[법과학] HPTLC 및 GC/MS를 이용한 유해화학물질의 스크리닝에 관한 연구
To perform an effective screening for toxic materials of forensic interest detected in high profile criminal case in biological and environmental samples, we tried to construct a searchable computerized database using HPTLC(High Performance Thin Layer Chromatography) and GC/MS. Retardation factor($R...
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| Veröffentlicht in: | Punsŏk kwahak 2000, Vol.13 (1), p.108-120 |
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| creator | 박성우(Sung-Woo Park) 장성길(Seong-Gil Jang) 박유신(You-Sin Park) 이진훈(Jin-Hoon Lee) 이상기(Sang-Ki Lee) 유재훈(Jae-Hoon You) 김동환(Dong-Hwan Kim) 진광호(Kwang-Ho Jin) 김기욱(Ki-Wook Kim) 김유나(Yu-Na Kim) 노동석(Dong-Seok Lho) |
| description | To perform an effective screening for toxic materials of forensic interest detected in high profile criminal case in biological and environmental samples, we tried to construct a searchable computerized database using HPTLC(High Performance Thin Layer Chromatography) and GC/MS. Retardation factor($R_f$) values and UV spectral data of HPTLC were investigated for 160 pesticides, 34 chemicals and 39 explosives of standard grade. The data were compiled in a library. We also analyzed 112 pesticides, 31 chemicals and 17 explosives and 57 volatile organic compounds(VOCs) by GC/MS. The data for RT and characteristic mass ions were also compiled in a library. 생체시료 및 환경시료에서 법과학분야에서 많이 다루어지는 유해화학물질의 효과적인 동시 스크리닝을 위해 HPTLC 및 GC/MS를 이용하여 분석한 후 데이터베이스를 구축하여 검색자료로 활용하고자 하였다. HPTLC 시스템을 이용하여 농약류 160종, 화공약품류 34종, 폭약류 39종 총 233종의 표준품에 대해 $R_f$치 및 UV 스펙트럼을 측정, database화 하였으며 또한 GC/MS를 이용하여 농약류 112종, 화공약품류 31종, 폭약류 17종, 휘발성 유기화합물류(VOCs) 57종 총 217종의 표준품에 대해 RT 및 특성질량이온들을 측정, dataobase화 하여 library를 구축하였다. |
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Retardation factor($R_f$) values and UV spectral data of HPTLC were investigated for 160 pesticides, 34 chemicals and 39 explosives of standard grade. The data were compiled in a library. We also analyzed 112 pesticides, 31 chemicals and 17 explosives and 57 volatile organic compounds(VOCs) by GC/MS. The data for RT and characteristic mass ions were also compiled in a library. 생체시료 및 환경시료에서 법과학분야에서 많이 다루어지는 유해화학물질의 효과적인 동시 스크리닝을 위해 HPTLC 및 GC/MS를 이용하여 분석한 후 데이터베이스를 구축하여 검색자료로 활용하고자 하였다. HPTLC 시스템을 이용하여 농약류 160종, 화공약품류 34종, 폭약류 39종 총 233종의 표준품에 대해 $R_f$치 및 UV 스펙트럼을 측정, database화 하였으며 또한 GC/MS를 이용하여 농약류 112종, 화공약품류 31종, 폭약류 17종, 휘발성 유기화합물류(VOCs) 57종 총 217종의 표준품에 대해 RT 및 특성질량이온들을 측정, dataobase화 하여 library를 구축하였다.</description><identifier>ISSN: 1225-0163</identifier><identifier>EISSN: 2288-8985</identifier><language>kor</language><publisher>한국분석과학회</publisher><ispartof>Punsŏk kwahak, 2000, Vol.13 (1), p.108-120</ispartof><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>230,314,776,780,881,4009</link.rule.ids></links><search><creatorcontrib>박성우(Sung-Woo Park)</creatorcontrib><creatorcontrib>장성길(Seong-Gil Jang)</creatorcontrib><creatorcontrib>박유신(You-Sin Park)</creatorcontrib><creatorcontrib>이진훈(Jin-Hoon Lee)</creatorcontrib><creatorcontrib>이상기(Sang-Ki Lee)</creatorcontrib><creatorcontrib>유재훈(Jae-Hoon You)</creatorcontrib><creatorcontrib>김동환(Dong-Hwan Kim)</creatorcontrib><creatorcontrib>진광호(Kwang-Ho Jin)</creatorcontrib><creatorcontrib>김기욱(Ki-Wook Kim)</creatorcontrib><creatorcontrib>김유나(Yu-Na Kim)</creatorcontrib><creatorcontrib>노동석(Dong-Seok Lho)</creatorcontrib><title>[법과학] HPTLC 및 GC/MS를 이용한 유해화학물질의 스크리닝에 관한 연구</title><title>Punsŏk kwahak</title><addtitle>Analytical science & technology</addtitle><description>To perform an effective screening for toxic materials of forensic interest detected in high profile criminal case in biological and environmental samples, we tried to construct a searchable computerized database using HPTLC(High Performance Thin Layer Chromatography) and GC/MS. Retardation factor($R_f$) values and UV spectral data of HPTLC were investigated for 160 pesticides, 34 chemicals and 39 explosives of standard grade. The data were compiled in a library. We also analyzed 112 pesticides, 31 chemicals and 17 explosives and 57 volatile organic compounds(VOCs) by GC/MS. The data for RT and characteristic mass ions were also compiled in a library. 생체시료 및 환경시료에서 법과학분야에서 많이 다루어지는 유해화학물질의 효과적인 동시 스크리닝을 위해 HPTLC 및 GC/MS를 이용하여 분석한 후 데이터베이스를 구축하여 검색자료로 활용하고자 하였다. HPTLC 시스템을 이용하여 농약류 160종, 화공약품류 34종, 폭약류 39종 총 233종의 표준품에 대해 $R_f$치 및 UV 스펙트럼을 측정, database화 하였으며 또한 GC/MS를 이용하여 농약류 112종, 화공약품류 31종, 폭약류 17종, 휘발성 유기화합물류(VOCs) 57종 총 217종의 표준품에 대해 RT 및 특성질량이온들을 측정, dataobase화 하여 library를 구축하였다.</description><issn>1225-0163</issn><issn>2288-8985</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2000</creationdate><recordtype>article</recordtype><sourceid>JDI</sourceid><recordid>eNpFjz9Lw0AAxQ9RsNR-h1scg3e5u-RuLLG2arWC3VRC0txBbC3S6OBmN9FBB0OttODgH4QMRevWT9RcvoNBBd_y3vDj8d4CKJgm5wYXnC2CAjZNZiBskWVQiqJjlItRmwirAA4P0o94_jnL4uERrO016w5MJ7ew6qzt7KcvM6jHU_34nsUjqEdPWTzNhvc5miYz_Xalxw9QXz9n_SR9TdKbsR7cwfn08gceTOZfyQpYUl4nkqU_L4LmRqXp1Ix6o7rplOtGm-fDmGoJQjjlkklFlOWbdgtRzw9s6dk-ZhQxC7eETyWVAVNeYDOkCKZKSkx9n5EiWP2tbYfRWeh2g6jjbpW3G2b-Ewtkcc6oQPSf6573whMZhJ57mgevd-HuNtYrCFmECczIN8Ficyg</recordid><startdate>2000</startdate><enddate>2000</enddate><creator>박성우(Sung-Woo Park)</creator><creator>장성길(Seong-Gil Jang)</creator><creator>박유신(You-Sin Park)</creator><creator>이진훈(Jin-Hoon Lee)</creator><creator>이상기(Sang-Ki Lee)</creator><creator>유재훈(Jae-Hoon You)</creator><creator>김동환(Dong-Hwan Kim)</creator><creator>진광호(Kwang-Ho Jin)</creator><creator>김기욱(Ki-Wook Kim)</creator><creator>김유나(Yu-Na Kim)</creator><creator>노동석(Dong-Seok Lho)</creator><general>한국분석과학회</general><scope>DBRKI</scope><scope>TDB</scope><scope>JDI</scope></search><sort><creationdate>2000</creationdate><title>[법과학] HPTLC 및 GC/MS를 이용한 유해화학물질의 스크리닝에 관한 연구</title><author>박성우(Sung-Woo Park) ; 장성길(Seong-Gil Jang) ; 박유신(You-Sin Park) ; 이진훈(Jin-Hoon Lee) ; 이상기(Sang-Ki Lee) ; 유재훈(Jae-Hoon You) ; 김동환(Dong-Hwan Kim) ; 진광호(Kwang-Ho Jin) ; 김기욱(Ki-Wook Kim) ; 김유나(Yu-Na Kim) ; 노동석(Dong-Seok Lho)</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-k825-5fc933848e5ef3f6b27c04abd7ea7b1540561c9b4e4ed5fad750f314fee14bb53</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>kor</language><creationdate>2000</creationdate><toplevel>online_resources</toplevel><creatorcontrib>박성우(Sung-Woo Park)</creatorcontrib><creatorcontrib>장성길(Seong-Gil Jang)</creatorcontrib><creatorcontrib>박유신(You-Sin Park)</creatorcontrib><creatorcontrib>이진훈(Jin-Hoon Lee)</creatorcontrib><creatorcontrib>이상기(Sang-Ki Lee)</creatorcontrib><creatorcontrib>유재훈(Jae-Hoon You)</creatorcontrib><creatorcontrib>김동환(Dong-Hwan Kim)</creatorcontrib><creatorcontrib>진광호(Kwang-Ho Jin)</creatorcontrib><creatorcontrib>김기욱(Ki-Wook Kim)</creatorcontrib><creatorcontrib>김유나(Yu-Na Kim)</creatorcontrib><creatorcontrib>노동석(Dong-Seok Lho)</creatorcontrib><collection>DBPIA - 디비피아</collection><collection>DBPIA</collection><collection>KoreaScience</collection><jtitle>Punsŏk kwahak</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>박성우(Sung-Woo Park)</au><au>장성길(Seong-Gil Jang)</au><au>박유신(You-Sin Park)</au><au>이진훈(Jin-Hoon Lee)</au><au>이상기(Sang-Ki Lee)</au><au>유재훈(Jae-Hoon You)</au><au>김동환(Dong-Hwan Kim)</au><au>진광호(Kwang-Ho Jin)</au><au>김기욱(Ki-Wook Kim)</au><au>김유나(Yu-Na Kim)</au><au>노동석(Dong-Seok Lho)</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>[법과학] HPTLC 및 GC/MS를 이용한 유해화학물질의 스크리닝에 관한 연구</atitle><jtitle>Punsŏk kwahak</jtitle><addtitle>Analytical science & technology</addtitle><date>2000</date><risdate>2000</risdate><volume>13</volume><issue>1</issue><spage>108</spage><epage>120</epage><pages>108-120</pages><issn>1225-0163</issn><eissn>2288-8985</eissn><abstract>To perform an effective screening for toxic materials of forensic interest detected in high profile criminal case in biological and environmental samples, we tried to construct a searchable computerized database using HPTLC(High Performance Thin Layer Chromatography) and GC/MS. Retardation factor($R_f$) values and UV spectral data of HPTLC were investigated for 160 pesticides, 34 chemicals and 39 explosives of standard grade. The data were compiled in a library. We also analyzed 112 pesticides, 31 chemicals and 17 explosives and 57 volatile organic compounds(VOCs) by GC/MS. The data for RT and characteristic mass ions were also compiled in a library. 생체시료 및 환경시료에서 법과학분야에서 많이 다루어지는 유해화학물질의 효과적인 동시 스크리닝을 위해 HPTLC 및 GC/MS를 이용하여 분석한 후 데이터베이스를 구축하여 검색자료로 활용하고자 하였다. HPTLC 시스템을 이용하여 농약류 160종, 화공약품류 34종, 폭약류 39종 총 233종의 표준품에 대해 $R_f$치 및 UV 스펙트럼을 측정, database화 하였으며 또한 GC/MS를 이용하여 농약류 112종, 화공약품류 31종, 폭약류 17종, 휘발성 유기화합물류(VOCs) 57종 총 217종의 표준품에 대해 RT 및 특성질량이온들을 측정, dataobase화 하여 library를 구축하였다.</abstract><pub>한국분석과학회</pub><tpages>13</tpages><oa>free_for_read</oa></addata></record> |
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| title | [법과학] HPTLC 및 GC/MS를 이용한 유해화학물질의 스크리닝에 관한 연구 |
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