A new strategy to activate liquid crystal polymer samples for electroless copper deposition
ABSTRACT In order to activate the polymers for electroless copper deposition, an alternative way of sample preparation is demonstrated. The samples are prepared by incorporation of a small amount (
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| Veröffentlicht in: | Journal of applied polymer science 2017-01, Vol.134 (1), p.np-n/a |
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| container_title | Journal of applied polymer science |
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| creator | Atli, A. Simon, S. Cadete Santos Aires, F. J. Cardenas, L. Ehret, E. Lourdin, P. |
| description | ABSTRACT
In order to activate the polymers for electroless copper deposition, an alternative way of sample preparation is demonstrated. The samples are prepared by incorporation of a small amount ( |
| doi_str_mv | 10.1002/app.44397 |
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In order to activate the polymers for electroless copper deposition, an alternative way of sample preparation is demonstrated. The samples are prepared by incorporation of a small amount (<1 wt %) of palladium, nickel, or copper acetate into the molten Liquid Crystal Polymer (LCP) in a blender. Since the blending temperature is kept higher than the decomposition temperature of acetates, the acetates are thermally decomposed during blending, leading to the metallic Pd, Ni, or Cu which are used as activators for electroless deposition. After preparing the samples, electroless copper deposition is successfully realized. The influence of different acetates (Pd, Ni, or Cu acetates) on the deposition is investigated. The copper amount is higher and the deposition kinetics is faster on LCP samples with 0.15 wt % Pd and 0.4 wt % Ni than that with 0.4 wt % Cu. The deposited copper layers are uniform and oxide‐free. Moreover, the possibility to substitute expensive Pd activator by cheaper Ni or Cu is shown. © 2016 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2016, 133, 44397.</description><identifier>ISSN: 0021-8995</identifier><identifier>EISSN: 1097-4628</identifier><identifier>DOI: 10.1002/app.44397</identifier><identifier>CODEN: JAPNAB</identifier><language>eng</language><publisher>Hoboken: Wiley Subscription Services, Inc</publisher><subject>ACETATES ; Blending ; Catalysis ; Chemical Sciences ; coatings ; Copper ; COPPER ACETATE ; COPPER RESOURCES ; DEPOSITION ; Electroless plating ; Environment and Society ; Environmental Sciences ; interfaces ; kinetics ; Liquid crystal polymers ; liquid crystals ; Materials science ; Nickel ; Palladium ; PLATING ; POLYMERS ; spectroscopy ; surfaces</subject><ispartof>Journal of applied polymer science, 2017-01, Vol.134 (1), p.np-n/a</ispartof><rights>2016 Wiley Periodicals, Inc.</rights><rights>Distributed under a Creative Commons Attribution 4.0 International License</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c3647-2e4a408f0be6d819ee61c0d7a3de710e2259f9b3d237c1c736e4ae2dbe3427163</citedby><cites>FETCH-LOGICAL-c3647-2e4a408f0be6d819ee61c0d7a3de710e2259f9b3d237c1c736e4ae2dbe3427163</cites><orcidid>0000-0003-4617-0227 ; 0000-0003-0643-0784</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1002%2Fapp.44397$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1002%2Fapp.44397$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>230,314,776,780,881,1411,27901,27902,45550,45551</link.rule.ids><backlink>$$Uhttps://hal.science/hal-01407422$$DView record in HAL$$Hfree_for_read</backlink></links><search><creatorcontrib>Atli, A.</creatorcontrib><creatorcontrib>Simon, S.</creatorcontrib><creatorcontrib>Cadete Santos Aires, F. J.</creatorcontrib><creatorcontrib>Cardenas, L.</creatorcontrib><creatorcontrib>Ehret, E.</creatorcontrib><creatorcontrib>Lourdin, P.</creatorcontrib><title>A new strategy to activate liquid crystal polymer samples for electroless copper deposition</title><title>Journal of applied polymer science</title><description>ABSTRACT
In order to activate the polymers for electroless copper deposition, an alternative way of sample preparation is demonstrated. The samples are prepared by incorporation of a small amount (<1 wt %) of palladium, nickel, or copper acetate into the molten Liquid Crystal Polymer (LCP) in a blender. Since the blending temperature is kept higher than the decomposition temperature of acetates, the acetates are thermally decomposed during blending, leading to the metallic Pd, Ni, or Cu which are used as activators for electroless deposition. After preparing the samples, electroless copper deposition is successfully realized. The influence of different acetates (Pd, Ni, or Cu acetates) on the deposition is investigated. The copper amount is higher and the deposition kinetics is faster on LCP samples with 0.15 wt % Pd and 0.4 wt % Ni than that with 0.4 wt % Cu. The deposited copper layers are uniform and oxide‐free. Moreover, the possibility to substitute expensive Pd activator by cheaper Ni or Cu is shown. © 2016 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2016, 133, 44397.</description><subject>ACETATES</subject><subject>Blending</subject><subject>Catalysis</subject><subject>Chemical Sciences</subject><subject>coatings</subject><subject>Copper</subject><subject>COPPER ACETATE</subject><subject>COPPER RESOURCES</subject><subject>DEPOSITION</subject><subject>Electroless plating</subject><subject>Environment and Society</subject><subject>Environmental Sciences</subject><subject>interfaces</subject><subject>kinetics</subject><subject>Liquid crystal polymers</subject><subject>liquid crystals</subject><subject>Materials science</subject><subject>Nickel</subject><subject>Palladium</subject><subject>PLATING</subject><subject>POLYMERS</subject><subject>spectroscopy</subject><subject>surfaces</subject><issn>0021-8995</issn><issn>1097-4628</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2017</creationdate><recordtype>article</recordtype><recordid>eNp1kU1P3DAQhi1UJLbAgX9gqZf2EPDYTpwcV6sWkFYqh3LiYHmdCRh518bOLsq_ryGolSr1NJp5n_nSS8gFsEtgjF-ZGC-lFJ06Igtgnapkw9tPZFE0qNquq0_I55yfGQOoWbMgD0u6w1eax2RGfJzoGKixozuUjHr3snc9tWnKo_E0Bj9tMdFsttFjpkNIFD3aMYWSZmpDjEXuMYbsRhd2Z-R4MD7j-Uc8Jfc_vv9a3VTrn9e3q-W6sqKRquIojWTtwDbY9C10iA1Y1isjelTAkPO6G7qN6LlQFqwSTWlA3m9QSK6gEafk2zz3yXgdk9uaNOlgnL5ZrvVbjYFkSnJ-gMJ-ndmYwsse86i3Llv03uww7LOGVtYtrwFkQb_8gz6HfdqVTwrFeQdKMfF3uU0h54TDnwuA6TdLdLFEv1tS2KuZfXUep_-Denl3N3f8Bqd5jOI</recordid><startdate>20170105</startdate><enddate>20170105</enddate><creator>Atli, A.</creator><creator>Simon, S.</creator><creator>Cadete Santos Aires, F. J.</creator><creator>Cardenas, L.</creator><creator>Ehret, E.</creator><creator>Lourdin, P.</creator><general>Wiley Subscription Services, Inc</general><general>Wiley</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8FD</scope><scope>JG9</scope><scope>H8G</scope><scope>1XC</scope><orcidid>https://orcid.org/0000-0003-4617-0227</orcidid><orcidid>https://orcid.org/0000-0003-0643-0784</orcidid></search><sort><creationdate>20170105</creationdate><title>A new strategy to activate liquid crystal polymer samples for electroless copper deposition</title><author>Atli, A. ; Simon, S. ; Cadete Santos Aires, F. J. ; Cardenas, L. ; Ehret, E. ; Lourdin, P.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c3647-2e4a408f0be6d819ee61c0d7a3de710e2259f9b3d237c1c736e4ae2dbe3427163</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2017</creationdate><topic>ACETATES</topic><topic>Blending</topic><topic>Catalysis</topic><topic>Chemical Sciences</topic><topic>coatings</topic><topic>Copper</topic><topic>COPPER ACETATE</topic><topic>COPPER RESOURCES</topic><topic>DEPOSITION</topic><topic>Electroless plating</topic><topic>Environment and Society</topic><topic>Environmental Sciences</topic><topic>interfaces</topic><topic>kinetics</topic><topic>Liquid crystal polymers</topic><topic>liquid crystals</topic><topic>Materials science</topic><topic>Nickel</topic><topic>Palladium</topic><topic>PLATING</topic><topic>POLYMERS</topic><topic>spectroscopy</topic><topic>surfaces</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Atli, A.</creatorcontrib><creatorcontrib>Simon, S.</creatorcontrib><creatorcontrib>Cadete Santos Aires, F. J.</creatorcontrib><creatorcontrib>Cardenas, L.</creatorcontrib><creatorcontrib>Ehret, E.</creatorcontrib><creatorcontrib>Lourdin, P.</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Copper Technical Reference Library</collection><collection>Hyper Article en Ligne (HAL)</collection><jtitle>Journal of applied polymer science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Atli, A.</au><au>Simon, S.</au><au>Cadete Santos Aires, F. J.</au><au>Cardenas, L.</au><au>Ehret, E.</au><au>Lourdin, P.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>A new strategy to activate liquid crystal polymer samples for electroless copper deposition</atitle><jtitle>Journal of applied polymer science</jtitle><date>2017-01-05</date><risdate>2017</risdate><volume>134</volume><issue>1</issue><spage>np</spage><epage>n/a</epage><pages>np-n/a</pages><issn>0021-8995</issn><eissn>1097-4628</eissn><coden>JAPNAB</coden><abstract>ABSTRACT
In order to activate the polymers for electroless copper deposition, an alternative way of sample preparation is demonstrated. The samples are prepared by incorporation of a small amount (<1 wt %) of palladium, nickel, or copper acetate into the molten Liquid Crystal Polymer (LCP) in a blender. Since the blending temperature is kept higher than the decomposition temperature of acetates, the acetates are thermally decomposed during blending, leading to the metallic Pd, Ni, or Cu which are used as activators for electroless deposition. After preparing the samples, electroless copper deposition is successfully realized. The influence of different acetates (Pd, Ni, or Cu acetates) on the deposition is investigated. The copper amount is higher and the deposition kinetics is faster on LCP samples with 0.15 wt % Pd and 0.4 wt % Ni than that with 0.4 wt % Cu. The deposited copper layers are uniform and oxide‐free. Moreover, the possibility to substitute expensive Pd activator by cheaper Ni or Cu is shown. © 2016 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2016, 133, 44397.</abstract><cop>Hoboken</cop><pub>Wiley Subscription Services, Inc</pub><doi>10.1002/app.44397</doi><tpages>12</tpages><orcidid>https://orcid.org/0000-0003-4617-0227</orcidid><orcidid>https://orcid.org/0000-0003-0643-0784</orcidid></addata></record> |
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| source | Wiley Online Library Journals Frontfile Complete |
| subjects | ACETATES Blending Catalysis Chemical Sciences coatings Copper COPPER ACETATE COPPER RESOURCES DEPOSITION Electroless plating Environment and Society Environmental Sciences interfaces kinetics Liquid crystal polymers liquid crystals Materials science Nickel Palladium PLATING POLYMERS spectroscopy surfaces |
| title | A new strategy to activate liquid crystal polymer samples for electroless copper deposition |
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