Laboratory intercomparison study for the analysis of nonylphenol and octylphenol in river water
In support of the implementation of the European Union (EU) Water Framework Directive (WFD), the European Commission (EC) Joint Research Centre (JRC) organized a laboratory and sampling intercomparison study for the chemical monitoring of polyaromatic hydrocarbons (PAHs), polybrominated diphenyl eth...
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| Veröffentlicht in: | TrAC, Trends in analytical chemistry (Regular ed.) Trends in analytical chemistry (Regular ed.), 2008, Vol.27 (1), p.89-95 |
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| creator | Loos, R. Wollgast, J. Castro-Jiménez, J. Mariani, G. Huber, T. Locoro, G. Hanke, G. Umlauf, G. Bidoglio, G. Hohenblum, P. Moche, W. Weiss, S. Schmid, H. Leiendecker, F. Ternes, T. Ortega, A. Navarro Hildebrandt, A. Barceló, D. Lepom, P. Dimitrova, I. Nitcheva, O. Polesello, S. Valsecchi, S. Boutrup, S. Sortkjaer, O. de Boer, R. Staeb, J. |
| description | In support of the implementation of the European Union (EU) Water Framework Directive (WFD), the European Commission (EC) Joint Research Centre (JRC) organized a laboratory and sampling intercomparison study for the chemical monitoring of polyaromatic hydrocarbons (PAHs), polybrominated diphenyl ethers (PBDEs), and nonylphenol and octylphenol (NP/OP), priority substances of the WFD, in river water. EU Member State laboratories were invited to analyze a standard solution with unknown concentration levels and a river-water extract, as well as a real water sample from the River Po (Italy). For the standard solution and the river-water extract, good agreement was achieved for five laboratories. Triple-quadrupole liquid chromatography with tandem mass spectrometry (LC-MS
2) and gas chromatography with MS (GC-MS) with or without derivatization proved to be comparable methods for the analysis of NP and OP. Fluorescence detection can also be used to analyze NP and OP, but it is less specific. The results of the River Po water sample showed that some laboratories have problems in analyzing NP at concentration levels below 100 ng/L due to contamination of laboratory blanks. Plastics materials should not be used during extraction and sample preparation. |
| doi_str_mv | 10.1016/j.trac.2007.10.011 |
| format | Article |
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2) and gas chromatography with MS (GC-MS) with or without derivatization proved to be comparable methods for the analysis of NP and OP. Fluorescence detection can also be used to analyze NP and OP, but it is less specific. The results of the River Po water sample showed that some laboratories have problems in analyzing NP at concentration levels below 100 ng/L due to contamination of laboratory blanks. Plastics materials should not be used during extraction and sample preparation.</description><identifier>ISSN: 0165-9936</identifier><identifier>EISSN: 1879-3142</identifier><identifier>EISSN: 0165-9936</identifier><identifier>DOI: 10.1016/j.trac.2007.10.011</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>Analytical chemistry ; Chemical Sciences ; Chemistry ; Chromatographic methods and physical methods associated with chromatography ; Environmental Sciences ; Exact sciences and technology ; Gas chromatographic methods ; Laboratory intercomparison ; Nonylphenol ; Octylphenol ; Other chromatographic methods ; Priority substance ; Proficiency testing ; QA/QC ; Quality assurance ; Quality control ; Sampling intercomparison ; Spectrometric and optical methods ; Water Framework Directive</subject><ispartof>TrAC, Trends in analytical chemistry (Regular ed.), 2008, Vol.27 (1), p.89-95</ispartof><rights>2007 Elsevier Ltd</rights><rights>2008 INIST-CNRS</rights><rights>Distributed under a Creative Commons Attribution 4.0 International License</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c364t-4e16d94e7b7f8b347ddce9101c592823b6e00ec23aca7beb1df3592ab3c1c11f3</citedby><cites>FETCH-LOGICAL-c364t-4e16d94e7b7f8b347ddce9101c592823b6e00ec23aca7beb1df3592ab3c1c11f3</cites><orcidid>0000-0001-8456-3932</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.sciencedirect.com/science/article/pii/S0165993607002373$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>230,314,776,780,881,3537,4010,27900,27901,27902,65306</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=20136753$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://hal.science/hal-02138526$$DView record in HAL$$Hfree_for_read</backlink></links><search><creatorcontrib>Loos, R.</creatorcontrib><creatorcontrib>Wollgast, J.</creatorcontrib><creatorcontrib>Castro-Jiménez, J.</creatorcontrib><creatorcontrib>Mariani, G.</creatorcontrib><creatorcontrib>Huber, T.</creatorcontrib><creatorcontrib>Locoro, G.</creatorcontrib><creatorcontrib>Hanke, G.</creatorcontrib><creatorcontrib>Umlauf, G.</creatorcontrib><creatorcontrib>Bidoglio, G.</creatorcontrib><creatorcontrib>Hohenblum, P.</creatorcontrib><creatorcontrib>Moche, W.</creatorcontrib><creatorcontrib>Weiss, S.</creatorcontrib><creatorcontrib>Schmid, H.</creatorcontrib><creatorcontrib>Leiendecker, F.</creatorcontrib><creatorcontrib>Ternes, T.</creatorcontrib><creatorcontrib>Ortega, A. Navarro</creatorcontrib><creatorcontrib>Hildebrandt, A.</creatorcontrib><creatorcontrib>Barceló, D.</creatorcontrib><creatorcontrib>Lepom, P.</creatorcontrib><creatorcontrib>Dimitrova, I.</creatorcontrib><creatorcontrib>Nitcheva, O.</creatorcontrib><creatorcontrib>Polesello, S.</creatorcontrib><creatorcontrib>Valsecchi, S.</creatorcontrib><creatorcontrib>Boutrup, S.</creatorcontrib><creatorcontrib>Sortkjaer, O.</creatorcontrib><creatorcontrib>de Boer, R.</creatorcontrib><creatorcontrib>Staeb, J.</creatorcontrib><title>Laboratory intercomparison study for the analysis of nonylphenol and octylphenol in river water</title><title>TrAC, Trends in analytical chemistry (Regular ed.)</title><description>In support of the implementation of the European Union (EU) Water Framework Directive (WFD), the European Commission (EC) Joint Research Centre (JRC) organized a laboratory and sampling intercomparison study for the chemical monitoring of polyaromatic hydrocarbons (PAHs), polybrominated diphenyl ethers (PBDEs), and nonylphenol and octylphenol (NP/OP), priority substances of the WFD, in river water. EU Member State laboratories were invited to analyze a standard solution with unknown concentration levels and a river-water extract, as well as a real water sample from the River Po (Italy). For the standard solution and the river-water extract, good agreement was achieved for five laboratories. Triple-quadrupole liquid chromatography with tandem mass spectrometry (LC-MS
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EU Member State laboratories were invited to analyze a standard solution with unknown concentration levels and a river-water extract, as well as a real water sample from the River Po (Italy). For the standard solution and the river-water extract, good agreement was achieved for five laboratories. Triple-quadrupole liquid chromatography with tandem mass spectrometry (LC-MS
2) and gas chromatography with MS (GC-MS) with or without derivatization proved to be comparable methods for the analysis of NP and OP. Fluorescence detection can also be used to analyze NP and OP, but it is less specific. The results of the River Po water sample showed that some laboratories have problems in analyzing NP at concentration levels below 100 ng/L due to contamination of laboratory blanks. Plastics materials should not be used during extraction and sample preparation.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><doi>10.1016/j.trac.2007.10.011</doi><tpages>7</tpages><orcidid>https://orcid.org/0000-0001-8456-3932</orcidid></addata></record> |
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| subjects | Analytical chemistry Chemical Sciences Chemistry Chromatographic methods and physical methods associated with chromatography Environmental Sciences Exact sciences and technology Gas chromatographic methods Laboratory intercomparison Nonylphenol Octylphenol Other chromatographic methods Priority substance Proficiency testing QA/QC Quality assurance Quality control Sampling intercomparison Spectrometric and optical methods Water Framework Directive |
| title | Laboratory intercomparison study for the analysis of nonylphenol and octylphenol in river water |
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