Experimental Study of Pt Solubility in the CO-CO2 Fluid at Low fO2 and Subsolidus Conditions of the Ultramafic-Mafic Intrusions
The solubility of Pt in CO-CO2 fluid was studied experimentally at P = 50–200 MPa and T = 950 °C. A mixture of MgC2O4 and MgCO3 was used as a source of the fluid. Upon the reaction of the Pt capsule walls and the fluid, a carbonyl of platinum is formed. The use of the high-temperature quartz ceramic...
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| creator | Simakin, Alexander Salova, Tamara Borisova, Anastassia Y. Pokrovski, Gleb S. Shaposhnikova, Olga Tyutyunnik, Oksana Bondarenko, Galina Nekrasov, Alexey Isaenko, Sergey I. |
| description | The solubility of Pt in CO-CO2 fluid was studied experimentally at P = 50–200 MPa and T = 950 °C. A mixture of MgC2O4 and MgCO3 was used as a source of the fluid. Upon the reaction of the Pt capsule walls and the fluid, a carbonyl of platinum is formed. The use of the high-temperature quartz ceramics as a fluid trap avoids the effect of mechanical contamination with Pt from the eroded capsule walls. The total content of platinum in the porous fluid traps was measured by the Electrothermal Atomic Absorption (ET-AAS) method. In some experiments, the local analysis of traps was carried out by the Laser Ablation Inductively Coupled Plasma Mass Spectrometry (LA-ICP-MS) method. The composition of fluid in bubbles captured in an albite glass trap was studied by micro-Raman spectroscopy. On the capsule walls and MgO, Pt “whiskers” of submicron diameter were observed, which were formed as a product of carbonyl decomposition during quenching. About 5–15% of carbonyl withstands quenching resulting in 1.5 to 2 ppm Pt soluble in acetone (runs at P = 200 MPa) in a quartz glass trap. The amount of Pt soluble in acetone from the capsule walls corresponds to a concentration of up to 8 ppm in the fluid. A high content of soluble Pt of 2000–3000 ppm was determined in a carbon coated MgO matrix. Our study demonstrated that the solubility of Pt in the CO-CO2 fluid is 15–150 ppm, presumably in the form of Pt3(CO)62− under conditions corresponding to the conditions of the subsolidus stage of layered ultramafic-mafic and ultramafic-alkaline intrusions formation. Our preliminary data showed that this solubility will increase with the addition of water at low fO2. |
| doi_str_mv | 10.3390/min11020225 |
| format | Article |
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A mixture of MgC2O4 and MgCO3 was used as a source of the fluid. Upon the reaction of the Pt capsule walls and the fluid, a carbonyl of platinum is formed. The use of the high-temperature quartz ceramics as a fluid trap avoids the effect of mechanical contamination with Pt from the eroded capsule walls. The total content of platinum in the porous fluid traps was measured by the Electrothermal Atomic Absorption (ET-AAS) method. In some experiments, the local analysis of traps was carried out by the Laser Ablation Inductively Coupled Plasma Mass Spectrometry (LA-ICP-MS) method. The composition of fluid in bubbles captured in an albite glass trap was studied by micro-Raman spectroscopy. On the capsule walls and MgO, Pt “whiskers” of submicron diameter were observed, which were formed as a product of carbonyl decomposition during quenching. About 5–15% of carbonyl withstands quenching resulting in 1.5 to 2 ppm Pt soluble in acetone (runs at P = 200 MPa) in a quartz glass trap. The amount of Pt soluble in acetone from the capsule walls corresponds to a concentration of up to 8 ppm in the fluid. A high content of soluble Pt of 2000–3000 ppm was determined in a carbon coated MgO matrix. Our study demonstrated that the solubility of Pt in the CO-CO2 fluid is 15–150 ppm, presumably in the form of Pt3(CO)62− under conditions corresponding to the conditions of the subsolidus stage of layered ultramafic-mafic and ultramafic-alkaline intrusions formation. Our preliminary data showed that this solubility will increase with the addition of water at low fO2.</description><identifier>ISSN: 2075-163X</identifier><identifier>EISSN: 2075-163X</identifier><identifier>DOI: 10.3390/min11020225</identifier><language>eng</language><publisher>Basel: MDPI AG</publisher><subject>Ablation ; Acetone ; Analytical methods ; Carbon dioxide ; Carbonyl compounds ; Carbonyls ; Ceramics ; Contamination ; Decomposition ; Diameters ; Earth Sciences ; Geochemistry ; Glass ; Graphite ; High temperature ; Inductively coupled plasma mass spectrometry ; Laser ablation ; Lasers ; Magnesium carbonate ; Magnesium oxide ; Mass spectrometry ; Mass spectroscopy ; Mineralogy ; Platinum ; Quartz ; Quenching ; Raman spectroscopy ; Sciences of the Universe ; Silica glass ; Solubility ; Spectral analysis ; Temperature ; Traps ; Walls ; Whiskers (metals)</subject><ispartof>Minerals (Basel), 2021-02, Vol.11 (2), p.225</ispartof><rights>2021. 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A mixture of MgC2O4 and MgCO3 was used as a source of the fluid. Upon the reaction of the Pt capsule walls and the fluid, a carbonyl of platinum is formed. The use of the high-temperature quartz ceramics as a fluid trap avoids the effect of mechanical contamination with Pt from the eroded capsule walls. The total content of platinum in the porous fluid traps was measured by the Electrothermal Atomic Absorption (ET-AAS) method. In some experiments, the local analysis of traps was carried out by the Laser Ablation Inductively Coupled Plasma Mass Spectrometry (LA-ICP-MS) method. The composition of fluid in bubbles captured in an albite glass trap was studied by micro-Raman spectroscopy. On the capsule walls and MgO, Pt “whiskers” of submicron diameter were observed, which were formed as a product of carbonyl decomposition during quenching. About 5–15% of carbonyl withstands quenching resulting in 1.5 to 2 ppm Pt soluble in acetone (runs at P = 200 MPa) in a quartz glass trap. The amount of Pt soluble in acetone from the capsule walls corresponds to a concentration of up to 8 ppm in the fluid. A high content of soluble Pt of 2000–3000 ppm was determined in a carbon coated MgO matrix. Our study demonstrated that the solubility of Pt in the CO-CO2 fluid is 15–150 ppm, presumably in the form of Pt3(CO)62− under conditions corresponding to the conditions of the subsolidus stage of layered ultramafic-mafic and ultramafic-alkaline intrusions formation. Our preliminary data showed that this solubility will increase with the addition of water at low fO2.</description><subject>Ablation</subject><subject>Acetone</subject><subject>Analytical methods</subject><subject>Carbon dioxide</subject><subject>Carbonyl compounds</subject><subject>Carbonyls</subject><subject>Ceramics</subject><subject>Contamination</subject><subject>Decomposition</subject><subject>Diameters</subject><subject>Earth Sciences</subject><subject>Geochemistry</subject><subject>Glass</subject><subject>Graphite</subject><subject>High temperature</subject><subject>Inductively coupled plasma mass spectrometry</subject><subject>Laser ablation</subject><subject>Lasers</subject><subject>Magnesium carbonate</subject><subject>Magnesium oxide</subject><subject>Mass spectrometry</subject><subject>Mass spectroscopy</subject><subject>Mineralogy</subject><subject>Platinum</subject><subject>Quartz</subject><subject>Quenching</subject><subject>Raman spectroscopy</subject><subject>Sciences of the Universe</subject><subject>Silica glass</subject><subject>Solubility</subject><subject>Spectral analysis</subject><subject>Temperature</subject><subject>Traps</subject><subject>Walls</subject><subject>Whiskers (metals)</subject><issn>2075-163X</issn><issn>2075-163X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2021</creationdate><recordtype>article</recordtype><sourceid>BENPR</sourceid><recordid>eNpNkVtLwzAYhoMoOOau_AMBr0SqOTQ9XI6yuUFlwhx4V9ImYRlZM5tU3ZV_3ZSJLBfJx5vne_kOANxi9Ehpjp72usUYEUQIuwAjglIW4YS-X57F12Di3A6Fk2OaMTICP7Pvg-z0XraeG7j2vThCq-Crh2tr-lob7Y9Qt9BvJSxWUbEicG56LSD3sLRfUAWBtwKu-9pZo0XvYGFbob22rRuchsSN8R3fc6Wb6GW44bL1Xe8G5AZcKW6cnPy9Y7CZz96KRVSunpfFtIwaEofimYgTqdI0lTxXKGmyJqklybFKWGhYNIJQLpAk4aOpVdIwViskRBYjwuowFDoG9yffLTfVITTMu2Nlua4W07IaNERxglmWf-LA3p3YQ2c_eul8tbN914byKhLnMUrCkAfq4UQ1nXWuk-rfFqNqWEh1thD6C-OvfQw</recordid><startdate>20210201</startdate><enddate>20210201</enddate><creator>Simakin, Alexander</creator><creator>Salova, 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Study of Pt Solubility in the CO-CO2 Fluid at Low fO2 and Subsolidus Conditions of the Ultramafic-Mafic Intrusions</title><author>Simakin, Alexander ; Salova, Tamara ; Borisova, Anastassia Y. ; Pokrovski, Gleb S. ; Shaposhnikova, Olga ; Tyutyunnik, Oksana ; Bondarenko, Galina ; Nekrasov, Alexey ; Isaenko, Sergey I.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c2475-5d46ef777ea9f06c8c6be291f65202dcd23ad0e2c8ccbf6c55bf0dd84025b1023</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2021</creationdate><topic>Ablation</topic><topic>Acetone</topic><topic>Analytical methods</topic><topic>Carbon dioxide</topic><topic>Carbonyl compounds</topic><topic>Carbonyls</topic><topic>Ceramics</topic><topic>Contamination</topic><topic>Decomposition</topic><topic>Diameters</topic><topic>Earth Sciences</topic><topic>Geochemistry</topic><topic>Glass</topic><topic>Graphite</topic><topic>High temperature</topic><topic>Inductively coupled plasma mass spectrometry</topic><topic>Laser ablation</topic><topic>Lasers</topic><topic>Magnesium carbonate</topic><topic>Magnesium oxide</topic><topic>Mass spectrometry</topic><topic>Mass spectroscopy</topic><topic>Mineralogy</topic><topic>Platinum</topic><topic>Quartz</topic><topic>Quenching</topic><topic>Raman spectroscopy</topic><topic>Sciences of the Universe</topic><topic>Silica glass</topic><topic>Solubility</topic><topic>Spectral analysis</topic><topic>Temperature</topic><topic>Traps</topic><topic>Walls</topic><topic>Whiskers (metals)</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Simakin, Alexander</creatorcontrib><creatorcontrib>Salova, Tamara</creatorcontrib><creatorcontrib>Borisova, Anastassia Y.</creatorcontrib><creatorcontrib>Pokrovski, Gleb S.</creatorcontrib><creatorcontrib>Shaposhnikova, Olga</creatorcontrib><creatorcontrib>Tyutyunnik, 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Edition</collection><collection>ProQuest Central Basic</collection><collection>Hyper Article en Ligne (HAL)</collection><collection>Hyper Article en Ligne (HAL) (Open Access)</collection><jtitle>Minerals (Basel)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Simakin, Alexander</au><au>Salova, Tamara</au><au>Borisova, Anastassia Y.</au><au>Pokrovski, Gleb S.</au><au>Shaposhnikova, Olga</au><au>Tyutyunnik, Oksana</au><au>Bondarenko, Galina</au><au>Nekrasov, Alexey</au><au>Isaenko, Sergey I.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Experimental Study of Pt Solubility in the CO-CO2 Fluid at Low fO2 and Subsolidus Conditions of the Ultramafic-Mafic Intrusions</atitle><jtitle>Minerals (Basel)</jtitle><date>2021-02-01</date><risdate>2021</risdate><volume>11</volume><issue>2</issue><spage>225</spage><pages>225-</pages><issn>2075-163X</issn><eissn>2075-163X</eissn><abstract>The solubility of Pt in CO-CO2 fluid was studied experimentally at P = 50–200 MPa and T = 950 °C. A mixture of MgC2O4 and MgCO3 was used as a source of the fluid. Upon the reaction of the Pt capsule walls and the fluid, a carbonyl of platinum is formed. The use of the high-temperature quartz ceramics as a fluid trap avoids the effect of mechanical contamination with Pt from the eroded capsule walls. The total content of platinum in the porous fluid traps was measured by the Electrothermal Atomic Absorption (ET-AAS) method. In some experiments, the local analysis of traps was carried out by the Laser Ablation Inductively Coupled Plasma Mass Spectrometry (LA-ICP-MS) method. The composition of fluid in bubbles captured in an albite glass trap was studied by micro-Raman spectroscopy. On the capsule walls and MgO, Pt “whiskers” of submicron diameter were observed, which were formed as a product of carbonyl decomposition during quenching. About 5–15% of carbonyl withstands quenching resulting in 1.5 to 2 ppm Pt soluble in acetone (runs at P = 200 MPa) in a quartz glass trap. The amount of Pt soluble in acetone from the capsule walls corresponds to a concentration of up to 8 ppm in the fluid. A high content of soluble Pt of 2000–3000 ppm was determined in a carbon coated MgO matrix. Our study demonstrated that the solubility of Pt in the CO-CO2 fluid is 15–150 ppm, presumably in the form of Pt3(CO)62− under conditions corresponding to the conditions of the subsolidus stage of layered ultramafic-mafic and ultramafic-alkaline intrusions formation. Our preliminary data showed that this solubility will increase with the addition of water at low fO2.</abstract><cop>Basel</cop><pub>MDPI AG</pub><doi>10.3390/min11020225</doi><orcidid>https://orcid.org/0000-0002-6498-7188</orcidid><orcidid>https://orcid.org/0000-0001-6373-726X</orcidid><orcidid>https://orcid.org/0000-0003-2050-3310</orcidid><orcidid>https://orcid.org/0000-0003-0906-1689</orcidid><oa>free_for_read</oa></addata></record> |
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| ispartof | Minerals (Basel), 2021-02, Vol.11 (2), p.225 |
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| source | MDPI - Multidisciplinary Digital Publishing Institute; Elektronische Zeitschriftenbibliothek - Frei zugängliche E-Journals; Alma/SFX Local Collection |
| subjects | Ablation Acetone Analytical methods Carbon dioxide Carbonyl compounds Carbonyls Ceramics Contamination Decomposition Diameters Earth Sciences Geochemistry Glass Graphite High temperature Inductively coupled plasma mass spectrometry Laser ablation Lasers Magnesium carbonate Magnesium oxide Mass spectrometry Mass spectroscopy Mineralogy Platinum Quartz Quenching Raman spectroscopy Sciences of the Universe Silica glass Solubility Spectral analysis Temperature Traps Walls Whiskers (metals) |
| title | Experimental Study of Pt Solubility in the CO-CO2 Fluid at Low fO2 and Subsolidus Conditions of the Ultramafic-Mafic Intrusions |
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