Low temperature matrix synthesis by activated nitridation of a TiSi2 powder
This paper describes a new method to prepare a matrix for Ceramic Matrix Composites (CMC) at low temperatures from a solid/gas chemical reaction. Contrary to previous works, a TiSi2 powder is fully nitrided at 1100°C leading to the formation of Si3N4 and TiN phases while avoiding the presence of fre...
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| Veröffentlicht in: | Journal of the European Ceramic Society 2017-10, Vol.37 (13), p.3885-3889 |
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| container_issue | 13 |
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| container_title | Journal of the European Ceramic Society |
| container_volume | 37 |
| creator | Maillé, L. Le Petitcorps, Y. Roger, J. |
| description | This paper describes a new method to prepare a matrix for Ceramic Matrix Composites (CMC) at low temperatures from a solid/gas chemical reaction. Contrary to previous works, a TiSi2 powder is fully nitrided at 1100°C leading to the formation of Si3N4 and TiN phases while avoiding the presence of free silicon. This new result can be obtained by the addition of a chemical element promoting a full chemical conversion. In the present case, thermochemical computations led to select nickel (Ni) as this chemical element. |
| doi_str_mv | 10.1016/j.jeurceramsoc.2017.05.019 |
| format | Article |
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Contrary to previous works, a TiSi2 powder is fully nitrided at 1100°C leading to the formation of Si3N4 and TiN phases while avoiding the presence of free silicon. This new result can be obtained by the addition of a chemical element promoting a full chemical conversion. In the present case, thermochemical computations led to select nickel (Ni) as this chemical element.</description><subject>Ceramic matrix composites (CMC)</subject><subject>Chemical reactivity</subject><subject>Chemical Sciences</subject><subject>Material chemistry</subject><subject>Matrix</subject><subject>Nitridation</subject><issn>0955-2219</issn><issn>1873-619X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2017</creationdate><recordtype>article</recordtype><recordid>eNqNkEtLAzEUhYMoWB__IbhzMWMymcwk7kp9VBxwYQV3IU3u0AydpiRpa_-9Uyri0tWFc8_54ByEbijJKaHVXZd3sAkGgu6jN3lBaJ0TnhMqT9CIipplFZWfp2hEJOdZUVB5ji5i7MhgJFKO0GvjdzhBvx4QaRMA9zoF94XjfpUWEF3E8z3WJrmtTmDxyg1fq5PzK-xbrPHMvbsCr_3OQrhCZ61eRrj-uZfo4-lxNplmzdvzy2TcZIZxkbLKasHm5dxwQysrJS_NoBBuWU3qVnJWCWoJLUpuaspLxnirgRnBbMsKAZZdotsjd6GXah1cr8Neee3UdNyog0aoKEtGxZYO3vuj1wQfY4D2N0CJOkyoOvV3QnWYUBE-MOQQfjiGYWizdRBUNA5WBqwLYJKy3v0H8w3KhoFe</recordid><startdate>201710</startdate><enddate>201710</enddate><creator>Maillé, L.</creator><creator>Le Petitcorps, Y.</creator><creator>Roger, J.</creator><general>Elsevier Ltd</general><general>Elsevier</general><scope>AAYXX</scope><scope>CITATION</scope><scope>1XC</scope></search><sort><creationdate>201710</creationdate><title>Low temperature matrix synthesis by activated nitridation of a TiSi2 powder</title><author>Maillé, L. ; Le Petitcorps, Y. ; Roger, J.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c358t-6da83b4bc5c16d9954cda805d3707f953681d01245c7154335fae3c83df328ed3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2017</creationdate><topic>Ceramic matrix composites (CMC)</topic><topic>Chemical reactivity</topic><topic>Chemical Sciences</topic><topic>Material chemistry</topic><topic>Matrix</topic><topic>Nitridation</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Maillé, L.</creatorcontrib><creatorcontrib>Le Petitcorps, Y.</creatorcontrib><creatorcontrib>Roger, J.</creatorcontrib><collection>CrossRef</collection><collection>Hyper Article en Ligne (HAL)</collection><jtitle>Journal of the European Ceramic Society</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Maillé, L.</au><au>Le Petitcorps, Y.</au><au>Roger, J.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Low temperature matrix synthesis by activated nitridation of a TiSi2 powder</atitle><jtitle>Journal of the European Ceramic Society</jtitle><date>2017-10</date><risdate>2017</risdate><volume>37</volume><issue>13</issue><spage>3885</spage><epage>3889</epage><pages>3885-3889</pages><issn>0955-2219</issn><eissn>1873-619X</eissn><abstract>This paper describes a new method to prepare a matrix for Ceramic Matrix Composites (CMC) at low temperatures from a solid/gas chemical reaction. Contrary to previous works, a TiSi2 powder is fully nitrided at 1100°C leading to the formation of Si3N4 and TiN phases while avoiding the presence of free silicon. This new result can be obtained by the addition of a chemical element promoting a full chemical conversion. In the present case, thermochemical computations led to select nickel (Ni) as this chemical element.</abstract><pub>Elsevier Ltd</pub><doi>10.1016/j.jeurceramsoc.2017.05.019</doi><tpages>5</tpages></addata></record> |
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| ispartof | Journal of the European Ceramic Society, 2017-10, Vol.37 (13), p.3885-3889 |
| issn | 0955-2219 1873-619X |
| language | eng |
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| source | Elsevier ScienceDirect Journals |
| subjects | Ceramic matrix composites (CMC) Chemical reactivity Chemical Sciences Material chemistry Matrix Nitridation |
| title | Low temperature matrix synthesis by activated nitridation of a TiSi2 powder |
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