GC/MS를 이용한 혈액 중 유기인제류 농약의 동시 분석에 관한 방법의 유효화

GC/MS를 이용한 혈액 중 유기인제류 농약의 동시 분석에 관한 방법의 유효화

The purpose of this study was to provide the standard method for the analysis of organophosphorous pesticides such as chlorpyrifos, diazinon, malathion and parathion in blood. We performed method validation for these pesticides in blood according to EURACHEM (A focus For Analytical Chemistry in Euro...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:환경독성학회지 2005, Vol.20 (4), p.297-302
Hauptverfasser: 박미정, 양자열, 김기욱, 박유신, 정희선, 이상기, Park Mee Jung, Yang Ja Youl, Kim Ki Wook, Park Yoo Shin, Chung Hee Sun, Lee Sang Ki
Format: Artikel
Sprache:kor
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
container_end_page 302
container_issue 4
container_start_page 297
container_title 환경독성학회지
container_volume 20
creator 박미정
양자열
김기욱
박유신
정희선
이상기
Park Mee Jung
Yang Ja Youl
Kim Ki Wook
Park Yoo Shin
Chung Hee Sun
Lee Sang Ki
description The purpose of this study was to provide the standard method for the analysis of organophosphorous pesticides such as chlorpyrifos, diazinon, malathion and parathion in blood. We performed method validation for these pesticides in blood according to EURACHEM (A focus For Analytical Chemistry in Europe) guide. For the analysis of the pesticides, we used solid-phase extraction ,column (Waters Oasis $HLB^{(R)}$. After the extraction, the supernatants were evaporated to dryness under the nitrogen stream. They were analyzed by gas chromatography/mass spectrometry (GC/MS) after reconstituting with ethanol. Terbufos was used as an internal standard. To validate this method, we performed verification procedures with the following parameters: selectivity, linearity of calibration, accuracy, precision, limit of detection and quantification. Validation data according to Eurachem guide were adequate for our purpose for the analysis of chlorpyrifos, diazinon, malathion and parathion in blood.
format Article
fullrecord <record><control><sourceid>kisti</sourceid><recordid>TN_cdi_kisti_ndsl_JAKO200511722570618</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>JAKO200511722570618</sourcerecordid><originalsourceid>FETCH-kisti_ndsl_JAKO2005117225706183</originalsourceid><addsrcrecordid>eNpjYeA0NDIy07U0NLXgYOAtLs5MMjAwNDQwNza25GRIdnfW9w1-vXSPwpu5W97MWvl26hyFtzM63kxdqPBmyUSFN3MWvNqx4c3cHW8WzHm9dIbC67beN1P3vpkLZPXPfNM9R-H1tpY3LXPfTJ-g8GpLA0jz6w0rX2-aClIB1Pt21oq3M6fwMLCmJeYUp_JCaW4GVTfXEGcP3ezM4pLM-LyU4px4L0dvfyMDA1NDQ3MjI1NzAzNDC2Ni1QEALpVeSA</addsrcrecordid><sourcetype>Open Access Repository</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype></control><display><type>article</type><title>GC/MS를 이용한 혈액 중 유기인제류 농약의 동시 분석에 관한 방법의 유효화</title><source>EZB-FREE-00999 freely available EZB journals</source><creator>박미정 ; 양자열 ; 김기욱 ; 박유신 ; 정희선 ; 이상기 ; Park Mee Jung ; Yang Ja Youl ; Kim Ki Wook ; Park Yoo Shin ; Chung Hee Sun ; Lee Sang Ki</creator><creatorcontrib>박미정 ; 양자열 ; 김기욱 ; 박유신 ; 정희선 ; 이상기 ; Park Mee Jung ; Yang Ja Youl ; Kim Ki Wook ; Park Yoo Shin ; Chung Hee Sun ; Lee Sang Ki</creatorcontrib><description>The purpose of this study was to provide the standard method for the analysis of organophosphorous pesticides such as chlorpyrifos, diazinon, malathion and parathion in blood. We performed method validation for these pesticides in blood according to EURACHEM (A focus For Analytical Chemistry in Europe) guide. For the analysis of the pesticides, we used solid-phase extraction ,column (Waters Oasis $HLB^{(R)}$. After the extraction, the supernatants were evaporated to dryness under the nitrogen stream. They were analyzed by gas chromatography/mass spectrometry (GC/MS) after reconstituting with ethanol. Terbufos was used as an internal standard. To validate this method, we performed verification procedures with the following parameters: selectivity, linearity of calibration, accuracy, precision, limit of detection and quantification. Validation data according to Eurachem guide were adequate for our purpose for the analysis of chlorpyrifos, diazinon, malathion and parathion in blood.</description><identifier>ISSN: 1226-9158</identifier><language>kor</language><ispartof>환경독성학회지, 2005, Vol.20 (4), p.297-302</ispartof><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>230,314,780,784,885,4024</link.rule.ids></links><search><creatorcontrib>박미정</creatorcontrib><creatorcontrib>양자열</creatorcontrib><creatorcontrib>김기욱</creatorcontrib><creatorcontrib>박유신</creatorcontrib><creatorcontrib>정희선</creatorcontrib><creatorcontrib>이상기</creatorcontrib><creatorcontrib>Park Mee Jung</creatorcontrib><creatorcontrib>Yang Ja Youl</creatorcontrib><creatorcontrib>Kim Ki Wook</creatorcontrib><creatorcontrib>Park Yoo Shin</creatorcontrib><creatorcontrib>Chung Hee Sun</creatorcontrib><creatorcontrib>Lee Sang Ki</creatorcontrib><title>GC/MS를 이용한 혈액 중 유기인제류 농약의 동시 분석에 관한 방법의 유효화</title><title>환경독성학회지</title><addtitle>Journal of environmental toxicology</addtitle><description>The purpose of this study was to provide the standard method for the analysis of organophosphorous pesticides such as chlorpyrifos, diazinon, malathion and parathion in blood. We performed method validation for these pesticides in blood according to EURACHEM (A focus For Analytical Chemistry in Europe) guide. For the analysis of the pesticides, we used solid-phase extraction ,column (Waters Oasis $HLB^{(R)}$. After the extraction, the supernatants were evaporated to dryness under the nitrogen stream. They were analyzed by gas chromatography/mass spectrometry (GC/MS) after reconstituting with ethanol. Terbufos was used as an internal standard. To validate this method, we performed verification procedures with the following parameters: selectivity, linearity of calibration, accuracy, precision, limit of detection and quantification. Validation data according to Eurachem guide were adequate for our purpose for the analysis of chlorpyrifos, diazinon, malathion and parathion in blood.</description><issn>1226-9158</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2005</creationdate><recordtype>article</recordtype><sourceid>JDI</sourceid><recordid>eNpjYeA0NDIy07U0NLXgYOAtLs5MMjAwNDQwNza25GRIdnfW9w1-vXSPwpu5W97MWvl26hyFtzM63kxdqPBmyUSFN3MWvNqx4c3cHW8WzHm9dIbC67beN1P3vpkLZPXPfNM9R-H1tpY3LXPfTJ-g8GpLA0jz6w0rX2-aClIB1Pt21oq3M6fwMLCmJeYUp_JCaW4GVTfXEGcP3ezM4pLM-LyU4px4L0dvfyMDA1NDQ3MjI1NzAzNDC2Ni1QEALpVeSA</recordid><startdate>2005</startdate><enddate>2005</enddate><creator>박미정</creator><creator>양자열</creator><creator>김기욱</creator><creator>박유신</creator><creator>정희선</creator><creator>이상기</creator><creator>Park Mee Jung</creator><creator>Yang Ja Youl</creator><creator>Kim Ki Wook</creator><creator>Park Yoo Shin</creator><creator>Chung Hee Sun</creator><creator>Lee Sang Ki</creator><scope>JDI</scope></search><sort><creationdate>2005</creationdate><title>GC/MS를 이용한 혈액 중 유기인제류 농약의 동시 분석에 관한 방법의 유효화</title><author>박미정 ; 양자열 ; 김기욱 ; 박유신 ; 정희선 ; 이상기 ; Park Mee Jung ; Yang Ja Youl ; Kim Ki Wook ; Park Yoo Shin ; Chung Hee Sun ; Lee Sang Ki</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-kisti_ndsl_JAKO2005117225706183</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>kor</language><creationdate>2005</creationdate><toplevel>online_resources</toplevel><creatorcontrib>박미정</creatorcontrib><creatorcontrib>양자열</creatorcontrib><creatorcontrib>김기욱</creatorcontrib><creatorcontrib>박유신</creatorcontrib><creatorcontrib>정희선</creatorcontrib><creatorcontrib>이상기</creatorcontrib><creatorcontrib>Park Mee Jung</creatorcontrib><creatorcontrib>Yang Ja Youl</creatorcontrib><creatorcontrib>Kim Ki Wook</creatorcontrib><creatorcontrib>Park Yoo Shin</creatorcontrib><creatorcontrib>Chung Hee Sun</creatorcontrib><creatorcontrib>Lee Sang Ki</creatorcontrib><collection>KoreaScience</collection><jtitle>환경독성학회지</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>박미정</au><au>양자열</au><au>김기욱</au><au>박유신</au><au>정희선</au><au>이상기</au><au>Park Mee Jung</au><au>Yang Ja Youl</au><au>Kim Ki Wook</au><au>Park Yoo Shin</au><au>Chung Hee Sun</au><au>Lee Sang Ki</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>GC/MS를 이용한 혈액 중 유기인제류 농약의 동시 분석에 관한 방법의 유효화</atitle><jtitle>환경독성학회지</jtitle><addtitle>Journal of environmental toxicology</addtitle><date>2005</date><risdate>2005</risdate><volume>20</volume><issue>4</issue><spage>297</spage><epage>302</epage><pages>297-302</pages><issn>1226-9158</issn><abstract>The purpose of this study was to provide the standard method for the analysis of organophosphorous pesticides such as chlorpyrifos, diazinon, malathion and parathion in blood. We performed method validation for these pesticides in blood according to EURACHEM (A focus For Analytical Chemistry in Europe) guide. For the analysis of the pesticides, we used solid-phase extraction ,column (Waters Oasis $HLB^{(R)}$. After the extraction, the supernatants were evaporated to dryness under the nitrogen stream. They were analyzed by gas chromatography/mass spectrometry (GC/MS) after reconstituting with ethanol. Terbufos was used as an internal standard. To validate this method, we performed verification procedures with the following parameters: selectivity, linearity of calibration, accuracy, precision, limit of detection and quantification. Validation data according to Eurachem guide were adequate for our purpose for the analysis of chlorpyrifos, diazinon, malathion and parathion in blood.</abstract><oa>free_for_read</oa></addata></record>
fulltext fulltext
identifier ISSN: 1226-9158
ispartof 환경독성학회지, 2005, Vol.20 (4), p.297-302
issn 1226-9158
language kor
recordid cdi_kisti_ndsl_JAKO200511722570618
source EZB-FREE-00999 freely available EZB journals
title GC/MS를 이용한 혈액 중 유기인제류 농약의 동시 분석에 관한 방법의 유효화
url https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-07T00%3A29%3A23IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-kisti&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=GC/MS%EB%A5%BC%20%EC%9D%B4%EC%9A%A9%ED%95%9C%20%ED%98%88%EC%95%A1%20%EC%A4%91%20%EC%9C%A0%EA%B8%B0%EC%9D%B8%EC%A0%9C%EB%A5%98%20%EB%86%8D%EC%95%BD%EC%9D%98%20%EB%8F%99%EC%8B%9C%20%EB%B6%84%EC%84%9D%EC%97%90%20%EA%B4%80%ED%95%9C%20%EB%B0%A9%EB%B2%95%EC%9D%98%20%EC%9C%A0%ED%9A%A8%ED%99%94&rft.jtitle=%ED%99%98%EA%B2%BD%EB%8F%85%EC%84%B1%ED%95%99%ED%9A%8C%EC%A7%80&rft.au=%EB%B0%95%EB%AF%B8%EC%A0%95&rft.date=2005&rft.volume=20&rft.issue=4&rft.spage=297&rft.epage=302&rft.pages=297-302&rft.issn=1226-9158&rft_id=info:doi/&rft_dat=%3Ckisti%3EJAKO200511722570618%3C/kisti%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_id=info:pmid/&rfr_iscdi=true