Characterization of Ficus sycomorus tannin using ATR-FT MIR, MALDI-TOF MS and 13C NMR methods

The Ficus sycomorus bark tannin was extracted and characterized using Attenuated Total Reflectance Fourier Transform Middle Infrared (ATR-FT MIR) spectra in the 1800 and 600 cm −1 range, Matrix Assisted Laser Desorption Ionisation Time of Flight Mass Spectrometry (MALDI-TOF MS) and Carbon-13 Nuclear...

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Veröffentlicht in:European journal of wood and wood products 2017-09, Vol.75 (5), p.807-815
Hauptverfasser: Konai, Noel, Raidandi, Danwe, Pizzi, Antonio, Meva’a, Lucien
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container_issue 5
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container_title European journal of wood and wood products
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creator Konai, Noel
Raidandi, Danwe
Pizzi, Antonio
Meva’a, Lucien
description The Ficus sycomorus bark tannin was extracted and characterized using Attenuated Total Reflectance Fourier Transform Middle Infrared (ATR-FT MIR) spectra in the 1800 and 600 cm −1 range, Matrix Assisted Laser Desorption Ionisation Time of Flight Mass Spectrometry (MALDI-TOF MS) and Carbon-13 Nuclear Magnetic Resonance ( 13 C NMR) spectroscopy methods. Ficus sycomorus species have a very high percentage (46%) yield of tannin. These three characterization methods have shown that the Ficus sycomorus bark tannin is condensed and particularly a procyanidin type. It is composed of quercetin, apigenin, fisetinidin, catechin, gallocatechin, chalcone, radicinin, catechin gallate units with the presence of carbohydrates, quinone and gallic acid residues. The analysis results revealed that quercetin are the major constituents of Ficus sycomorus bark tannin. This procyanidin type tannin can give good wood adhesives.
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J. Wood Prod</addtitle><description>The Ficus sycomorus bark tannin was extracted and characterized using Attenuated Total Reflectance Fourier Transform Middle Infrared (ATR-FT MIR) spectra in the 1800 and 600 cm −1 range, Matrix Assisted Laser Desorption Ionisation Time of Flight Mass Spectrometry (MALDI-TOF MS) and Carbon-13 Nuclear Magnetic Resonance ( 13 C NMR) spectroscopy methods. Ficus sycomorus species have a very high percentage (46%) yield of tannin. These three characterization methods have shown that the Ficus sycomorus bark tannin is condensed and particularly a procyanidin type. It is composed of quercetin, apigenin, fisetinidin, catechin, gallocatechin, chalcone, radicinin, catechin gallate units with the presence of carbohydrates, quinone and gallic acid residues. The analysis results revealed that quercetin are the major constituents of Ficus sycomorus bark tannin. 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ispartof European journal of wood and wood products, 2017-09, Vol.75 (5), p.807-815
issn 0018-3768
1436-736X
language eng
recordid cdi_hal_primary_oai_HAL_hal_03101278v1
source SpringerLink Journals
subjects adhesives
apigenin
Bark
Biomedical and Life Sciences
Carbohydrates
Carbon 13
Catechin
Ceramics
chalcone
Composites
desorption
Engineering Sciences
epigallocatechin
Ficus sycomorus
Fourier analysis
Fourier transforms
Gallic acid
Glass
Infrared spectra
ionization
Ions
Life Sciences
Machines
Manufacturing
Mass spectrometry
Mass spectroscopy
matrix-assisted laser desorption-ionization mass spectrometry
Natural Materials
NMR
Nuclear magnetic resonance
nuclear magnetic resonance spectroscopy
Original
Processes
procyanidins
Quercetin
Quinones
reflectance
Tannins
wood
Wood Science & Technology
title Characterization of Ficus sycomorus tannin using ATR-FT MIR, MALDI-TOF MS and 13C NMR methods
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