High-yield aqueous synthesis of multi-branched iron oxide core–gold shell nanoparticles: SERS substrate for immobilization and magnetic separation of bacteria
The high product yield of multi-branched core–shell Fe 3− x O 4 @Au magnetic nanoparticles was synthesized used as magnetic separation platform and surface-enhanced Raman scattering (SERS) substrates. The multi-branched magnetic nanoparticles were prepared by a seed-mediated growth approach using ma...
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| Veröffentlicht in: | Journal of nanoparticle research : an interdisciplinary forum for nanoscale science and technology 2014-10, Vol.16 (10), p.1, Article 2624 |
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| creator | Tamer, Ugur Onay, Aykut Ciftci, Hakan Bozkurt, Akif Göktuğ Cetin, Demet Suludere, Zekiye Hakkı Boyacı, İsmail Daniel, Philippe Lagarde, Fabienne Yaacoub, Nader Greneche, Jean-Marc |
| description | The high product yield of multi-branched core–shell Fe
3−
x
O
4
@Au magnetic nanoparticles was synthesized used as magnetic separation platform and surface-enhanced Raman scattering (SERS) substrates. The multi-branched magnetic nanoparticles were prepared by a seed-mediated growth approach using magnetic gold nanospheres as the seeds and subsequent reduction of metal salt with ascorbic acid in the presence of a stabilizing agent chitosan biopolymer and silver ions. The anisotropic growth of nanoparticles was observed in the presence of chitosan polymer matrix resulting in multi-branched nanoparticles with a diameter over 100 nm, and silver ions also play a crucial role on the growth of multi-branched nanoparticles. We propose the mechanism of the formation of multi-branched nanoparticles while the properties of nanoparticles embedded in chitosan matrix are discussed. The surface morphology of nanoparticles was characterized with transmission electron microscopy, scanning electron microscopy, ultraviolet visible spectroscopy (UV–Vis), X-ray diffraction, and fourier transform infrared spectroscopy and
57
Fe Mössbauer spectrometry. Additionally, the magnetic properties of the nanoparticles were also examined. We also demonstrated that the synthesized Fe
3−
x
O
4
@Au multi-branched nanoparticle is capable of targeted separation of pathogens from matrix and sensing as SERS substrates. |
| doi_str_mv | 10.1007/s11051-014-2624-7 |
| format | Article |
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3−
x
O
4
@Au magnetic nanoparticles was synthesized used as magnetic separation platform and surface-enhanced Raman scattering (SERS) substrates. The multi-branched magnetic nanoparticles were prepared by a seed-mediated growth approach using magnetic gold nanospheres as the seeds and subsequent reduction of metal salt with ascorbic acid in the presence of a stabilizing agent chitosan biopolymer and silver ions. The anisotropic growth of nanoparticles was observed in the presence of chitosan polymer matrix resulting in multi-branched nanoparticles with a diameter over 100 nm, and silver ions also play a crucial role on the growth of multi-branched nanoparticles. We propose the mechanism of the formation of multi-branched nanoparticles while the properties of nanoparticles embedded in chitosan matrix are discussed. The surface morphology of nanoparticles was characterized with transmission electron microscopy, scanning electron microscopy, ultraviolet visible spectroscopy (UV–Vis), X-ray diffraction, and fourier transform infrared spectroscopy and
57
Fe Mössbauer spectrometry. Additionally, the magnetic properties of the nanoparticles were also examined. We also demonstrated that the synthesized Fe
3−
x
O
4
@Au multi-branched nanoparticle is capable of targeted separation of pathogens from matrix and sensing as SERS substrates.</description><identifier>ISSN: 1388-0764</identifier><identifier>EISSN: 1572-896X</identifier><identifier>DOI: 10.1007/s11051-014-2624-7</identifier><language>eng</language><publisher>Dordrecht: Springer Netherlands</publisher><subject>Biopolymers ; Characterization and Evaluation of Materials ; Chemical Sciences ; Chemistry and Materials Science ; Condensed matter: electronic structure, electrical, magnetic, and optical properties ; Condensed matter: structure, mechanical and thermal properties ; Cross-disciplinary physics: materials science; rheology ; Exact sciences and technology ; Fourier transforms ; Infrared spectroscopy ; Inorganic Chemistry ; Ions ; Iron oxides ; Lasers ; Low-dimensional structures (superlattices, quantum well structures, multilayers): structure, and nonelectronic properties ; Magnetic properties ; Magnetic properties and materials ; Magnetic properties of nanostructures ; Materials Science ; Methods of nanofabrication ; Nanoparticles ; Nanotechnology ; Optical Devices ; Optics ; Photonics ; Physical Chemistry ; Physics ; Polymers ; Research Paper ; Silver ; Small particles and nanoscale materials ; Spectrometry ; Studies of specific magnetic materials ; Surfaces and interfaces; thin films and whiskers (structure and nonelectronic properties) ; X-ray diffraction</subject><ispartof>Journal of nanoparticle research : an interdisciplinary forum for nanoscale science and technology, 2014-10, Vol.16 (10), p.1, Article 2624</ispartof><rights>Springer Science+Business Media Dordrecht 2014</rights><rights>2015 INIST-CNRS</rights><rights>Distributed under a Creative Commons Attribution 4.0 International License</rights><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c380t-e9818a48ef297f298898a592cdfe59223661721119449b9fa7d622710a82b07b3</citedby><cites>FETCH-LOGICAL-c380t-e9818a48ef297f298898a592cdfe59223661721119449b9fa7d622710a82b07b3</cites><orcidid>0000-0003-0292-5253 ; 0000-0002-4015-4376 ; 0000-0002-5583-1165 ; 0000-0001-7309-8633</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s11051-014-2624-7$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s11051-014-2624-7$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>230,314,778,782,883,27911,27912,41475,42544,51306</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=28888639$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://hal.science/hal-01974827$$DView record in HAL$$Hfree_for_read</backlink></links><search><creatorcontrib>Tamer, Ugur</creatorcontrib><creatorcontrib>Onay, Aykut</creatorcontrib><creatorcontrib>Ciftci, Hakan</creatorcontrib><creatorcontrib>Bozkurt, Akif Göktuğ</creatorcontrib><creatorcontrib>Cetin, Demet</creatorcontrib><creatorcontrib>Suludere, Zekiye</creatorcontrib><creatorcontrib>Hakkı Boyacı, İsmail</creatorcontrib><creatorcontrib>Daniel, Philippe</creatorcontrib><creatorcontrib>Lagarde, Fabienne</creatorcontrib><creatorcontrib>Yaacoub, Nader</creatorcontrib><creatorcontrib>Greneche, Jean-Marc</creatorcontrib><title>High-yield aqueous synthesis of multi-branched iron oxide core–gold shell nanoparticles: SERS substrate for immobilization and magnetic separation of bacteria</title><title>Journal of nanoparticle research : an interdisciplinary forum for nanoscale science and technology</title><addtitle>J Nanopart Res</addtitle><description>The high product yield of multi-branched core–shell Fe
3−
x
O
4
@Au magnetic nanoparticles was synthesized used as magnetic separation platform and surface-enhanced Raman scattering (SERS) substrates. The multi-branched magnetic nanoparticles were prepared by a seed-mediated growth approach using magnetic gold nanospheres as the seeds and subsequent reduction of metal salt with ascorbic acid in the presence of a stabilizing agent chitosan biopolymer and silver ions. The anisotropic growth of nanoparticles was observed in the presence of chitosan polymer matrix resulting in multi-branched nanoparticles with a diameter over 100 nm, and silver ions also play a crucial role on the growth of multi-branched nanoparticles. We propose the mechanism of the formation of multi-branched nanoparticles while the properties of nanoparticles embedded in chitosan matrix are discussed. The surface morphology of nanoparticles was characterized with transmission electron microscopy, scanning electron microscopy, ultraviolet visible spectroscopy (UV–Vis), X-ray diffraction, and fourier transform infrared spectroscopy and
57
Fe Mössbauer spectrometry. Additionally, the magnetic properties of the nanoparticles were also examined. We also demonstrated that the synthesized Fe
3−
x
O
4
@Au multi-branched nanoparticle is capable of targeted separation of pathogens from matrix and sensing as SERS substrates.</description><subject>Biopolymers</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemical Sciences</subject><subject>Chemistry and Materials Science</subject><subject>Condensed matter: electronic structure, electrical, magnetic, and optical properties</subject><subject>Condensed matter: structure, mechanical and thermal properties</subject><subject>Cross-disciplinary physics: materials science; rheology</subject><subject>Exact sciences and technology</subject><subject>Fourier transforms</subject><subject>Infrared spectroscopy</subject><subject>Inorganic Chemistry</subject><subject>Ions</subject><subject>Iron oxides</subject><subject>Lasers</subject><subject>Low-dimensional structures (superlattices, quantum well structures, multilayers): structure, and nonelectronic properties</subject><subject>Magnetic properties</subject><subject>Magnetic properties and materials</subject><subject>Magnetic properties of nanostructures</subject><subject>Materials Science</subject><subject>Methods of nanofabrication</subject><subject>Nanoparticles</subject><subject>Nanotechnology</subject><subject>Optical Devices</subject><subject>Optics</subject><subject>Photonics</subject><subject>Physical Chemistry</subject><subject>Physics</subject><subject>Polymers</subject><subject>Research Paper</subject><subject>Silver</subject><subject>Small particles and nanoscale materials</subject><subject>Spectrometry</subject><subject>Studies of specific magnetic materials</subject><subject>Surfaces and interfaces; thin films and whiskers (structure and nonelectronic properties)</subject><subject>X-ray 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aqueous synthesis of multi-branched iron oxide core–gold shell nanoparticles: SERS substrate for immobilization and magnetic separation of bacteria</title><author>Tamer, Ugur ; Onay, Aykut ; Ciftci, Hakan ; Bozkurt, Akif Göktuğ ; Cetin, Demet ; Suludere, Zekiye ; Hakkı Boyacı, İsmail ; Daniel, Philippe ; Lagarde, Fabienne ; Yaacoub, Nader ; Greneche, Jean-Marc</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c380t-e9818a48ef297f298898a592cdfe59223661721119449b9fa7d622710a82b07b3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2014</creationdate><topic>Biopolymers</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemical Sciences</topic><topic>Chemistry and Materials Science</topic><topic>Condensed matter: electronic structure, electrical, magnetic, and optical properties</topic><topic>Condensed matter: structure, mechanical and thermal properties</topic><topic>Cross-disciplinary physics: materials science; rheology</topic><topic>Exact sciences and technology</topic><topic>Fourier transforms</topic><topic>Infrared spectroscopy</topic><topic>Inorganic Chemistry</topic><topic>Ions</topic><topic>Iron oxides</topic><topic>Lasers</topic><topic>Low-dimensional structures (superlattices, quantum well structures, multilayers): structure, and nonelectronic properties</topic><topic>Magnetic properties</topic><topic>Magnetic properties and materials</topic><topic>Magnetic properties of nanostructures</topic><topic>Materials Science</topic><topic>Methods of nanofabrication</topic><topic>Nanoparticles</topic><topic>Nanotechnology</topic><topic>Optical Devices</topic><topic>Optics</topic><topic>Photonics</topic><topic>Physical Chemistry</topic><topic>Physics</topic><topic>Polymers</topic><topic>Research Paper</topic><topic>Silver</topic><topic>Small particles and nanoscale materials</topic><topic>Spectrometry</topic><topic>Studies 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Res</stitle><date>2014-10-01</date><risdate>2014</risdate><volume>16</volume><issue>10</issue><spage>1</spage><pages>1-</pages><artnum>2624</artnum><issn>1388-0764</issn><eissn>1572-896X</eissn><abstract>The high product yield of multi-branched core–shell Fe
3−
x
O
4
@Au magnetic nanoparticles was synthesized used as magnetic separation platform and surface-enhanced Raman scattering (SERS) substrates. The multi-branched magnetic nanoparticles were prepared by a seed-mediated growth approach using magnetic gold nanospheres as the seeds and subsequent reduction of metal salt with ascorbic acid in the presence of a stabilizing agent chitosan biopolymer and silver ions. The anisotropic growth of nanoparticles was observed in the presence of chitosan polymer matrix resulting in multi-branched nanoparticles with a diameter over 100 nm, and silver ions also play a crucial role on the growth of multi-branched nanoparticles. We propose the mechanism of the formation of multi-branched nanoparticles while the properties of nanoparticles embedded in chitosan matrix are discussed. The surface morphology of nanoparticles was characterized with transmission electron microscopy, scanning electron microscopy, ultraviolet visible spectroscopy (UV–Vis), X-ray diffraction, and fourier transform infrared spectroscopy and
57
Fe Mössbauer spectrometry. Additionally, the magnetic properties of the nanoparticles were also examined. We also demonstrated that the synthesized Fe
3−
x
O
4
@Au multi-branched nanoparticle is capable of targeted separation of pathogens from matrix and sensing as SERS substrates.</abstract><cop>Dordrecht</cop><pub>Springer Netherlands</pub><doi>10.1007/s11051-014-2624-7</doi><orcidid>https://orcid.org/0000-0003-0292-5253</orcidid><orcidid>https://orcid.org/0000-0002-4015-4376</orcidid><orcidid>https://orcid.org/0000-0002-5583-1165</orcidid><orcidid>https://orcid.org/0000-0001-7309-8633</orcidid></addata></record> |
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| identifier | ISSN: 1388-0764 |
| ispartof | Journal of nanoparticle research : an interdisciplinary forum for nanoscale science and technology, 2014-10, Vol.16 (10), p.1, Article 2624 |
| issn | 1388-0764 1572-896X |
| language | eng |
| recordid | cdi_hal_primary_oai_HAL_hal_01974827v1 |
| source | Springer Nature - Complete Springer Journals |
| subjects | Biopolymers Characterization and Evaluation of Materials Chemical Sciences Chemistry and Materials Science Condensed matter: electronic structure, electrical, magnetic, and optical properties Condensed matter: structure, mechanical and thermal properties Cross-disciplinary physics: materials science rheology Exact sciences and technology Fourier transforms Infrared spectroscopy Inorganic Chemistry Ions Iron oxides Lasers Low-dimensional structures (superlattices, quantum well structures, multilayers): structure, and nonelectronic properties Magnetic properties Magnetic properties and materials Magnetic properties of nanostructures Materials Science Methods of nanofabrication Nanoparticles Nanotechnology Optical Devices Optics Photonics Physical Chemistry Physics Polymers Research Paper Silver Small particles and nanoscale materials Spectrometry Studies of specific magnetic materials Surfaces and interfaces thin films and whiskers (structure and nonelectronic properties) X-ray diffraction |
| title | High-yield aqueous synthesis of multi-branched iron oxide core–gold shell nanoparticles: SERS substrate for immobilization and magnetic separation of bacteria |
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