Solvothermal Synthesis and Structure of a New Selenium-Rich Selenophosphate K3PSe4·2Se6

The compound K3PSe4·2Se6 was synthesized at 110 °C via solventothermal techniques from binary starting materials and Se in acetonitrile. The compound crystallizes in the space group Fd3̄ of the cubic system with eight formula units in a cell with a dimension of a = 16.415(2) Å at T = 193 K. The stru...

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Veröffentlicht in:	Inorganic chemistry 2002-02, Vol.41 (4), p.640-642
Hauptverfasser:	Dickerson, Christine A, Fisher, Mary J, Sykora, Richard E, Albrecht-Schmitt, Thomas E, Cody, Jason A
Format:	Artikel
Sprache:	eng
Online-Zugang:	Volltext
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