A calibration procedure for the assessment of work hardening part I: Effects of the microstructure and load type
This paper presents a methodology to define and quantify the level of work hardening locally in a material. The methodology is proposed after a thorough experimental study based on three complementary experimental techniques for microstructural characterizations: microhardness, X-ray diffraction (XR...
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Veröffentlicht in: | Materials characterization 2021-05, Vol.175, p.111067, Article 111067 |
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creator | Goulmy, J.P. Rouhaud, E. Kanoute, P. Toualbi, L. Kruch, S. Boyer, V. Badreddine, J. Retraint, D. |
description | This paper presents a methodology to define and quantify the level of work hardening locally in a material. The methodology is proposed after a thorough experimental study based on three complementary experimental techniques for microstructural characterizations: microhardness, X-ray diffraction (XRD) and Electron Backscatter Diffraction (EBSD) applied on Inconel 718 samples. In our analysis, several loading histories including single tension, single compression, high strain rates and low cycle fatigue have been investigated. The effects of the microstructure have been further investigated by modifying the size of the grains and the size of the strengthening precipitates. Experimental tests have also been simulated to choose a model variable able to represent work hardening. A reciprocal link between work hardening and experimental characterizations has then been established. Correlation curves have been proposed that enable to quantify the level of work hardening from the knowledge of the experimental data. Accuracy and complementarity of the three experimental approaches are discussed as well as the impact of the microstructure of the material on the measured quantities.
[Display omitted]
•The measurements performed are sensitive to the microstructure.•Correlate the level of equivalent plastic deformation with EBSD measurements.•Correlate the level of equivalent plastic deformation with XRD measurements.•Sensitivity to the microstructure is dependent on the characterization technique.•The characterization methods are complementary to determine work hardening. |
doi_str_mv | 10.1016/j.matchar.2021.111067 |
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[Display omitted]
•The measurements performed are sensitive to the microstructure.•Correlate the level of equivalent plastic deformation with EBSD measurements.•Correlate the level of equivalent plastic deformation with XRD measurements.•Sensitivity to the microstructure is dependent on the characterization technique.•The characterization methods are complementary to determine work hardening.</description><identifier>ISSN: 1044-5803</identifier><identifier>EISSN: 1873-4189</identifier><identifier>DOI: 10.1016/j.matchar.2021.111067</identifier><language>eng</language><publisher>Elsevier Inc</publisher><subject>Calibration ; EBSD ; Engineering Sciences ; Inconel 718 ; Mechanics ; Mechanics of materials ; Work hardening ; XRD</subject><ispartof>Materials characterization, 2021-05, Vol.175, p.111067, Article 111067</ispartof><rights>2021 Elsevier Inc.</rights><rights>Distributed under a Creative Commons Attribution 4.0 International License</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c390t-6f96f5e0b93a2953d2481171aee370f7d3049e2c64278b4e55f89b332a46b9be3</citedby><cites>FETCH-LOGICAL-c390t-6f96f5e0b93a2953d2481171aee370f7d3049e2c64278b4e55f89b332a46b9be3</cites><orcidid>0000-0003-2791-354X ; 0000-0001-6109-1389</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.sciencedirect.com/science/article/pii/S1044580321001972$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>230,314,776,780,881,3537,27901,27902,65306</link.rule.ids><backlink>$$Uhttps://hal.science/hal-03557016$$DView record in HAL$$Hfree_for_read</backlink></links><search><creatorcontrib>Goulmy, J.P.</creatorcontrib><creatorcontrib>Rouhaud, E.</creatorcontrib><creatorcontrib>Kanoute, P.</creatorcontrib><creatorcontrib>Toualbi, L.</creatorcontrib><creatorcontrib>Kruch, S.</creatorcontrib><creatorcontrib>Boyer, V.</creatorcontrib><creatorcontrib>Badreddine, J.</creatorcontrib><creatorcontrib>Retraint, D.</creatorcontrib><title>A calibration procedure for the assessment of work hardening part I: Effects of the microstructure and load type</title><title>Materials characterization</title><description>This paper presents a methodology to define and quantify the level of work hardening locally in a material. The methodology is proposed after a thorough experimental study based on three complementary experimental techniques for microstructural characterizations: microhardness, X-ray diffraction (XRD) and Electron Backscatter Diffraction (EBSD) applied on Inconel 718 samples. In our analysis, several loading histories including single tension, single compression, high strain rates and low cycle fatigue have been investigated. The effects of the microstructure have been further investigated by modifying the size of the grains and the size of the strengthening precipitates. Experimental tests have also been simulated to choose a model variable able to represent work hardening. A reciprocal link between work hardening and experimental characterizations has then been established. Correlation curves have been proposed that enable to quantify the level of work hardening from the knowledge of the experimental data. Accuracy and complementarity of the three experimental approaches are discussed as well as the impact of the microstructure of the material on the measured quantities.
[Display omitted]
•The measurements performed are sensitive to the microstructure.•Correlate the level of equivalent plastic deformation with EBSD measurements.•Correlate the level of equivalent plastic deformation with XRD measurements.•Sensitivity to the microstructure is dependent on the characterization technique.•The characterization methods are complementary to determine work hardening.</description><subject>Calibration</subject><subject>EBSD</subject><subject>Engineering Sciences</subject><subject>Inconel 718</subject><subject>Mechanics</subject><subject>Mechanics of materials</subject><subject>Work hardening</subject><subject>XRD</subject><issn>1044-5803</issn><issn>1873-4189</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2021</creationdate><recordtype>article</recordtype><recordid>eNqFkE9LAzEQxYMoWKsfQcjVw67JJvsnXqSUagsFL3oO2ezEpm43S5JW_PbussWrpxmG997M_BC6pySlhBaP-_Sgot4pn2YkoymllBTlBZrRqmQJp5W4HHrCeZJXhF2jmxD2hJCiouUM9QusVWtrr6J1He6909AcPWDjPI47wCoECOEAXcTO4G_nv_CwqYHOdp-4Vz7izRNeGQM6hlExeg5WexeiP-o4Rqmuwa1TDY4_PdyiK6PaAHfnOkcfL6v35TrZvr1ulottopkgMSmMKEwOpBZMZSJnTcYrSkuqAFhJTNkwwgVkuuBZWdUc8txUomYsU7yoRQ1sjh6m3J1qZe_tQfkf6ZSV68VWjjPC8rwc8J2yQZtP2vHs4MH8GSiRI2K5l2fEckQsJ8SD73nywfDIyYKXQVvoBoLWDzxk4-w_Cb-p0od-</recordid><startdate>20210501</startdate><enddate>20210501</enddate><creator>Goulmy, J.P.</creator><creator>Rouhaud, E.</creator><creator>Kanoute, P.</creator><creator>Toualbi, L.</creator><creator>Kruch, S.</creator><creator>Boyer, V.</creator><creator>Badreddine, J.</creator><creator>Retraint, D.</creator><general>Elsevier Inc</general><general>Elsevier</general><scope>AAYXX</scope><scope>CITATION</scope><scope>1XC</scope><scope>VOOES</scope><orcidid>https://orcid.org/0000-0003-2791-354X</orcidid><orcidid>https://orcid.org/0000-0001-6109-1389</orcidid></search><sort><creationdate>20210501</creationdate><title>A calibration procedure for the assessment of work hardening part I: Effects of the microstructure and load type</title><author>Goulmy, J.P. ; Rouhaud, E. ; Kanoute, P. ; Toualbi, L. ; Kruch, S. ; Boyer, V. ; Badreddine, J. ; Retraint, D.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c390t-6f96f5e0b93a2953d2481171aee370f7d3049e2c64278b4e55f89b332a46b9be3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2021</creationdate><topic>Calibration</topic><topic>EBSD</topic><topic>Engineering Sciences</topic><topic>Inconel 718</topic><topic>Mechanics</topic><topic>Mechanics of materials</topic><topic>Work hardening</topic><topic>XRD</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Goulmy, J.P.</creatorcontrib><creatorcontrib>Rouhaud, E.</creatorcontrib><creatorcontrib>Kanoute, P.</creatorcontrib><creatorcontrib>Toualbi, L.</creatorcontrib><creatorcontrib>Kruch, S.</creatorcontrib><creatorcontrib>Boyer, V.</creatorcontrib><creatorcontrib>Badreddine, J.</creatorcontrib><creatorcontrib>Retraint, D.</creatorcontrib><collection>CrossRef</collection><collection>Hyper Article en Ligne (HAL)</collection><collection>Hyper Article en Ligne (HAL) (Open Access)</collection><jtitle>Materials characterization</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Goulmy, J.P.</au><au>Rouhaud, E.</au><au>Kanoute, P.</au><au>Toualbi, L.</au><au>Kruch, S.</au><au>Boyer, V.</au><au>Badreddine, J.</au><au>Retraint, D.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>A calibration procedure for the assessment of work hardening part I: Effects of the microstructure and load type</atitle><jtitle>Materials characterization</jtitle><date>2021-05-01</date><risdate>2021</risdate><volume>175</volume><spage>111067</spage><pages>111067-</pages><artnum>111067</artnum><issn>1044-5803</issn><eissn>1873-4189</eissn><abstract>This paper presents a methodology to define and quantify the level of work hardening locally in a material. The methodology is proposed after a thorough experimental study based on three complementary experimental techniques for microstructural characterizations: microhardness, X-ray diffraction (XRD) and Electron Backscatter Diffraction (EBSD) applied on Inconel 718 samples. In our analysis, several loading histories including single tension, single compression, high strain rates and low cycle fatigue have been investigated. The effects of the microstructure have been further investigated by modifying the size of the grains and the size of the strengthening precipitates. Experimental tests have also been simulated to choose a model variable able to represent work hardening. A reciprocal link between work hardening and experimental characterizations has then been established. Correlation curves have been proposed that enable to quantify the level of work hardening from the knowledge of the experimental data. Accuracy and complementarity of the three experimental approaches are discussed as well as the impact of the microstructure of the material on the measured quantities.
[Display omitted]
•The measurements performed are sensitive to the microstructure.•Correlate the level of equivalent plastic deformation with EBSD measurements.•Correlate the level of equivalent plastic deformation with XRD measurements.•Sensitivity to the microstructure is dependent on the characterization technique.•The characterization methods are complementary to determine work hardening.</abstract><pub>Elsevier Inc</pub><doi>10.1016/j.matchar.2021.111067</doi><orcidid>https://orcid.org/0000-0003-2791-354X</orcidid><orcidid>https://orcid.org/0000-0001-6109-1389</orcidid><oa>free_for_read</oa></addata></record> |
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subjects | Calibration EBSD Engineering Sciences Inconel 718 Mechanics Mechanics of materials Work hardening XRD |
title | A calibration procedure for the assessment of work hardening part I: Effects of the microstructure and load type |
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