Combined angular and energy dispersive diffraction: optimized data acquisition, normalization and reduction
Combined angular and energy dispersive diffraction is particularly well suited to experiments at high pressures in large‐volume presses, and to the study of liquid or amorphous systems. This work describes the data acquisition, correction and reduction approach developed at the PSICHE beamline of th...
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| Veröffentlicht in: | Journal of applied crystallography 2022-04, Vol.55 (2), p.218-227 |
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| container_title | Journal of applied crystallography |
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| creator | King, A. Guignot, N. Henry, L. Morard, G. Clark, A. Le Godec, Y. Itié, J.-P. |
| description | Combined angular and energy dispersive diffraction is particularly well suited to experiments at high pressures in large‐volume presses, and to the study of liquid or amorphous systems. This work describes the data acquisition, correction and reduction approach developed at the PSICHE beamline of the SOLEIL synchrotron. The measured data were normalized for both the scattering volume and the effective incident energy spectrum. By optimizing the acquisition strategy, the measurement time and radiation dose are greatly reduced. The correction and reduction protocol outputs normalized scattering profiles that are suitable for pair distribution function or liquid structure analysis. These processes are demostrated with examples from a number of real experimental data sets.
An optimized methodology for collecting and analysing combined angular dispersive diffraction data is presented. This is particularly suitable for studying liquids or amorphous materials at high pressures. |
| doi_str_mv | 10.1107/S1600576722000322 |
| format | Article |
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An optimized methodology for collecting and analysing combined angular dispersive diffraction data is presented. This is particularly suitable for studying liquids or amorphous materials at high pressures.</description><identifier>ISSN: 1600-5767</identifier><identifier>ISSN: 0021-8898</identifier><identifier>EISSN: 1600-5767</identifier><identifier>DOI: 10.1107/S1600576722000322</identifier><language>eng</language><publisher>5 Abbey Square, Chester, Cheshire CH1 2HU, England: International Union of Crystallography</publisher><subject>amorphous structures ; Data acquisition ; Diffraction ; Dispersion ; Distribution functions ; Earth Sciences ; Energy ; Energy spectra ; Geophysics ; liquid structures ; Radiation ; Radiation dosage ; Radiation measurement ; Reduction ; Scattering ; Sciences of the Universe ; Structural analysis ; Structure-function relationships ; synchrotron ; Synchrotrons ; X‐ray diffraction</subject><ispartof>Journal of applied crystallography, 2022-04, Vol.55 (2), p.218-227</ispartof><rights>2022 A. King et al. published by IUCr Journals.</rights><rights>Copyright Blackwell Publishing Ltd. Apr 2022</rights><rights>Distributed under a Creative Commons Attribution 4.0 International License</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c4006-b37ea81d565257d8e8fa31be207651e520d61cb762744e212ac42ecf1a9f0f373</citedby><cites>FETCH-LOGICAL-c4006-b37ea81d565257d8e8fa31be207651e520d61cb762744e212ac42ecf1a9f0f373</cites><orcidid>0000-0001-6805-1283 ; 0000-0001-8542-1354 ; 0000-0002-4225-0767 ; 0000-0001-9006-5745</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1107%2FS1600576722000322$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1107%2FS1600576722000322$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>230,314,780,784,885,1417,27924,27925,45574,45575</link.rule.ids><backlink>$$Uhttps://hal.science/hal-03853157$$DView record in HAL$$Hfree_for_read</backlink></links><search><creatorcontrib>King, A.</creatorcontrib><creatorcontrib>Guignot, N.</creatorcontrib><creatorcontrib>Henry, L.</creatorcontrib><creatorcontrib>Morard, G.</creatorcontrib><creatorcontrib>Clark, A.</creatorcontrib><creatorcontrib>Le Godec, Y.</creatorcontrib><creatorcontrib>Itié, J.-P.</creatorcontrib><title>Combined angular and energy dispersive diffraction: optimized data acquisition, normalization and reduction</title><title>Journal of applied crystallography</title><description>Combined angular and energy dispersive diffraction is particularly well suited to experiments at high pressures in large‐volume presses, and to the study of liquid or amorphous systems. This work describes the data acquisition, correction and reduction approach developed at the PSICHE beamline of the SOLEIL synchrotron. The measured data were normalized for both the scattering volume and the effective incident energy spectrum. By optimizing the acquisition strategy, the measurement time and radiation dose are greatly reduced. The correction and reduction protocol outputs normalized scattering profiles that are suitable for pair distribution function or liquid structure analysis. These processes are demostrated with examples from a number of real experimental data sets.
An optimized methodology for collecting and analysing combined angular dispersive diffraction data is presented. This is particularly suitable for studying liquids or amorphous materials at high pressures.</description><subject>amorphous structures</subject><subject>Data acquisition</subject><subject>Diffraction</subject><subject>Dispersion</subject><subject>Distribution functions</subject><subject>Earth Sciences</subject><subject>Energy</subject><subject>Energy spectra</subject><subject>Geophysics</subject><subject>liquid structures</subject><subject>Radiation</subject><subject>Radiation dosage</subject><subject>Radiation measurement</subject><subject>Reduction</subject><subject>Scattering</subject><subject>Sciences of the Universe</subject><subject>Structural analysis</subject><subject>Structure-function relationships</subject><subject>synchrotron</subject><subject>Synchrotrons</subject><subject>X‐ray diffraction</subject><issn>1600-5767</issn><issn>0021-8898</issn><issn>1600-5767</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2022</creationdate><recordtype>article</recordtype><recordid>eNqFkE1LxDAQhoMouK7-AG8FT4LVJG2Srre1qKssCn6cQ9pO1qz9MmlXdn-97VZE8OBpZt55n5dhEDom-JwQLC6eCceYCS4oxRgHlO6gUS_5vbb7q99HB84tMSa9dYTe46pITAmZp8pFmyvb1cyDEuxi7WXG1WCdWUHXam1V2piqvPSqujGF2XRQphrlqfSjNc70uzOvrGyhcrNR_bgNs5C1W_AQ7WmVOzj6rmP0enP9Es_8-ePtXTyd-2mIMfeTQICKSMY4o0xkEURaBSQBigVnBBjFGSdpIjgVYQiUUJWGFFJN1ERjHYhgjE6H3DeVy9qaQtm1rJSRs-lc9hoOIhYQJlak854M3tpWHy24Ri6r1pbdeZLyUBDO2YR3LjK4Uls5Z0H_xBIs-__LP__vmMnAfJoc1v8D8j5-og9X3WE8-AI6ZohH</recordid><startdate>202204</startdate><enddate>202204</enddate><creator>King, A.</creator><creator>Guignot, N.</creator><creator>Henry, L.</creator><creator>Morard, G.</creator><creator>Clark, A.</creator><creator>Le Godec, Y.</creator><creator>Itié, J.-P.</creator><general>International Union of Crystallography</general><general>Blackwell Publishing Ltd</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope><scope>1XC</scope><scope>VOOES</scope><orcidid>https://orcid.org/0000-0001-6805-1283</orcidid><orcidid>https://orcid.org/0000-0001-8542-1354</orcidid><orcidid>https://orcid.org/0000-0002-4225-0767</orcidid><orcidid>https://orcid.org/0000-0001-9006-5745</orcidid></search><sort><creationdate>202204</creationdate><title>Combined angular and energy dispersive diffraction: optimized data acquisition, normalization and reduction</title><author>King, A. ; Guignot, N. ; Henry, L. ; Morard, G. ; Clark, A. ; Le Godec, Y. ; Itié, J.-P.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c4006-b37ea81d565257d8e8fa31be207651e520d61cb762744e212ac42ecf1a9f0f373</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2022</creationdate><topic>amorphous structures</topic><topic>Data acquisition</topic><topic>Diffraction</topic><topic>Dispersion</topic><topic>Distribution functions</topic><topic>Earth Sciences</topic><topic>Energy</topic><topic>Energy spectra</topic><topic>Geophysics</topic><topic>liquid structures</topic><topic>Radiation</topic><topic>Radiation dosage</topic><topic>Radiation measurement</topic><topic>Reduction</topic><topic>Scattering</topic><topic>Sciences of the Universe</topic><topic>Structural analysis</topic><topic>Structure-function relationships</topic><topic>synchrotron</topic><topic>Synchrotrons</topic><topic>X‐ray diffraction</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>King, A.</creatorcontrib><creatorcontrib>Guignot, N.</creatorcontrib><creatorcontrib>Henry, L.</creatorcontrib><creatorcontrib>Morard, G.</creatorcontrib><creatorcontrib>Clark, A.</creatorcontrib><creatorcontrib>Le Godec, Y.</creatorcontrib><creatorcontrib>Itié, J.-P.</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>Hyper Article en Ligne (HAL)</collection><collection>Hyper Article en Ligne (HAL) (Open Access)</collection><jtitle>Journal of applied crystallography</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>King, A.</au><au>Guignot, N.</au><au>Henry, L.</au><au>Morard, G.</au><au>Clark, A.</au><au>Le Godec, Y.</au><au>Itié, J.-P.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Combined angular and energy dispersive diffraction: optimized data acquisition, normalization and reduction</atitle><jtitle>Journal of applied crystallography</jtitle><date>2022-04</date><risdate>2022</risdate><volume>55</volume><issue>2</issue><spage>218</spage><epage>227</epage><pages>218-227</pages><issn>1600-5767</issn><issn>0021-8898</issn><eissn>1600-5767</eissn><abstract>Combined angular and energy dispersive diffraction is particularly well suited to experiments at high pressures in large‐volume presses, and to the study of liquid or amorphous systems. This work describes the data acquisition, correction and reduction approach developed at the PSICHE beamline of the SOLEIL synchrotron. The measured data were normalized for both the scattering volume and the effective incident energy spectrum. By optimizing the acquisition strategy, the measurement time and radiation dose are greatly reduced. The correction and reduction protocol outputs normalized scattering profiles that are suitable for pair distribution function or liquid structure analysis. These processes are demostrated with examples from a number of real experimental data sets.
An optimized methodology for collecting and analysing combined angular dispersive diffraction data is presented. This is particularly suitable for studying liquids or amorphous materials at high pressures.</abstract><cop>5 Abbey Square, Chester, Cheshire CH1 2HU, England</cop><pub>International Union of Crystallography</pub><doi>10.1107/S1600576722000322</doi><tpages>10</tpages><orcidid>https://orcid.org/0000-0001-6805-1283</orcidid><orcidid>https://orcid.org/0000-0001-8542-1354</orcidid><orcidid>https://orcid.org/0000-0002-4225-0767</orcidid><orcidid>https://orcid.org/0000-0001-9006-5745</orcidid><oa>free_for_read</oa></addata></record> |
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| ispartof | Journal of applied crystallography, 2022-04, Vol.55 (2), p.218-227 |
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| subjects | amorphous structures Data acquisition Diffraction Dispersion Distribution functions Earth Sciences Energy Energy spectra Geophysics liquid structures Radiation Radiation dosage Radiation measurement Reduction Scattering Sciences of the Universe Structural analysis Structure-function relationships synchrotron Synchrotrons X‐ray diffraction |
| title | Combined angular and energy dispersive diffraction: optimized data acquisition, normalization and reduction |
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