Wet‐Route Synthesis and Characterization of Yb:CaF 2 Optical Ceramics
This paper reports a new strainless fabrication method for ytterbium‐doped CaF 2 laser ceramics involving no drying step before green body casting. The nanoparticles were kept in aqueous solution until green body shaping. Centrifugation was used to obtain correct compactness of the green body before...
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| Veröffentlicht in: | Journal of the American Ceramic Society 2016-06, Vol.99 (6), p.1992-2000 |
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| container_end_page | 2000 |
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| container_issue | 6 |
| container_start_page | 1992 |
| container_title | Journal of the American Ceramic Society |
| container_volume | 99 |
| creator | Sarthou, Julia Aballéa, Pierre Patriarche, Gilles Serier‐Brault, Hélène Suganuma, Akiko Gredin, Patrick Mortier, Michel |
| description | This paper reports a new strainless fabrication method for ytterbium‐doped CaF
2
laser ceramics involving no drying step before green body casting. The nanoparticles were kept in aqueous solution until green body shaping. Centrifugation was used to obtain correct compactness of the green body before sintering. Characterizations were conducted at different steps of the fabrication process. No grain boundaries oxidation was observed in the sintered ceramics although the nanoparticles were permanently maintained in water until they were sintered. Finally, these ceramics are more homogeneous and have less light scattering defects (no porosity), and present improved optical properties when compared to ceramics obtained from dried nanopowders. |
| doi_str_mv | 10.1111/jace.14216 |
| format | Article |
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| issn | 0002-7820 1551-2916 |
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| source | Wiley Online Library All Journals |
| subjects | Condensed Matter Materials Science Physics |
| title | Wet‐Route Synthesis and Characterization of Yb:CaF 2 Optical Ceramics |
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