Class H Oil Well Cement Hydration at Elevated Temperatures in the Presence of Retarding Agents: An In Situ High-Energy X-ray Diffraction Study
In situ powder X-ray diffraction was used to examine the hydration of API Class H cement slurries, with a water-to-cement ratio of 0.394, at 66, 93, 121, and 177 °C under autogenous pressure in the presence of varying amounts of the additives tartaric acid, modified lignosulfonate, and AMPS (2-acryl...
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| Veröffentlicht in: | Industrial & engineering chemistry research 2005-07, Vol.44 (15), p.5579-5584 |
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| container_title | Industrial & engineering chemistry research |
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| creator | Jupe, Andrew C Wilkinson, Angus P Luke, Karen Funkhouser, Gary P |
| description | In situ powder X-ray diffraction was used to examine the hydration of API Class H cement slurries, with a water-to-cement ratio of 0.394, at 66, 93, 121, and 177 °C under autogenous pressure in the presence of varying amounts of the additives tartaric acid, modified lignosulfonate, and AMPS (2-acrylamido-2-methylpropanesulfonic acid) copolymer. All of these retarding agents inhibited the hydration of crystalline C3S (Ca3SiO5), but other modes of action were also apparent. The formation of ettringite was suppressed when tartaric acid was used by itself or in combination with other additives. Changes in the hydration of C3S vs time could not be correlated in a simple way with the observed pumping times for the cement slurries. The largest changes in pumping time as a function of temperature occurred in a temperature interval where ettringite/monosulfate decomposes and crystalline hydrogarnet starts to be formed. |
| doi_str_mv | 10.1021/ie049085t |
| format | Article |
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(ANL), Argonne, IL (United States). Advanced Photon Source (APS)</creatorcontrib><title>Class H Oil Well Cement Hydration at Elevated Temperatures in the Presence of Retarding Agents: An In Situ High-Energy X-ray Diffraction Study</title><title>Industrial & engineering chemistry research</title><addtitle>Ind. Eng. Chem. Res</addtitle><description>In situ powder X-ray diffraction was used to examine the hydration of API Class H cement slurries, with a water-to-cement ratio of 0.394, at 66, 93, 121, and 177 °C under autogenous pressure in the presence of varying amounts of the additives tartaric acid, modified lignosulfonate, and AMPS (2-acrylamido-2-methylpropanesulfonic acid) copolymer. All of these retarding agents inhibited the hydration of crystalline C3S (Ca3SiO5), but other modes of action were also apparent. The formation of ettringite was suppressed when tartaric acid was used by itself or in combination with other additives. Changes in the hydration of C3S vs time could not be correlated in a simple way with the observed pumping times for the cement slurries. The largest changes in pumping time as a function of temperature occurred in a temperature interval where ettringite/monosulfate decomposes and crystalline hydrogarnet starts to be formed.</description><subject>02 PETROLEUM</subject><subject>ADDITIVES</subject><subject>Applied sciences</subject><subject>CEMENTS</subject><subject>Chemical engineering</subject><subject>Exact sciences and technology</subject><subject>HYDRATION</subject><subject>OIL WELLS</subject><subject>PUMPING</subject><subject>SLURRIES</subject><subject>TARTARIC ACID</subject><subject>X-RAY DIFFRACTION</subject><issn>0888-5885</issn><issn>1520-5045</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2005</creationdate><recordtype>article</recordtype><recordid>eNptkMFuEzEQhi0EEqFw4A1GSBw4bLF37V0vtyiEpqioFQmi4mK53nHisvFGtlOxN64cecU-CYZU7YXTjGa--X_NT8hLRo8ZLdlbh5S3VIr0iEyYKGkhKBePyYRKKQshpXhKnsV4TSkVgvMJ-T3rdYywgHPXw1fse5jhFn2CxdgFndzgQSeY93ijE3awwu0O83wfMILzkDYIF7lHbxAGC58x6dA5v4bpOqvEd7c_f8HUw6mHpUt7WLj1pph7DOsRLougR3jvrA3a_HNapn03PidPrO4jvrirR-TLh_lqtijOzk9OZ9OzQleCp6JsS6pr0TYNshLbK41oZdVySw3vBFadLc0VpbrhhnV1w20lbMNkberGasba6oi8OugOMTkVjUtoNmbwHk1SjFJZN1WG3hwgE4YYA1q1C26rw5gJ9TdwdR94Zl8f2J2ORvf5K29cfDioW1FzITNXHDgXE_643-vwXWXLRqjVxVKVJ99o-7H9pC4fdLWJ6nrYB59j-Y__HxM5nAQ</recordid><startdate>20050720</startdate><enddate>20050720</enddate><creator>Jupe, Andrew C</creator><creator>Wilkinson, Angus P</creator><creator>Luke, Karen</creator><creator>Funkhouser, Gary P</creator><general>American Chemical Society</general><scope>BSCLL</scope><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>OTOTI</scope></search><sort><creationdate>20050720</creationdate><title>Class H Oil Well Cement Hydration at Elevated Temperatures in the Presence of Retarding Agents: An In Situ High-Energy X-ray Diffraction Study</title><author>Jupe, Andrew C ; Wilkinson, Angus P ; Luke, Karen ; Funkhouser, Gary P</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-a354t-2920a65977e12e9baeef8394f0c4d5e3df2cb00a74c1d674f35f7186c67fa1193</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2005</creationdate><topic>02 PETROLEUM</topic><topic>ADDITIVES</topic><topic>Applied sciences</topic><topic>CEMENTS</topic><topic>Chemical engineering</topic><topic>Exact sciences and technology</topic><topic>HYDRATION</topic><topic>OIL WELLS</topic><topic>PUMPING</topic><topic>SLURRIES</topic><topic>TARTARIC ACID</topic><topic>X-RAY DIFFRACTION</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Jupe, Andrew C</creatorcontrib><creatorcontrib>Wilkinson, Angus P</creatorcontrib><creatorcontrib>Luke, Karen</creatorcontrib><creatorcontrib>Funkhouser, Gary P</creatorcontrib><creatorcontrib>Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)</creatorcontrib><collection>Istex</collection><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>OSTI.GOV</collection><jtitle>Industrial & engineering chemistry research</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Jupe, Andrew C</au><au>Wilkinson, Angus P</au><au>Luke, Karen</au><au>Funkhouser, Gary P</au><aucorp>Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)</aucorp><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Class H Oil Well Cement Hydration at Elevated Temperatures in the Presence of Retarding Agents: An In Situ High-Energy X-ray Diffraction Study</atitle><jtitle>Industrial & engineering chemistry research</jtitle><addtitle>Ind. Eng. Chem. Res</addtitle><date>2005-07-20</date><risdate>2005</risdate><volume>44</volume><issue>15</issue><spage>5579</spage><epage>5584</epage><pages>5579-5584</pages><issn>0888-5885</issn><eissn>1520-5045</eissn><coden>IECRED</coden><abstract>In situ powder X-ray diffraction was used to examine the hydration of API Class H cement slurries, with a water-to-cement ratio of 0.394, at 66, 93, 121, and 177 °C under autogenous pressure in the presence of varying amounts of the additives tartaric acid, modified lignosulfonate, and AMPS (2-acrylamido-2-methylpropanesulfonic acid) copolymer. All of these retarding agents inhibited the hydration of crystalline C3S (Ca3SiO5), but other modes of action were also apparent. The formation of ettringite was suppressed when tartaric acid was used by itself or in combination with other additives. Changes in the hydration of C3S vs time could not be correlated in a simple way with the observed pumping times for the cement slurries. The largest changes in pumping time as a function of temperature occurred in a temperature interval where ettringite/monosulfate decomposes and crystalline hydrogarnet starts to be formed.</abstract><cop>Washington, DC</cop><pub>American Chemical Society</pub><doi>10.1021/ie049085t</doi><tpages>6</tpages></addata></record> |
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| ispartof | Industrial & engineering chemistry research, 2005-07, Vol.44 (15), p.5579-5584 |
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| source | American Chemical Society Journals |
| subjects | 02 PETROLEUM ADDITIVES Applied sciences CEMENTS Chemical engineering Exact sciences and technology HYDRATION OIL WELLS PUMPING SLURRIES TARTARIC ACID X-RAY DIFFRACTION |
| title | Class H Oil Well Cement Hydration at Elevated Temperatures in the Presence of Retarding Agents: An In Situ High-Energy X-ray Diffraction Study |
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