Signal enhancement of J-HMQC experiments in solid-state NMR involving half-integer quadrupolar nuclei
We show that for half-integer quadrupolar nuclei, the manipulation of the satellite transitions can accelerate and enhance coherence transfer to other isotopes. This novel strategy is demonstrated to improve the sensitivity of (31)P-{(27)Al} J-HMQC experiments for a layered aluminophosphate Mu-4.
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Veröffentlicht in: | Chemical communications (Cambridge, England) England), 2013-01, Vol.49 (59), p.6653-6655 |
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container_title | Chemical communications (Cambridge, England) |
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creator | Wang, Qiang Trébosc, Julien Li, Yixuan Xu, Jun Hu, Bingwen Feng, Ningdong Chen, Qun Lafon, Oliver Amoureux, Jean-Paul Deng, Feng |
description | We show that for half-integer quadrupolar nuclei, the manipulation of the satellite transitions can accelerate and enhance coherence transfer to other isotopes. This novel strategy is demonstrated to improve the sensitivity of (31)P-{(27)Al} J-HMQC experiments for a layered aluminophosphate Mu-4. |
doi_str_mv | 10.1039/c3cc42961j |
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This novel strategy is demonstrated to improve the sensitivity of (31)P-{(27)Al} J-HMQC experiments for a layered aluminophosphate Mu-4.</description><identifier>ISSN: 1359-7345</identifier><identifier>EISSN: 1364-548X</identifier><identifier>DOI: 10.1039/c3cc42961j</identifier><identifier>PMID: 23770976</identifier><language>eng</language><publisher>England: Royal Society of Chemistry</publisher><subject>Aluminophosphates ; Chemical Sciences ; Coherence ; Communication satellites ; Isotopes ; Nuclear magnetic resonance ; Nuclei ; Satellites ; Strategy</subject><ispartof>Chemical communications (Cambridge, England), 2013-01, Vol.49 (59), p.6653-6655</ispartof><rights>Distributed under a Creative Commons Attribution 4.0 International License</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c354t-f9b544563ce0ce1d02075af1b2bccc4043ae4c7ac97972866fc9956e217020a73</citedby><cites>FETCH-LOGICAL-c354t-f9b544563ce0ce1d02075af1b2bccc4043ae4c7ac97972866fc9956e217020a73</cites><orcidid>0000-0002-9654-0268 ; 0000-0002-4034-855X ; 0000-0003-3772-6801</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>230,314,780,784,885,27922,27923</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/23770976$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink><backlink>$$Uhttps://hal.science/hal-02043754$$DView record in HAL$$Hfree_for_read</backlink></links><search><creatorcontrib>Wang, Qiang</creatorcontrib><creatorcontrib>Trébosc, Julien</creatorcontrib><creatorcontrib>Li, Yixuan</creatorcontrib><creatorcontrib>Xu, Jun</creatorcontrib><creatorcontrib>Hu, Bingwen</creatorcontrib><creatorcontrib>Feng, Ningdong</creatorcontrib><creatorcontrib>Chen, Qun</creatorcontrib><creatorcontrib>Lafon, Oliver</creatorcontrib><creatorcontrib>Amoureux, Jean-Paul</creatorcontrib><creatorcontrib>Deng, Feng</creatorcontrib><title>Signal enhancement of J-HMQC experiments in solid-state NMR involving half-integer quadrupolar nuclei</title><title>Chemical communications (Cambridge, England)</title><addtitle>Chem Commun (Camb)</addtitle><description>We show that for half-integer quadrupolar nuclei, the manipulation of the satellite transitions can accelerate and enhance coherence transfer to other isotopes. This novel strategy is demonstrated to improve the sensitivity of (31)P-{(27)Al} J-HMQC experiments for a layered aluminophosphate Mu-4.</description><subject>Aluminophosphates</subject><subject>Chemical Sciences</subject><subject>Coherence</subject><subject>Communication satellites</subject><subject>Isotopes</subject><subject>Nuclear magnetic resonance</subject><subject>Nuclei</subject><subject>Satellites</subject><subject>Strategy</subject><issn>1359-7345</issn><issn>1364-548X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2013</creationdate><recordtype>article</recordtype><recordid>eNqFkVtLAzEQhYMo1tuLP0DyqMJqsrk1j1LUKq3iDXxb0nS2RtJsu9kt-u_NUi-PzssMh4_hzByEDik5o4Tpc8us5bmW9H0D7VAmeSZ4_3Wzm4XOFOOih3ZjfCepqOhvo17OlCJayR0ET24WjMcQ3kywMIfQ4KrEt9lw_DDA8LGA2nVixC7gWHk3zWJjGsB348ckrSq_cmGG34wvMxcamEGNl62Z1u2i8qbGobUe3D7aKo2PcPDd99DL1eXzYJiN7q9vBhejzDLBm6zUE8G5kMwCsUCnJCdKmJJO8olNJxLODHCrjNVKq7wvZWm1FhJyqhJqFNtDJ-u9yU-xSM5N_VlUxhXDi1HRaQnjTAm-ook9XrOLulq2EJti7qIF702Aqo0FlSr9T0lB_keZyqWWTHYOTteorasYayh_bVBSdGkVf2kl-Oh7bzuZw_QX_YmHfQGYfo7S</recordid><startdate>20130101</startdate><enddate>20130101</enddate><creator>Wang, Qiang</creator><creator>Trébosc, Julien</creator><creator>Li, Yixuan</creator><creator>Xu, Jun</creator><creator>Hu, Bingwen</creator><creator>Feng, Ningdong</creator><creator>Chen, Qun</creator><creator>Lafon, Oliver</creator><creator>Amoureux, Jean-Paul</creator><creator>Deng, Feng</creator><general>Royal Society of Chemistry</general><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope><scope>7SP</scope><scope>7U5</scope><scope>8FD</scope><scope>L7M</scope><scope>1XC</scope><orcidid>https://orcid.org/0000-0002-9654-0268</orcidid><orcidid>https://orcid.org/0000-0002-4034-855X</orcidid><orcidid>https://orcid.org/0000-0003-3772-6801</orcidid></search><sort><creationdate>20130101</creationdate><title>Signal enhancement of J-HMQC experiments in solid-state NMR involving half-integer quadrupolar nuclei</title><author>Wang, Qiang ; Trébosc, Julien ; Li, Yixuan ; Xu, Jun ; Hu, Bingwen ; Feng, Ningdong ; Chen, Qun ; Lafon, Oliver ; Amoureux, Jean-Paul ; Deng, Feng</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c354t-f9b544563ce0ce1d02075af1b2bccc4043ae4c7ac97972866fc9956e217020a73</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2013</creationdate><topic>Aluminophosphates</topic><topic>Chemical Sciences</topic><topic>Coherence</topic><topic>Communication satellites</topic><topic>Isotopes</topic><topic>Nuclear magnetic resonance</topic><topic>Nuclei</topic><topic>Satellites</topic><topic>Strategy</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Wang, Qiang</creatorcontrib><creatorcontrib>Trébosc, Julien</creatorcontrib><creatorcontrib>Li, Yixuan</creatorcontrib><creatorcontrib>Xu, Jun</creatorcontrib><creatorcontrib>Hu, Bingwen</creatorcontrib><creatorcontrib>Feng, Ningdong</creatorcontrib><creatorcontrib>Chen, Qun</creatorcontrib><creatorcontrib>Lafon, Oliver</creatorcontrib><creatorcontrib>Amoureux, Jean-Paul</creatorcontrib><creatorcontrib>Deng, Feng</creatorcontrib><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><collection>Electronics & Communications Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>Hyper Article en Ligne (HAL)</collection><jtitle>Chemical communications (Cambridge, England)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Wang, Qiang</au><au>Trébosc, Julien</au><au>Li, Yixuan</au><au>Xu, Jun</au><au>Hu, Bingwen</au><au>Feng, Ningdong</au><au>Chen, Qun</au><au>Lafon, Oliver</au><au>Amoureux, Jean-Paul</au><au>Deng, Feng</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Signal enhancement of J-HMQC experiments in solid-state NMR involving half-integer quadrupolar nuclei</atitle><jtitle>Chemical communications (Cambridge, England)</jtitle><addtitle>Chem Commun (Camb)</addtitle><date>2013-01-01</date><risdate>2013</risdate><volume>49</volume><issue>59</issue><spage>6653</spage><epage>6655</epage><pages>6653-6655</pages><issn>1359-7345</issn><eissn>1364-548X</eissn><abstract>We show that for half-integer quadrupolar nuclei, the manipulation of the satellite transitions can accelerate and enhance coherence transfer to other isotopes. 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issn | 1359-7345 1364-548X |
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source | Royal Society Of Chemistry Journals 2008-; Alma/SFX Local Collection |
subjects | Aluminophosphates Chemical Sciences Coherence Communication satellites Isotopes Nuclear magnetic resonance Nuclei Satellites Strategy |
title | Signal enhancement of J-HMQC experiments in solid-state NMR involving half-integer quadrupolar nuclei |
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