Using PDMS Plasma Cavity SERS Substrate for the Detection of Aspartame

Surface-enhanced Raman spectroscopy (SERS) was used to simply and sensitively detect the artificial sweetener aspartame added to purified water. In this paper, a cavity formed spontaneously by silver ion droplets, and liquid polydimethylsiloxane (PDMS) is used as an SERS substrate to integrate plasm...

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Veröffentlicht in:Journal of Spectroscopy 2020-01, Vol.2020 (2020), p.1-7
Hauptverfasser: Xu, Jianwen, Chen, Guoqing, Wang, Tingyu, Zhu, Zhuowei, Gao, Hui, Gu, Jiao, Zhu, Chun, Li, Lei, Ma, Chaoqun, Chen, Lvming, Du, Chenxu
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container_end_page 7
container_issue 2020
container_start_page 1
container_title Journal of Spectroscopy
container_volume 2020
creator Xu, Jianwen
Chen, Guoqing
Wang, Tingyu
Zhu, Zhuowei
Gao, Hui
Gu, Jiao
Zhu, Chun
Li, Lei
Ma, Chaoqun
Chen, Lvming
Du, Chenxu
description Surface-enhanced Raman spectroscopy (SERS) was used to simply and sensitively detect the artificial sweetener aspartame added to purified water. In this paper, a cavity formed spontaneously by silver ion droplets, and liquid polydimethylsiloxane (PDMS) is used as an SERS substrate to integrate plasma nanoparticles into optical devices. Firstly, Raman spectral characteristics of aspartame powder and aspartame aqueous solution were analyzed. Secondly, the effect of aspartame content in purified water on SERS intensity was investigated by using the prepared PDMS plasma cavity to test the samples. Thirdly, the SERS calibration curve was established by using the characteristic peak intensity of aspartame, and a good linearity relationship between the concentration of aspartame added in purified water and the characteristic peak intensity of 1588(±5) cm-1 was obtained. The linear regression equation and correlation coefficient (r) were y = 11412.73874 x + 107.36722 and 0.99593, respectively. The average recovery of aspartame in purified water was 101–106%, and the relative standard deviation (RSD) was 0.121–0.496%. The experimental results show that using this method can detect aspartame in purified water correctly, which is expected to be used in the identification and detection of sweeteners in purified water.
doi_str_mv 10.1155/2020/4212787
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In this paper, a cavity formed spontaneously by silver ion droplets, and liquid polydimethylsiloxane (PDMS) is used as an SERS substrate to integrate plasma nanoparticles into optical devices. Firstly, Raman spectral characteristics of aspartame powder and aspartame aqueous solution were analyzed. Secondly, the effect of aspartame content in purified water on SERS intensity was investigated by using the prepared PDMS plasma cavity to test the samples. Thirdly, the SERS calibration curve was established by using the characteristic peak intensity of aspartame, and a good linearity relationship between the concentration of aspartame added in purified water and the characteristic peak intensity of 1588(±5) cm-1 was obtained. The linear regression equation and correlation coefficient (r) were y = 11412.73874 x + 107.36722 and 0.99593, respectively. The average recovery of aspartame in purified water was 101–106%, and the relative standard deviation (RSD) was 0.121–0.496%. 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subjects Adsorption
Aqueous solutions
Aspartame
Correlation coefficients
Curing
Dimethylpolysiloxane
Flexibility
Linearity
Methods
Nanoparticles
Plasma
Polydimethylsiloxane
Purification
Raman spectroscopy
Regression analysis
Silicone resins
Soft drinks
Spectrum analysis
Substrates
Sweeteners
Water
Water purification
title Using PDMS Plasma Cavity SERS Substrate for the Detection of Aspartame
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