Synthesis of high-purity polycrystalline MAX phases in Ti–Al–C system through Mechanically Activated Self-propagating High-temperature Synthesis
Ternary MAX phase compounds were synthesized using an alternative route called MASHS (Mechanically Activated Self-propagating High-temperature Synthesis). This original process combines a short duration ball milling (MA) of reactants (Ti, Al, C) with a self-sustaining combustion (SHS). The particle...
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| Veröffentlicht in: | Journal of the European Ceramic Society 2010-03, Vol.30 (4), p.1049-1057 |
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| container_issue | 4 |
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| container_title | Journal of the European Ceramic Society |
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| creator | Hendaoui, A. Vrel, D. Amara, A. Langlois, P. Andasmas, M. Guerioune, M. |
| description | Ternary MAX phase compounds were synthesized using an alternative route called MASHS (Mechanically Activated Self-propagating High-temperature Synthesis). This original process combines a short duration ball milling (MA) of reactants (Ti, Al, C) with a self-sustaining combustion (SHS). The particle size evolution of the powder mixture during Mechanical Activation was monitored using XRD profile analysis. The effect of Al-excess was also discussed. XRD and SEM analyses have proved that the activation of the reaction kinetics must be accompanied by a decrease in the overall exothermicity in order to synthesize pure Ti–Al–C MAX phases by MASHS. |
| doi_str_mv | 10.1016/j.jeurceramsoc.2009.10.001 |
| format | Article |
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This original process combines a short duration ball milling (MA) of reactants (Ti, Al, C) with a self-sustaining combustion (SHS). The particle size evolution of the powder mixture during Mechanical Activation was monitored using XRD profile analysis. The effect of Al-excess was also discussed. 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| issn | 0955-2219 1873-619X |
| language | eng |
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| source | Elsevier ScienceDirect Journals |
| subjects | Carbides Electron microscopy Engineering Sciences Materials Microstructure-final Powders-solid state reaction X-ray methods |
| title | Synthesis of high-purity polycrystalline MAX phases in Ti–Al–C system through Mechanically Activated Self-propagating High-temperature Synthesis |
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