“Thiol-ene” photoclick chemistry as a rapid and localizable functionalization pathway for silica capillary monolithic columns

•Novel photografting process for in situ silica monolithic column functionalization.•Photografting based on the photo-click thiol-ene reaction.•Photografting of octadecanthiol leads to ODS functionalized silica monolith. Herein, we report the “ene-thiol” photografting of 1-octadecanethiol onto vinyl...

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Veröffentlicht in:	Journal of Chromatography A 2014-08, Vol.1355, p.296-300
Hauptverfasser:	Laaniste, A., Marechal, A., El-Debs, R., Randon, J., Dugas, V., Demesmay, C.
Format:	Artikel
Sprache:	eng
Schlagworte:	Analytical chemistry Chemical Sciences Chemistry Chromatographic methods and physical methods associated with chromatography Chromatography Click Chemistry - instrumentation Click Chemistry - methods Exact sciences and technology Illumination Irradiation Marine Nano-LC Nanostructure Other chromatographic methods Permeability Photoclick thiol-ene reaction Photografting Polymerization Selectivity Silica monolithic columns Silicon dioxide Silicon Dioxide - chemistry Sulfhydryl Compounds - chemistry Surface functionalization
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