A new purification method for 2-mercaptobenzothiazole and its application as vulcanization accelerator
In this work, a new purification method for 2-Mercaptobenzothiazole (MBT) and its application as a vulcanization accelerator was reported, and the properties of MBT samples were comprehensively investigated. According to the chemical equation of this purified reaction, the byproduct of the CO 2 meth...
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| Veröffentlicht in: | Materials research express 2023-04, Vol.10 (4), p.45101 |
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| creator | Shen, Yuhong Jing, Xianhong Mu, Xueliang Dou, Jinpeng Zhang, Qingwei Zhang, Yidong Liu, Yanjun Li, Zhenqiu |
| description | In this work, a new purification method for 2-Mercaptobenzothiazole (MBT) and its application as a vulcanization accelerator was reported, and the properties of MBT samples were comprehensively investigated. According to the chemical equation of this purified reaction, the byproduct of the CO
2
method was easy to treat. Results showed that the melting point and yield of experimental CAMBT samples were increased to 173.6 °C and 93.11%, respectively. The chemical structure and crystal absorption peak of all MBT samples were also measured by the FTIR and XRD analysis. Thermogravimetric analysis was used to study the residue of resin in MBT samples. Element content confirmed the existence of C, N, H, and S elements, and there were no other elements in the products. What is more important, the mechanical properties of experimental CDMBT@NR and SAMBT@NR samples were better than that of UMBT@NR. Thus, this paper offers a new purification method for MBT and investigates its application as a vulcanization accelerator. |
| doi_str_mv | 10.1088/2053-1591/acca6a |
| format | Article |
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2
method was easy to treat. Results showed that the melting point and yield of experimental CAMBT samples were increased to 173.6 °C and 93.11%, respectively. The chemical structure and crystal absorption peak of all MBT samples were also measured by the FTIR and XRD analysis. Thermogravimetric analysis was used to study the residue of resin in MBT samples. Element content confirmed the existence of C, N, H, and S elements, and there were no other elements in the products. What is more important, the mechanical properties of experimental CDMBT@NR and SAMBT@NR samples were better than that of UMBT@NR. Thus, this paper offers a new purification method for MBT and investigates its application as a vulcanization accelerator.</description><identifier>ISSN: 2053-1591</identifier><identifier>EISSN: 2053-1591</identifier><identifier>DOI: 10.1088/2053-1591/acca6a</identifier><language>eng</language><publisher>Bristol: IOP Publishing</publisher><subject>2-mercaptobenzothiazole ; carbon dioxide ; Mechanical properties ; Melting points ; Mercaptobenzothiazole ; Purification ; rubber accelerator ; Thermogravimetric analysis ; Vulcanization</subject><ispartof>Materials research express, 2023-04, Vol.10 (4), p.45101</ispartof><rights>2023 The Author(s). Published by IOP Publishing Ltd</rights><rights>2023 The Author(s). Published by IOP Publishing Ltd. This work is published under http://creativecommons.org/licenses/by/4.0/ (the “License”). Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License.</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c401t-8f82640607e999503b0141969dddf7eae348dbde2a41eb3a1cae1b4e4cdacc83</cites><orcidid>0000-0003-4070-8276</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://iopscience.iop.org/article/10.1088/2053-1591/acca6a/pdf$$EPDF$$P50$$Giop$$Hfree_for_read</linktopdf><link.rule.ids>314,780,784,864,2102,27924,27925,38868,38890,53840,53867</link.rule.ids></links><search><creatorcontrib>Shen, Yuhong</creatorcontrib><creatorcontrib>Jing, Xianhong</creatorcontrib><creatorcontrib>Mu, Xueliang</creatorcontrib><creatorcontrib>Dou, Jinpeng</creatorcontrib><creatorcontrib>Zhang, Qingwei</creatorcontrib><creatorcontrib>Zhang, Yidong</creatorcontrib><creatorcontrib>Liu, Yanjun</creatorcontrib><creatorcontrib>Li, Zhenqiu</creatorcontrib><title>A new purification method for 2-mercaptobenzothiazole and its application as vulcanization accelerator</title><title>Materials research express</title><addtitle>MRX</addtitle><addtitle>Mater. Res. Express</addtitle><description>In this work, a new purification method for 2-Mercaptobenzothiazole (MBT) and its application as a vulcanization accelerator was reported, and the properties of MBT samples were comprehensively investigated. According to the chemical equation of this purified reaction, the byproduct of the CO
2
method was easy to treat. Results showed that the melting point and yield of experimental CAMBT samples were increased to 173.6 °C and 93.11%, respectively. The chemical structure and crystal absorption peak of all MBT samples were also measured by the FTIR and XRD analysis. Thermogravimetric analysis was used to study the residue of resin in MBT samples. Element content confirmed the existence of C, N, H, and S elements, and there were no other elements in the products. What is more important, the mechanical properties of experimental CDMBT@NR and SAMBT@NR samples were better than that of UMBT@NR. Thus, this paper offers a new purification method for MBT and investigates its application as a vulcanization accelerator.</description><subject>2-mercaptobenzothiazole</subject><subject>carbon dioxide</subject><subject>Mechanical properties</subject><subject>Melting points</subject><subject>Mercaptobenzothiazole</subject><subject>Purification</subject><subject>rubber accelerator</subject><subject>Thermogravimetric analysis</subject><subject>Vulcanization</subject><issn>2053-1591</issn><issn>2053-1591</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><sourceid>O3W</sourceid><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><sourceid>DOA</sourceid><recordid>eNp9UU1P3TAQjKpWKgLuHC31wKWBteMk9hGhtiAhceFubex18VNeHBy_0r5f34Tw0QPqaVejmdnVTFGccDjjoNS5gLoqea35OVqLDX4oDl6hj__sn4vjadoAgGh1VYvmoPAXbKBHNu5S8MFiDnFgW8r30TEfExPllpLFMceOhn3M9wH3sSeGg2MhTwzHsX-R4cR-7XqLQ9g_A9ZSTwlzTEfFJ4_9RMfP87C4-_7t7vKqvLn9cX15cVNaCTyXyivRSGigJa11DVUHXHLdaOecbwmpksp1jgRKTl2F3CLxTpK0bj6mqsPierV1ETdmTGGL6Y-JGMwTENNPgykH25NBj7z2BIDQSN-2upVzKl4I8gq7evH6snqNKT7saMpmE3dpmL83QgEXmistZhasLJviNCXyr1c5mKUbs4RvlvDN2s0s-bpKQhzfPP9DP32Hvk2_F4k0IGsO3IzOV38B8cifdQ</recordid><startdate>20230401</startdate><enddate>20230401</enddate><creator>Shen, Yuhong</creator><creator>Jing, Xianhong</creator><creator>Mu, Xueliang</creator><creator>Dou, Jinpeng</creator><creator>Zhang, Qingwei</creator><creator>Zhang, Yidong</creator><creator>Liu, Yanjun</creator><creator>Li, Zhenqiu</creator><general>IOP Publishing</general><scope>O3W</scope><scope>TSCCA</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>KB.</scope><scope>PDBOC</scope><scope>PIMPY</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>DOA</scope><orcidid>https://orcid.org/0000-0003-4070-8276</orcidid></search><sort><creationdate>20230401</creationdate><title>A new purification method for 2-mercaptobenzothiazole and its application as vulcanization accelerator</title><author>Shen, Yuhong ; Jing, Xianhong ; Mu, Xueliang ; Dou, Jinpeng ; Zhang, Qingwei ; Zhang, Yidong ; Liu, Yanjun ; Li, Zhenqiu</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c401t-8f82640607e999503b0141969dddf7eae348dbde2a41eb3a1cae1b4e4cdacc83</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2023</creationdate><topic>2-mercaptobenzothiazole</topic><topic>carbon dioxide</topic><topic>Mechanical properties</topic><topic>Melting points</topic><topic>Mercaptobenzothiazole</topic><topic>Purification</topic><topic>rubber accelerator</topic><topic>Thermogravimetric analysis</topic><topic>Vulcanization</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Shen, Yuhong</creatorcontrib><creatorcontrib>Jing, Xianhong</creatorcontrib><creatorcontrib>Mu, Xueliang</creatorcontrib><creatorcontrib>Dou, Jinpeng</creatorcontrib><creatorcontrib>Zhang, Qingwei</creatorcontrib><creatorcontrib>Zhang, Yidong</creatorcontrib><creatorcontrib>Liu, Yanjun</creatorcontrib><creatorcontrib>Li, Zhenqiu</creatorcontrib><collection>Institute of Physics Open Access Journal Titles</collection><collection>IOPscience (Open Access)</collection><collection>CrossRef</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central Essentials</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>Materials Science Database</collection><collection>Materials Science Collection</collection><collection>Access via ProQuest (Open Access)</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>DOAJ Directory of Open Access Journals</collection><jtitle>Materials research express</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Shen, Yuhong</au><au>Jing, Xianhong</au><au>Mu, Xueliang</au><au>Dou, Jinpeng</au><au>Zhang, Qingwei</au><au>Zhang, Yidong</au><au>Liu, Yanjun</au><au>Li, Zhenqiu</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>A new purification method for 2-mercaptobenzothiazole and its application as vulcanization accelerator</atitle><jtitle>Materials research express</jtitle><stitle>MRX</stitle><addtitle>Mater. Res. Express</addtitle><date>2023-04-01</date><risdate>2023</risdate><volume>10</volume><issue>4</issue><spage>45101</spage><pages>45101-</pages><issn>2053-1591</issn><eissn>2053-1591</eissn><abstract>In this work, a new purification method for 2-Mercaptobenzothiazole (MBT) and its application as a vulcanization accelerator was reported, and the properties of MBT samples were comprehensively investigated. According to the chemical equation of this purified reaction, the byproduct of the CO
2
method was easy to treat. Results showed that the melting point and yield of experimental CAMBT samples were increased to 173.6 °C and 93.11%, respectively. The chemical structure and crystal absorption peak of all MBT samples were also measured by the FTIR and XRD analysis. Thermogravimetric analysis was used to study the residue of resin in MBT samples. Element content confirmed the existence of C, N, H, and S elements, and there were no other elements in the products. What is more important, the mechanical properties of experimental CDMBT@NR and SAMBT@NR samples were better than that of UMBT@NR. Thus, this paper offers a new purification method for MBT and investigates its application as a vulcanization accelerator.</abstract><cop>Bristol</cop><pub>IOP Publishing</pub><doi>10.1088/2053-1591/acca6a</doi><tpages>8</tpages><orcidid>https://orcid.org/0000-0003-4070-8276</orcidid><oa>free_for_read</oa></addata></record> |
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| subjects | 2-mercaptobenzothiazole carbon dioxide Mechanical properties Melting points Mercaptobenzothiazole Purification rubber accelerator Thermogravimetric analysis Vulcanization |
| title | A new purification method for 2-mercaptobenzothiazole and its application as vulcanization accelerator |
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