Analysis and determination of secondary organic aerosol (SOA) tracers (markers) in particulate matter standard reference material (SRM 1649b, urban dust)
Secondary organic aerosol (SOA) accounts for a significant fraction of particulate matter (PM) in the atmosphere. Source identification, including the SOA fraction, is critical for the effective management of air pollution. Molecular SOA markers (tracers) are key compounds allowing the source apport...
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| Veröffentlicht in: | Analytical and bioanalytical chemistry 2019-09, Vol.411 (23), p.5975-5983 |
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| creator | Albinet, Alexandre Lanzafame, Grazia Maria Srivastava, Deepchandra Bonnaire, Nicolas Nalin, Frederica Wise, Stephen A. |
| description | Secondary organic aerosol (SOA) accounts for a significant fraction of particulate matter (PM) in the atmosphere. Source identification, including the SOA fraction, is critical for the effective management of air pollution. Molecular SOA markers (tracers) are key compounds allowing the source apportionment of SOA using different methodologies. Therefore, accurate SOA marker measurements in ambient air PM are important. This study determined the concentrations of 12 key SOA markers (biogenic and anthropogenic) in the urban dust standard reference material available from the National Institute of Standards and Technology (NIST) (SRM 1649b). Two extraction procedures, sonication and QuEChERS-like (quick easy cheap effective rugged and safe), have been compared. Three research laboratories/institutes using two analytical techniques (gas chromatography/mass spectrometry (GC/MS) and ultra-high-pressure liquid chromatography/tandem mass spectrometry (HPLC/MS-MS)) carried out the analyses. The results obtained were all in good agreement, except for 2-methylerythritol. The analysis of this compound still seems to be challenging by both GC/MS (large injection repeatability) and HPLC/MS-MS (separation issues of both 2-methyltetrols: 2-methylthreitol and 2-methylerythritol). Possible inhomogeneity in the SRM for this compound could also explain the large discrepancies observed. Sonication and QuEChERS-like procedures gave comparable results for the extraction of the SOA markers showing that QuEChERS-like extraction is suitable for the analysis of SOA markers in ambient air PM. As this study provides, for the first time, indicative values in a reference material for typical SOA markers, the analysis of SRM 1649b (urban dust) could be used for quality control/assurance purposes.
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| doi_str_mv | 10.1007/s00216-019-02015-6 |
| format | Article |
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Graphical abstract</description><subject>Aerosols</subject><subject>Air pollution</subject><subject>Analytical Chemistry</subject><subject>Anthropogenic factors</subject><subject>Biochemistry</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Chromatography</subject><subject>Continental interfaces, environment</subject><subject>Dust</subject><subject>Dust control</subject><subject>Food Science</subject><subject>Gas chromatography</subject><subject>High performance liquid chromatography</subject><subject>Inhomogeneity</subject><subject>Laboratories</subject><subject>Laboratory Medicine</subject><subject>Liquid chromatography</subject><subject>Markers</subject><subject>Mass spectrometry</subject><subject>Mass spectroscopy</subject><subject>Monitoring/Environmental Analysis</subject><subject>Ocean, Atmosphere</subject><subject>Paper in Forefront</subject><subject>Particulate 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and determination of secondary organic aerosol (SOA) tracers (markers) in particulate matter standard reference material (SRM 1649b, urban dust)</title><author>Albinet, Alexandre ; Lanzafame, Grazia Maria ; Srivastava, Deepchandra ; Bonnaire, Nicolas ; Nalin, Frederica ; Wise, Stephen A.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c490t-62e912e968906b0373c3ec2a65b871d6af41d120db2ee479299264a7bb7e91203</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2019</creationdate><topic>Aerosols</topic><topic>Air pollution</topic><topic>Analytical Chemistry</topic><topic>Anthropogenic factors</topic><topic>Biochemistry</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Chromatography</topic><topic>Continental interfaces, environment</topic><topic>Dust</topic><topic>Dust control</topic><topic>Food 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Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Albinet, Alexandre</au><au>Lanzafame, Grazia Maria</au><au>Srivastava, Deepchandra</au><au>Bonnaire, Nicolas</au><au>Nalin, Frederica</au><au>Wise, Stephen A.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Analysis and determination of secondary organic aerosol (SOA) tracers (markers) in particulate matter standard reference material (SRM 1649b, urban dust)</atitle><jtitle>Analytical and bioanalytical chemistry</jtitle><stitle>Anal Bioanal Chem</stitle><addtitle>Anal Bioanal Chem</addtitle><date>2019-09-01</date><risdate>2019</risdate><volume>411</volume><issue>23</issue><spage>5975</spage><epage>5983</epage><pages>5975-5983</pages><issn>1618-2642</issn><eissn>1618-2650</eissn><abstract>Secondary organic aerosol (SOA) accounts for a significant fraction of particulate matter (PM) in the atmosphere. Source identification, including the SOA fraction, is critical for the effective management of air pollution. Molecular SOA markers (tracers) are key compounds allowing the source apportionment of SOA using different methodologies. Therefore, accurate SOA marker measurements in ambient air PM are important. This study determined the concentrations of 12 key SOA markers (biogenic and anthropogenic) in the urban dust standard reference material available from the National Institute of Standards and Technology (NIST) (SRM 1649b). Two extraction procedures, sonication and QuEChERS-like (quick easy cheap effective rugged and safe), have been compared. Three research laboratories/institutes using two analytical techniques (gas chromatography/mass spectrometry (GC/MS) and ultra-high-pressure liquid chromatography/tandem mass spectrometry (HPLC/MS-MS)) carried out the analyses. The results obtained were all in good agreement, except for 2-methylerythritol. The analysis of this compound still seems to be challenging by both GC/MS (large injection repeatability) and HPLC/MS-MS (separation issues of both 2-methyltetrols: 2-methylthreitol and 2-methylerythritol). Possible inhomogeneity in the SRM for this compound could also explain the large discrepancies observed. Sonication and QuEChERS-like procedures gave comparable results for the extraction of the SOA markers showing that QuEChERS-like extraction is suitable for the analysis of SOA markers in ambient air PM. As this study provides, for the first time, indicative values in a reference material for typical SOA markers, the analysis of SRM 1649b (urban dust) could be used for quality control/assurance purposes.
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| subjects | Aerosols Air pollution Analytical Chemistry Anthropogenic factors Biochemistry Characterization and Evaluation of Materials Chemistry Chemistry and Materials Science Chromatography Continental interfaces, environment Dust Dust control Food Science Gas chromatography High performance liquid chromatography Inhomogeneity Laboratories Laboratory Medicine Liquid chromatography Markers Mass spectrometry Mass spectroscopy Monitoring/Environmental Analysis Ocean, Atmosphere Paper in Forefront Particulate emissions Particulate matter Quality assurance Quality control Reference materials Sciences of the Universe Scientific imaging Sonication Spectroscopy Tracers |
| title | Analysis and determination of secondary organic aerosol (SOA) tracers (markers) in particulate matter standard reference material (SRM 1649b, urban dust) |
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