Revealing the Mechanisms behind SnO2 Nanoparticle Formation and Growth during Hydrothermal Synthesis: An In Situ Total Scattering Study

The formation and growth mechanisms in the hydrothermal synthesis of SnO2 nanoparticles from aqueous solutions of SnCl4·5H2O have been elucidated by means of in situ X-ray total scattering (PDF) measurements. The analysis of the data reveals that when the tin(IV) chloride precursor is dissolved, chl...

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Veröffentlicht in:	Journal of the American Chemical Society 2012-04, Vol.134 (15), p.6785-6792
Hauptverfasser:	Jensen, Kirsten M. Ø., Christensen, Mogens, Juhas, Pavol, Tyrsted, Christoffer, Bøjesen, Espen D., Lock, Nina, Billinge, Simon J. L., Iversen, Bo B.
Format:	Artikel
Sprache:	eng
Schlagworte:	AQUEOUS SOLUTIONS CHLORIDES CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY DIFFUSION HEATING HYDROTHERMAL SYNTHESIS in situ x-ray total scattering (PDF) measurements ions metal oxide nanoparticles MORPHOLOGY nanoparticles Ostwald ripening PARTICLE SIZE PRECURSOR RIPENING RUTILE SCATTERING SYNTHESIS temperature TETRAGONAL LATTICES tin tin dioxide WATER X-radiation
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