Preparation of functionalized Kraft lignin beads
Kraft lignin from black liquor wastes have been converted into epichlorohydrin-crosslinked beads by inverse suspension polymerization. A careful control of the different parameters allowed the preparation of spherical beads with a relatively narrow diameter size distribution. The obtained beads, wit...
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Veröffentlicht in: | Journal of applied polymer science 2010-04, Vol.116 (2), p.1184-1189 |
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container_title | Journal of applied polymer science |
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creator | Saidane, Dorra Barbe, Jean-Christophe Birot, Marc Deleuze, Hervé |
description | Kraft lignin from black liquor wastes have been converted into epichlorohydrin-crosslinked beads by inverse suspension polymerization. A careful control of the different parameters allowed the preparation of spherical beads with a relatively narrow diameter size distribution. The obtained beads, without permanent porosity, swell well in hydroalcoholic media. Grafting of the sulfonylhydrazine moiety using a two-step route was further performed to apply them to carbonyl compounds scavenging. |
doi_str_mv | 10.1002/app.31659 |
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A careful control of the different parameters allowed the preparation of spherical beads with a relatively narrow diameter size distribution. The obtained beads, without permanent porosity, swell well in hydroalcoholic media. Grafting of the sulfonylhydrazine moiety using a two-step route was further performed to apply them to carbonyl compounds scavenging.</description><identifier>ISSN: 0021-8995</identifier><identifier>ISSN: 1097-4628</identifier><identifier>EISSN: 1097-4628</identifier><identifier>DOI: 10.1002/app.31659</identifier><identifier>CODEN: JAPNAB</identifier><language>eng</language><publisher>Hoboken: Wiley Subscription Services, Inc., A Wiley Company</publisher><subject>Applied sciences ; Beads ; Black liquor ; Carbonyl compounds ; Chemical and Process Engineering ; Engineering Sciences ; Exact sciences and technology ; Food engineering ; functionalization of polymers ; Inverse ; inverse suspension polymerization ; Kraft lignin ; Life Sciences ; Lignin and derivatives ; Natural polymers ; Physicochemistry of polymers ; Porosity ; Reproduction ; Scavenging ; Suspension polymerization ; swelling ; waste ; Wastes</subject><ispartof>Journal of applied polymer science, 2010-04, Vol.116 (2), p.1184-1189</ispartof><rights>Copyright © 2009 Wiley Periodicals, Inc.</rights><rights>2015 INIST-CNRS</rights><rights>Distributed under a Creative Commons Attribution 4.0 International License</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c5679-9a5b62418f4ac7ca47b236d17648bf1edf04c7b933db6ad6d0fd90f3bedd75713</citedby><cites>FETCH-LOGICAL-c5679-9a5b62418f4ac7ca47b236d17648bf1edf04c7b933db6ad6d0fd90f3bedd75713</cites><orcidid>0000-0002-5626-8212</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1002%2Fapp.31659$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1002%2Fapp.31659$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>230,314,776,780,881,1411,27901,27902,45550,45551</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=22428317$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://hal.inrae.fr/hal-02660924$$DView record in HAL$$Hfree_for_read</backlink></links><search><creatorcontrib>Saidane, Dorra</creatorcontrib><creatorcontrib>Barbe, Jean-Christophe</creatorcontrib><creatorcontrib>Birot, Marc</creatorcontrib><creatorcontrib>Deleuze, Hervé</creatorcontrib><title>Preparation of functionalized Kraft lignin beads</title><title>Journal of applied polymer science</title><addtitle>J. Appl. Polym. Sci</addtitle><description>Kraft lignin from black liquor wastes have been converted into epichlorohydrin-crosslinked beads by inverse suspension polymerization. A careful control of the different parameters allowed the preparation of spherical beads with a relatively narrow diameter size distribution. The obtained beads, without permanent porosity, swell well in hydroalcoholic media. Grafting of the sulfonylhydrazine moiety using a two-step route was further performed to apply them to carbonyl compounds scavenging.</description><subject>Applied sciences</subject><subject>Beads</subject><subject>Black liquor</subject><subject>Carbonyl compounds</subject><subject>Chemical and Process Engineering</subject><subject>Engineering Sciences</subject><subject>Exact sciences and technology</subject><subject>Food engineering</subject><subject>functionalization of polymers</subject><subject>Inverse</subject><subject>inverse suspension polymerization</subject><subject>Kraft lignin</subject><subject>Life Sciences</subject><subject>Lignin and derivatives</subject><subject>Natural polymers</subject><subject>Physicochemistry of polymers</subject><subject>Porosity</subject><subject>Reproduction</subject><subject>Scavenging</subject><subject>Suspension polymerization</subject><subject>swelling</subject><subject>waste</subject><subject>Wastes</subject><issn>0021-8995</issn><issn>1097-4628</issn><issn>1097-4628</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2010</creationdate><recordtype>article</recordtype><recordid>eNp9kEtv1DAUhS1EJYaWBb-AbBBlkfbaTvxYjlpoESMYKFUlNtaNH8WQJsGeAcqvJyFlWMHKlv2dc889hDymcEQB2DEOwxGnotb3yIKClmUlmLpPFuMfLZXW9QPyMOfPAJTWIBYE1skPmHAT-67oQxG2nZ3u2Maf3hWvE4ZN0cbrLnZF49HlA7IXsM3-0d25Ty5fvvhwcl6u3p69OlmuSlsLqUuNdSNYRVWo0EqLlWwYF45KUakmUO8CVFY2mnPXCHTCQXAaAm-8c7KWlO-T57PvJ2zNkOINplvTYzTny5WZ3oAJAZpV3yb22cwOqf-69XljbmK2vm2x8_02G6UFlUoKNZKH_yWpGEcDSA5_A9jU55x82KWgYKauzdi1-d31yD69s8VssQ0JOxvzTsBYxRSncuSOZ-57bP3tvw3Ncr3-41zOipg3_sdOgemLEZLL2ly9OTNXpxfvxMf3p2Za8MnMB-wNXqcxxeUFg3EpKnXNFee_AM6oo6I</recordid><startdate>20100415</startdate><enddate>20100415</enddate><creator>Saidane, Dorra</creator><creator>Barbe, Jean-Christophe</creator><creator>Birot, Marc</creator><creator>Deleuze, Hervé</creator><general>Wiley Subscription Services, Inc., A Wiley Company</general><general>Wiley</general><scope>FBQ</scope><scope>BSCLL</scope><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8FD</scope><scope>JG9</scope><scope>1XC</scope><orcidid>https://orcid.org/0000-0002-5626-8212</orcidid></search><sort><creationdate>20100415</creationdate><title>Preparation of functionalized Kraft lignin beads</title><author>Saidane, Dorra ; Barbe, Jean-Christophe ; Birot, Marc ; Deleuze, Hervé</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c5679-9a5b62418f4ac7ca47b236d17648bf1edf04c7b933db6ad6d0fd90f3bedd75713</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2010</creationdate><topic>Applied sciences</topic><topic>Beads</topic><topic>Black liquor</topic><topic>Carbonyl compounds</topic><topic>Chemical and Process Engineering</topic><topic>Engineering Sciences</topic><topic>Exact sciences and technology</topic><topic>Food engineering</topic><topic>functionalization of polymers</topic><topic>Inverse</topic><topic>inverse suspension polymerization</topic><topic>Kraft lignin</topic><topic>Life Sciences</topic><topic>Lignin and derivatives</topic><topic>Natural polymers</topic><topic>Physicochemistry of polymers</topic><topic>Porosity</topic><topic>Reproduction</topic><topic>Scavenging</topic><topic>Suspension polymerization</topic><topic>swelling</topic><topic>waste</topic><topic>Wastes</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Saidane, Dorra</creatorcontrib><creatorcontrib>Barbe, Jean-Christophe</creatorcontrib><creatorcontrib>Birot, Marc</creatorcontrib><creatorcontrib>Deleuze, Hervé</creatorcontrib><collection>AGRIS</collection><collection>Istex</collection><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Hyper Article en Ligne (HAL)</collection><jtitle>Journal of applied polymer science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Saidane, Dorra</au><au>Barbe, Jean-Christophe</au><au>Birot, Marc</au><au>Deleuze, Hervé</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Preparation of functionalized Kraft lignin beads</atitle><jtitle>Journal of applied polymer science</jtitle><addtitle>J. Appl. Polym. Sci</addtitle><date>2010-04-15</date><risdate>2010</risdate><volume>116</volume><issue>2</issue><spage>1184</spage><epage>1189</epage><pages>1184-1189</pages><issn>0021-8995</issn><issn>1097-4628</issn><eissn>1097-4628</eissn><coden>JAPNAB</coden><abstract>Kraft lignin from black liquor wastes have been converted into epichlorohydrin-crosslinked beads by inverse suspension polymerization. A careful control of the different parameters allowed the preparation of spherical beads with a relatively narrow diameter size distribution. The obtained beads, without permanent porosity, swell well in hydroalcoholic media. Grafting of the sulfonylhydrazine moiety using a two-step route was further performed to apply them to carbonyl compounds scavenging.</abstract><cop>Hoboken</cop><pub>Wiley Subscription Services, Inc., A Wiley Company</pub><doi>10.1002/app.31659</doi><tpages>6</tpages><orcidid>https://orcid.org/0000-0002-5626-8212</orcidid></addata></record> |
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subjects | Applied sciences Beads Black liquor Carbonyl compounds Chemical and Process Engineering Engineering Sciences Exact sciences and technology Food engineering functionalization of polymers Inverse inverse suspension polymerization Kraft lignin Life Sciences Lignin and derivatives Natural polymers Physicochemistry of polymers Porosity Reproduction Scavenging Suspension polymerization swelling waste Wastes |
title | Preparation of functionalized Kraft lignin beads |
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