Synthesis of 6-Hydroxy-2-methyl-3-thioxo-2H-1,2,4-triazin-5-one

Synthesis of 6-Hydroxy-2-methyl-3-thioxo-2H-1,2,4-triazin-5-one

The title compound has been prepared in three steps from 2-methylthiosemicarbazide following acylation, cyclisation and cation exchange chromatography. It was fully characterised by the usual spectroscopic means as well as by 15 N nmr spectroscopy and X-ray crystallographic analysis.

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Veröffentlicht in:Synthetic communications 1996-01, Vol.26 (11), p.2075-2084
Hauptverfasser: Branch, Clive L., Eggleston, Drake S., Haltiwanger, R. Curtis, Kaura, Arun C., Tyler, John W.
Format: Artikel
Sprache:eng
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Zusammenfassung:The title compound has been prepared in three steps from 2-methylthiosemicarbazide following acylation, cyclisation and cation exchange chromatography. It was fully characterised by the usual spectroscopic means as well as by 15 N nmr spectroscopy and X-ray crystallographic analysis.
ISSN:0039-7911
1532-2432
DOI:10.1080/00397919608003566