The morphology of submicronsized core–shell latex particles: An electron microscopy study
The core–shell structure of a range of acrylic–acrylic latexes has been investigated by combining different specimen preparation methods with transmission electron microscopy (TEM), dark-field scanning transmission electron microscopy (DSTEM) and low-voltage scanning electron microscopy (LV-SEM), in...
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| Veröffentlicht in: | Micron (Oxford, England : 1993) England : 1993), 2007-01, Vol.38 (5), p.522-535 |
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| container_title | Micron (Oxford, England : 1993) |
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| creator | Gaillard, Cédric Fuchs, Gilbert Plummer, Christopher J.G. Stadelmann, Pierre A. |
| description | The core–shell structure of a range of acrylic–acrylic latexes has been investigated by combining different specimen preparation methods with transmission electron microscopy (TEM), dark-field scanning transmission electron microscopy (DSTEM) and low-voltage scanning electron microscopy (LV-SEM), including the first reported use of LV-SEM to observe composite latex particles at ambient and subambient temperatures. Spin-coating of liquid latex dispersions directly onto TEM grids or SEM stubs is shown to be a relatively straightforward mean of avoiding film formation during specimen preparation. In conjunction with double staining techniques, it has been found to be particularly convenient for characterizing the fine structure of particles with diameters down to below 100
nm. |
| doi_str_mv | 10.1016/j.micron.2006.07.023 |
| format | Article |
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| ispartof | Micron (Oxford, England : 1993), 2007-01, Vol.38 (5), p.522-535 |
| issn | 0968-4328 1878-4291 |
| language | eng |
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| source | Elsevier ScienceDirect Journals |
| subjects | Chemical and Process Engineering Core–shell latex Engineering Sciences Food engineering Life Sciences Low-voltage scanning electron microscopy (LV-SEM) Morphological characterization Multiple chemical staining Rubber toughened PMMA Spin-coating Transmission electron microscopy (TEM) |
| title | The morphology of submicronsized core–shell latex particles: An electron microscopy study |
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