ru(x))2As2 single crystals to the freezing of the pressure media and cross-checked with corresponding anomalies observed in the resistance of the manganin coil that served as the ambient temperature resistive manometer. In addition to establishing the temperature-pressure line separating the liquid (hydrostatic) and frozen (non-hydrostatic) phases, these data permit rough estimates of the freezing pressure of these media at ambient temperature. This pressure establishes the extreme limit for the medium to be considered hydrostatic. For higher applied pressures, the medium has to be treated as non-hydrostatic.</description><subject>Ambient temperature</subject><subject>electrical resistivity</subject><subject>Ethanol</subject><subject>Freezing</subject><subject>glass transitions</subject><subject>high pressure</subject><subject>hydrostatics</subject><subject>Manganin</subject><subject>Mineral oils</subject><subject>OTHER INSTRUMENTATION</subject><subject>Pressure dependence</subject><subject>Scientific apparatus & instruments</subject><subject>Single crystals</subject><subject>Solidification</subject><subject>Temperature dependence</subject><issn>0034-6748</issn><issn>1089-7623</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2015</creationdate><recordtype>article</recordtype><recordid>eNpdkU1LAzEQhoMotlYP_gEJetHD1nxn9yjFLyh4UMFbyCZZmrK7qcnuof_elFYPzuWFmYdh5n0BuMRojpGg93jOKiqZLI_AFKOyKqQg9BhMEaKsEJKVE3CW0hrl4hifggkRkjDE2BR8vYfWW994owcfeqh7C9uQEgwNXG1tDGnIA-OHLfQ9bP336C3snPUajslZ2IQIN9GlNEaX-3qnneuHdA5OGt0md3HQGfh8evxYvBTLt-fXxcOyMIzhoSB1rZkuHW-s4JXTlBFTESsaTmRNnODaYqNLzjSvc6dyZd0gVtO6wpgzW9IZuN7vzZd6lfKlzqxM6HtnBoVJNoaKDN3uoU0M36NLg-p8Mq5tde_CmBSWnCJUMcozevMPXYcx9vkFRTChUiLJZabu9pTJDqXoGrWJvtNxqzBSu0wUVodMMnt12DjW2bk_8jcE-gOD04Xt</recordid><startdate>20151201</startdate><enddate>20151201</enddate><creator>Torikachvili, M S</creator><creator>Kim, S K</creator><creator>Colombier, E</creator><creator>Bud'ko, S L</creator><creator>Canfield, P C</creator><general>American Institute of Physics</general><general>American Institute of Physics (AIP)</general><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>8FD</scope><scope>H8D</scope><scope>L7M</scope><scope>7X8</scope><scope>OIOZB</scope><scope>OTOTI</scope><orcidid>https://orcid.org/0000-0003-1651-3655</orcidid><orcidid>https://orcid.org/0000000316513655</orcidid></search><sort><creationdate>20151201</creationdate><title>Solidification and loss of hydrostaticity in liquid media used for pressure measurements</title><author>Torikachvili, M S ; Kim, S K ; Colombier, E ; Bud'ko, S L ; Canfield, P C</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c441t-2bba4a8e5fd659ea342c92d6f527b2e65ad1ca854a5b27b9e8bf04b3b91154d83</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2015</creationdate><topic>Ambient temperature</topic><topic>electrical resistivity</topic><topic>Ethanol</topic><topic>Freezing</topic><topic>glass transitions</topic><topic>high pressure</topic><topic>hydrostatics</topic><topic>Manganin</topic><topic>Mineral oils</topic><topic>OTHER INSTRUMENTATION</topic><topic>Pressure dependence</topic><topic>Scientific apparatus & instruments</topic><topic>Single crystals</topic><topic>Solidification</topic><topic>Temperature dependence</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Torikachvili, M S</creatorcontrib><creatorcontrib>Kim, S K</creatorcontrib><creatorcontrib>Colombier, E</creatorcontrib><creatorcontrib>Bud'ko, S L</creatorcontrib><creatorcontrib>Canfield, P C</creatorcontrib><creatorcontrib>Ames Laboratory (AMES), Ames, IA (United States)</creatorcontrib><collection>PubMed</collection><collection>CrossRef</collection><collection>Technology Research Database</collection><collection>Aerospace Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>MEDLINE - Academic</collection><collection>OSTI.GOV - Hybrid</collection><collection>OSTI.GOV</collection><jtitle>Review of scientific instruments</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Torikachvili, M S</au><au>Kim, S K</au><au>Colombier, E</au><au>Bud'ko, S L</au><au>Canfield, P C</au><aucorp>Ames Laboratory (AMES), Ames, IA (United States)</aucorp><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Solidification and loss of hydrostaticity in liquid media used for pressure measurements</atitle><jtitle>Review of scientific instruments</jtitle><addtitle>Rev Sci Instrum</addtitle><date>2015-12-01</date><risdate>2015</risdate><volume>86</volume><issue>12</issue><spage>123904</spage><epage>123904</epage><pages>123904-123904</pages><issn>0034-6748</issn><eissn>1089-7623</eissn><abstract>We carried out a study of the pressure dependence of the solidification temperature in nine pressure transmitting media that are liquid at ambient temperature, under pressures up to 2.3 GPa. These fluids are 1:1 isopentane/n-pentane, 4:6 light mineral oil/n-pentane, 1:1 isoamyl alcohol/n-pentane, 4:1 methanol/ethanol, 1:1 FC72/FC84 (Fluorinert), Daphne 7373, isopentane, and Dow Corning PMX silicone oils 200 and 60,000 cS. We relied on the high sensitivity of the electrical resistivity of Ba(Fe(1-x)Ru(x))2As2 single crystals to the freezing of the pressure media and cross-checked with corresponding anomalies observed in the resistance of the manganin coil that served as the ambient temperature resistive manometer. In addition to establishing the temperature-pressure line separating the liquid (hydrostatic) and frozen (non-hydrostatic) phases, these data permit rough estimates of the freezing pressure of these media at ambient temperature. This pressure establishes the extreme limit for the medium to be considered hydrostatic. 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subjects | Ambient temperature electrical resistivity Ethanol Freezing glass transitions high pressure hydrostatics Manganin Mineral oils OTHER INSTRUMENTATION Pressure dependence Scientific apparatus & instruments Single crystals Solidification Temperature dependence |
title | Solidification and loss of hydrostaticity in liquid media used for pressure measurements |
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