Characterization of the conglomerate form of acetyl-dl-leucine by thermal analysis and solubility measurements

Starting from a mixture of enantiomers in solution, crystallization can generate different types of crystals. In order to determine which type of crystal is obtained in the case of acetyl leucine, an active pharmaceutical ingredient (API), analytical methods have been used to partially elucidate the...

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Veröffentlicht in:	Journal of crystal growth 2012-03, Vol.342 (1), p.28-33
Hauptverfasser:	Estime, N., Pena, R., Teychené, S., Autret, J.M., Biscans, B.
Format:	Artikel
Sprache:	eng
Schlagworte:	A1. Conglomerate A1. Phase diagram A1. Racemic A2. Crystallization B1. Acetyl leucine Binary systems Chemical engineering Chemical Sciences Condensed matter: structure, mechanical and thermal properties Cristallography Crystalline state (including molecular motions in solids) Crystallization Crystallographic aspects of phase transformations pressure effects Crystals Differential scanning calorimetry Enantiomers Engineering Sciences Equations of state, phase equilibria, and phase transitions Exact sciences and technology Fluid Dynamics Ingredients Life Sciences Mechanics Organic compounds Pharmaceutical sciences Phase diagrams Physics Solubility Solubility, segregation, and mixing phase separation Structure of solids and liquids crystallography Structure of specific crystalline solids Thermics
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