Carbothermal Synthesis of Aluminum Nitride

A synthetic route is described for making carbothermally reduced powders from colloidal oxide precursors trapped in a polymer matrix. The entrapping resin, which is formed by polymerization of a monomer dissolved in the colloid, serves both to minimize particle agglomeration during reaction and as t...

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Veröffentlicht in:Advanced Ceramic Materials 1988-07, Vol.3 (4), p.418-419
1. Verfasser: SILVERMAN, LANCE D.
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description A synthetic route is described for making carbothermally reduced powders from colloidal oxide precursors trapped in a polymer matrix. The entrapping resin, which is formed by polymerization of a monomer dissolved in the colloid, serves both to minimize particle agglomeration during reaction and as the source of carbon for reduction. Following reduction, the remaining carbon matrix is removed by oxidation. This strategy was used to synthesize aluminum nitride powder via trapping of colloidal alumina in poly(furfuryl alcohol) resin.
doi_str_mv 10.1111/j.1551-2916.1988.tb00248.x
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identifier ISSN: 0883-5551
ispartof Advanced Ceramic Materials, 1988-07, Vol.3 (4), p.418-419
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1551-2916
language eng
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source Wiley Online Library All Journals
subjects 360201 - Ceramics, Cermets, & Refractories- Preparation & Fabrication
360202 - Ceramics, Cermets, & Refractories- Structure & Phase Studies
400101 - Activation, Nuclear Reaction, Radiometric & Radiochemical Procedures
ACTIVATION ANALYSIS
ALUMINIUM COMPOUNDS
ALUMINIUM NITRIDES
CHEMICAL ANALYSIS
COHERENT SCATTERING
DATA
DIFFRACTION
ELECTRON MICROSCOPY
EXPERIMENTAL DATA
INFORMATION
INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY
MATERIALS SCIENCE
MEASURING METHODS
MICROSCOPY
NEUTRON ACTIVATION ANALYSIS
NITRIDES
NITROGEN COMPOUNDS
NUMERICAL DATA
PNICTIDES
POWDERS
SCATTERING
SYNTHESIS
TRANSMISSION ELECTRON MICROSCOPY
X-RAY DIFFRACTION
title Carbothermal Synthesis of Aluminum Nitride
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