Surface Modification of 304L Stainless Steel and Interface Engineering by HiPIMS Pre-Treatment
A clean and defect-free substrate/coating interface is required to guarantee good adhesion of coatings under service conditions. For this purpose, an etching pre-treatment using High-Power Impulse Magnetron Sputtering (HiPIMS) was performed to modify the surface of 304L stainless steel. The effect o...
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| Veröffentlicht in: | Coatings (Basel) 2022-06, Vol.12 (6), p.727 |
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| creator | Chabanon, Angélique Michau, Alexandre Schlegel, Michel Léon Gündüz, Deniz C. Puga, Beatriz Miserque, Frédéric Schuster, Frédéric Maskrot, Hicham Pareige, Cristelle Cadel, Emmanuel Beainy, Georges Cloute-Cazalaa, Véronique Narasimalu, Srikanth Yao, Bingqing Dong, Zhili Balbaud-Célérier, Fanny |
| description | A clean and defect-free substrate/coating interface is required to guarantee good adhesion of coatings under service conditions. For this purpose, an etching pre-treatment using High-Power Impulse Magnetron Sputtering (HiPIMS) was performed to modify the surface of 304L stainless steel. The effect of three etching procedures on the substrate properties, such as corrosion resistance and adhesion, was investigated with unprecedented spatial resolution and spectroscopic details. Glancing angle X-ray diffraction showed modification in phase content but no neoformation after steel etching. X-ray photoelectron spectroscopy confirmed the presence of etchant species (6–7 at.%) on the extreme surface of the substrate. Transmission Electron Microscopy and Atomic Probe Tomography showed that the interface was less than a few nanometers wide. Polarization curves in a nitric acid solution at boiling temperature showed, for the first time, that the Ti+ and Zr+ etchings decreased the corrosion current density compared to the untreated original surface. Scratch-test measurements indicated better substrate/coating adhesion using HiPIMS metal ion etching. Electrochemical characterization revealed that Zr etching and thin coating improve the anti-corrosion properties of stainless steel in strong nitric acid conditions. |
| doi_str_mv | 10.3390/coatings12060727 |
| format | Article |
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For this purpose, an etching pre-treatment using High-Power Impulse Magnetron Sputtering (HiPIMS) was performed to modify the surface of 304L stainless steel. The effect of three etching procedures on the substrate properties, such as corrosion resistance and adhesion, was investigated with unprecedented spatial resolution and spectroscopic details. Glancing angle X-ray diffraction showed modification in phase content but no neoformation after steel etching. X-ray photoelectron spectroscopy confirmed the presence of etchant species (6–7 at.%) on the extreme surface of the substrate. Transmission Electron Microscopy and Atomic Probe Tomography showed that the interface was less than a few nanometers wide. Polarization curves in a nitric acid solution at boiling temperature showed, for the first time, that the Ti+ and Zr+ etchings decreased the corrosion current density compared to the untreated original surface. Scratch-test measurements indicated better substrate/coating adhesion using HiPIMS metal ion etching. Electrochemical characterization revealed that Zr etching and thin coating improve the anti-corrosion properties of stainless steel in strong nitric acid conditions.</description><identifier>ISSN: 2079-6412</identifier><identifier>EISSN: 2079-6412</identifier><identifier>DOI: 10.3390/coatings12060727</identifier><language>eng</language><publisher>Basel: MDPI AG</publisher><subject>Adhesion ; Austenitic stainless steels ; Bias ; Chemical bonds ; Condensed Matter ; Corrosion currents ; Corrosion effects ; Corrosion prevention ; Corrosion resistance ; Corrosion resistant steels ; Electrochemical analysis ; Engineering Sciences ; Etchants ; Interfaces ; Ion etching ; Magnetron sputtering ; Materials ; Mechanical properties ; Nitric acid ; Photoelectrons ; Physics ; Plasma etching ; Pretreatment ; Protective coatings ; Spatial resolution ; Stainless steel ; Substrates ; Titanium ; Zirconium</subject><ispartof>Coatings (Basel), 2022-06, Vol.12 (6), p.727</ispartof><rights>2022 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). 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Scratch-test measurements indicated better substrate/coating adhesion using HiPIMS metal ion etching. Electrochemical characterization revealed that Zr etching and thin coating improve the anti-corrosion properties of stainless steel in strong nitric acid conditions.</description><subject>Adhesion</subject><subject>Austenitic stainless steels</subject><subject>Bias</subject><subject>Chemical bonds</subject><subject>Condensed Matter</subject><subject>Corrosion currents</subject><subject>Corrosion effects</subject><subject>Corrosion prevention</subject><subject>Corrosion resistance</subject><subject>Corrosion resistant steels</subject><subject>Electrochemical analysis</subject><subject>Engineering Sciences</subject><subject>Etchants</subject><subject>Interfaces</subject><subject>Ion etching</subject><subject>Magnetron sputtering</subject><subject>Materials</subject><subject>Mechanical properties</subject><subject>Nitric acid</subject><subject>Photoelectrons</subject><subject>Physics</subject><subject>Plasma etching</subject><subject>Pretreatment</subject><subject>Protective coatings</subject><subject>Spatial resolution</subject><subject>Stainless steel</subject><subject>Substrates</subject><subject>Titanium</subject><subject>Zirconium</subject><issn>2079-6412</issn><issn>2079-6412</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2022</creationdate><recordtype>article</recordtype><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNpdkM1Lw0AQxRdRsGjvHhc8eYjuR7Ifx1KqLaRYaL0aNsls3ZJu6m4q9L83JSLiXOYx_ObN8BC6o-SRc02eqtZ0zm8jZUQQyeQFGjEidSJSyi7_6Gs0jnFH-tKUK6pH6H19DNZUgJdt7ayrep_W49ZiTtIcrzvjfAMx9gqgwcbXeOE7GFZmfus8QOgv4_KE5261WK7xKkCyCWC6PfjuFl1Z00QY__Qb9PY820znSf76sphO8qTiqewSm2nOakG0BqYrRZWoFSgJ1GZUEqZNTdKKGKZEyUvFy5pAatPMSKOU4CTjN-hh8P0wTXEIbm_CqWiNK-aTvDjPCBeK8ZR90Z69H9hDaD-PELti1x6D798rmJBa0kymoqfIQFWhjTGA_bWlpDiHXvwPnX8Dqvhz3g</recordid><startdate>20220601</startdate><enddate>20220601</enddate><creator>Chabanon, Angélique</creator><creator>Michau, Alexandre</creator><creator>Schlegel, Michel Léon</creator><creator>Gündüz, Deniz C.</creator><creator>Puga, Beatriz</creator><creator>Miserque, Frédéric</creator><creator>Schuster, Frédéric</creator><creator>Maskrot, Hicham</creator><creator>Pareige, Cristelle</creator><creator>Cadel, Emmanuel</creator><creator>Beainy, Georges</creator><creator>Cloute-Cazalaa, Véronique</creator><creator>Narasimalu, Srikanth</creator><creator>Yao, Bingqing</creator><creator>Dong, Zhili</creator><creator>Balbaud-Célérier, Fanny</creator><general>MDPI AG</general><general>MDPI</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>PDBOC</scope><scope>PIMPY</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>1XC</scope><scope>VOOES</scope><orcidid>https://orcid.org/0000-0002-7168-5006</orcidid><orcidid>https://orcid.org/0000-0001-8116-6747</orcidid><orcidid>https://orcid.org/0000-0002-8704-5038</orcidid><orcidid>https://orcid.org/0000-0002-7769-021X</orcidid><orcidid>https://orcid.org/0000-0002-3965-9588</orcidid><orcidid>https://orcid.org/0000-0003-1943-2631</orcidid><orcidid>https://orcid.org/0000-0002-2952-337X</orcidid><orcidid>https://orcid.org/0000-0002-7765-2854</orcidid></search><sort><creationdate>20220601</creationdate><title>Surface Modification of 304L Stainless Steel and Interface Engineering by HiPIMS Pre-Treatment</title><author>Chabanon, Angélique ; 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For this purpose, an etching pre-treatment using High-Power Impulse Magnetron Sputtering (HiPIMS) was performed to modify the surface of 304L stainless steel. The effect of three etching procedures on the substrate properties, such as corrosion resistance and adhesion, was investigated with unprecedented spatial resolution and spectroscopic details. Glancing angle X-ray diffraction showed modification in phase content but no neoformation after steel etching. X-ray photoelectron spectroscopy confirmed the presence of etchant species (6–7 at.%) on the extreme surface of the substrate. Transmission Electron Microscopy and Atomic Probe Tomography showed that the interface was less than a few nanometers wide. Polarization curves in a nitric acid solution at boiling temperature showed, for the first time, that the Ti+ and Zr+ etchings decreased the corrosion current density compared to the untreated original surface. 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| source | MDPI - Multidisciplinary Digital Publishing Institute; EZB-FREE-00999 freely available EZB journals; Alma/SFX Local Collection |
| subjects | Adhesion Austenitic stainless steels Bias Chemical bonds Condensed Matter Corrosion currents Corrosion effects Corrosion prevention Corrosion resistance Corrosion resistant steels Electrochemical analysis Engineering Sciences Etchants Interfaces Ion etching Magnetron sputtering Materials Mechanical properties Nitric acid Photoelectrons Physics Plasma etching Pretreatment Protective coatings Spatial resolution Stainless steel Substrates Titanium Zirconium |
| title | Surface Modification of 304L Stainless Steel and Interface Engineering by HiPIMS Pre-Treatment |
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