Design of organically modified sepiolite and its use as adsorbent for hazardous Malachite Green dye removal from water
A novel adsorbent design method, based on organic surface modification and carbonization at 350–500 °C, of sepiolite, was used to prepare carbon@sepiolite composites which were used for hazardous malachite green dye removal from water. Prior to their use as adsorbent, the structure and the morpholog...
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| Veröffentlicht in: | Water, air, and soil pollution air, and soil pollution, 2023-03, Vol.234 (3), p.183, Article 183 |
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| creator | Largo, Fadwa Haounati, Redouane Ouachtak, Hassan Hafid, Naima Jada, Amane Addi, Abdelaziz Ait |
| description | A novel adsorbent design method, based on organic surface modification and carbonization at 350–500 °C, of sepiolite, was used to prepare carbon@sepiolite composites which were used for hazardous malachite green dye removal from water. Prior to their use as adsorbent, the structure and the morphology of the carbon@sepiolite composites were assessed by various methods, such as Fourier transform infrared (FTIR) spectroscopy, scanning (SEM) and transmission (TEM) electron microscopy, energy-dispersive analysis of X-rays (EDAX), and N
2
adsorption/desorption isotherms (BET method). The designed adsorbents showed good adsorption properties for MG molecules, reaching a maximum dye adsorbed amount of 1198.67 mg/g at 25 °C for the carbon@sepiolite composites calcinated at 500 °C. Further, the kinetics and the equilibrium adsorption isotherms of the MG molecules from water onto the sepiolite-based composites were well fitted by, respectively, the pseudo-second-order model (
R
2
= 0.98) and the Langmuir isotherm (
R
2
= 0.94) models, indicating that the MG molecules were homogenously adsorbed and formed a monolayer on the organically modified sepiolite surface. Moreover, the values of the thermodynamic parameters, such as ∆
G
, ∆
H
, and ∆
S
related to the adsorption process, indicated that the adsorption reaction was spontaneous, feasible, and endothermic. In the overall, the present work offers facile ways for the design of organically modified sepiolite which can be used at large scale as adsorbents for waste recycling. |
| doi_str_mv | 10.1007/s11270-023-06185-z |
| format | Article |
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2
adsorption/desorption isotherms (BET method). The designed adsorbents showed good adsorption properties for MG molecules, reaching a maximum dye adsorbed amount of 1198.67 mg/g at 25 °C for the carbon@sepiolite composites calcinated at 500 °C. Further, the kinetics and the equilibrium adsorption isotherms of the MG molecules from water onto the sepiolite-based composites were well fitted by, respectively, the pseudo-second-order model (
R
2
= 0.98) and the Langmuir isotherm (
R
2
= 0.94) models, indicating that the MG molecules were homogenously adsorbed and formed a monolayer on the organically modified sepiolite surface. Moreover, the values of the thermodynamic parameters, such as ∆
G
, ∆
H
, and ∆
S
related to the adsorption process, indicated that the adsorption reaction was spontaneous, feasible, and endothermic. In the overall, the present work offers facile ways for the design of organically modified sepiolite which can be used at large scale as adsorbents for waste recycling.</description><identifier>ISSN: 0049-6979</identifier><identifier>EISSN: 1573-2932</identifier><identifier>DOI: 10.1007/s11270-023-06185-z</identifier><language>eng</language><publisher>Cham: Springer International Publishing</publisher><subject>Adsorbents ; Adsorption ; Analysis ; Analytical methods ; Atmospheric Protection/Air Quality Control/Air Pollution ; Carbon ; Chemical Sciences ; Climate Change/Climate Change Impacts ; Color removal ; Composite materials ; Design ; Dyes ; Earth and Environmental Science ; Electron microscopy ; Endothermic reactions ; Environment ; Environmental monitoring ; Fourier transforms ; Hydrogeology ; Infrared analysis ; Isotherms ; Kinetics ; Malachite green ; Parameter modification ; Recycling (Waste, etc.) ; Removal ; Sepiolite ; Soil Science & Conservation ; Surface chemistry ; Waste recycling ; Water ; Water Quality/Water Pollution</subject><ispartof>Water, air, and soil pollution, 2023-03, Vol.234 (3), p.183, Article 183</ispartof><rights>The Author(s), under exclusive licence to Springer Nature Switzerland AG 2023. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.</rights><rights>COPYRIGHT 2023 Springer</rights><rights>Distributed under a Creative Commons Attribution 4.0 International License</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c392t-932eaaceb55a82b14cd7aa72674fc1dfe898d2dff4e50400c0cd10ff256914d73</citedby><cites>FETCH-LOGICAL-c392t-932eaaceb55a82b14cd7aa72674fc1dfe898d2dff4e50400c0cd10ff256914d73</cites><orcidid>0000-0003-4740-9025</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s11270-023-06185-z$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s11270-023-06185-z$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>230,315,781,785,886,27929,27930,41493,42562,51324</link.rule.ids><backlink>$$Uhttps://hal.science/hal-04298025$$DView record in HAL$$Hfree_for_read</backlink></links><search><creatorcontrib>Largo, Fadwa</creatorcontrib><creatorcontrib>Haounati, Redouane</creatorcontrib><creatorcontrib>Ouachtak, Hassan</creatorcontrib><creatorcontrib>Hafid, Naima</creatorcontrib><creatorcontrib>Jada, Amane</creatorcontrib><creatorcontrib>Addi, Abdelaziz Ait</creatorcontrib><title>Design of organically modified sepiolite and its use as adsorbent for hazardous Malachite Green dye removal from water</title><title>Water, air, and soil pollution</title><addtitle>Water Air Soil Pollut</addtitle><description>A novel adsorbent design method, based on organic surface modification and carbonization at 350–500 °C, of sepiolite, was used to prepare carbon@sepiolite composites which were used for hazardous malachite green dye removal from water. Prior to their use as adsorbent, the structure and the morphology of the carbon@sepiolite composites were assessed by various methods, such as Fourier transform infrared (FTIR) spectroscopy, scanning (SEM) and transmission (TEM) electron microscopy, energy-dispersive analysis of X-rays (EDAX), and N
2
adsorption/desorption isotherms (BET method). The designed adsorbents showed good adsorption properties for MG molecules, reaching a maximum dye adsorbed amount of 1198.67 mg/g at 25 °C for the carbon@sepiolite composites calcinated at 500 °C. Further, the kinetics and the equilibrium adsorption isotherms of the MG molecules from water onto the sepiolite-based composites were well fitted by, respectively, the pseudo-second-order model (
R
2
= 0.98) and the Langmuir isotherm (
R
2
= 0.94) models, indicating that the MG molecules were homogenously adsorbed and formed a monolayer on the organically modified sepiolite surface. Moreover, the values of the thermodynamic parameters, such as ∆
G
, ∆
H
, and ∆
S
related to the adsorption process, indicated that the adsorption reaction was spontaneous, feasible, and endothermic. In the overall, the present work offers facile ways for the design of organically modified sepiolite which can be used at large scale as adsorbents for waste recycling.</description><subject>Adsorbents</subject><subject>Adsorption</subject><subject>Analysis</subject><subject>Analytical methods</subject><subject>Atmospheric Protection/Air Quality Control/Air Pollution</subject><subject>Carbon</subject><subject>Chemical Sciences</subject><subject>Climate Change/Climate Change Impacts</subject><subject>Color removal</subject><subject>Composite materials</subject><subject>Design</subject><subject>Dyes</subject><subject>Earth and Environmental Science</subject><subject>Electron microscopy</subject><subject>Endothermic reactions</subject><subject>Environment</subject><subject>Environmental monitoring</subject><subject>Fourier transforms</subject><subject>Hydrogeology</subject><subject>Infrared analysis</subject><subject>Isotherms</subject><subject>Kinetics</subject><subject>Malachite green</subject><subject>Parameter modification</subject><subject>Recycling (Waste, etc.)</subject><subject>Removal</subject><subject>Sepiolite</subject><subject>Soil Science & Conservation</subject><subject>Surface chemistry</subject><subject>Waste recycling</subject><subject>Water</subject><subject>Water Quality/Water 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Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Largo, Fadwa</au><au>Haounati, Redouane</au><au>Ouachtak, Hassan</au><au>Hafid, Naima</au><au>Jada, Amane</au><au>Addi, Abdelaziz Ait</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Design of organically modified sepiolite and its use as adsorbent for hazardous Malachite Green dye removal from water</atitle><jtitle>Water, air, and soil pollution</jtitle><stitle>Water Air Soil Pollut</stitle><date>2023-03-01</date><risdate>2023</risdate><volume>234</volume><issue>3</issue><spage>183</spage><pages>183-</pages><artnum>183</artnum><issn>0049-6979</issn><eissn>1573-2932</eissn><abstract>A novel adsorbent design method, based on organic surface modification and carbonization at 350–500 °C, of sepiolite, was used to prepare carbon@sepiolite composites which were used for hazardous malachite green dye removal from water. Prior to their use as adsorbent, the structure and the morphology of the carbon@sepiolite composites were assessed by various methods, such as Fourier transform infrared (FTIR) spectroscopy, scanning (SEM) and transmission (TEM) electron microscopy, energy-dispersive analysis of X-rays (EDAX), and N
2
adsorption/desorption isotherms (BET method). The designed adsorbents showed good adsorption properties for MG molecules, reaching a maximum dye adsorbed amount of 1198.67 mg/g at 25 °C for the carbon@sepiolite composites calcinated at 500 °C. Further, the kinetics and the equilibrium adsorption isotherms of the MG molecules from water onto the sepiolite-based composites were well fitted by, respectively, the pseudo-second-order model (
R
2
= 0.98) and the Langmuir isotherm (
R
2
= 0.94) models, indicating that the MG molecules were homogenously adsorbed and formed a monolayer on the organically modified sepiolite surface. Moreover, the values of the thermodynamic parameters, such as ∆
G
, ∆
H
, and ∆
S
related to the adsorption process, indicated that the adsorption reaction was spontaneous, feasible, and endothermic. In the overall, the present work offers facile ways for the design of organically modified sepiolite which can be used at large scale as adsorbents for waste recycling.</abstract><cop>Cham</cop><pub>Springer International Publishing</pub><doi>10.1007/s11270-023-06185-z</doi><orcidid>https://orcid.org/0000-0003-4740-9025</orcidid><oa>free_for_read</oa></addata></record> |
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| identifier | ISSN: 0049-6979 |
| ispartof | Water, air, and soil pollution, 2023-03, Vol.234 (3), p.183, Article 183 |
| issn | 0049-6979 1573-2932 |
| language | eng |
| recordid | cdi_hal_primary_oai_HAL_hal_04298025v1 |
| source | SpringerLink Journals - AutoHoldings |
| subjects | Adsorbents Adsorption Analysis Analytical methods Atmospheric Protection/Air Quality Control/Air Pollution Carbon Chemical Sciences Climate Change/Climate Change Impacts Color removal Composite materials Design Dyes Earth and Environmental Science Electron microscopy Endothermic reactions Environment Environmental monitoring Fourier transforms Hydrogeology Infrared analysis Isotherms Kinetics Malachite green Parameter modification Recycling (Waste, etc.) Removal Sepiolite Soil Science & Conservation Surface chemistry Waste recycling Water Water Quality/Water Pollution |
| title | Design of organically modified sepiolite and its use as adsorbent for hazardous Malachite Green dye removal from water |
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