CRISTAPRESS: an optical cell for structure development in high-pressure crystallization
An original optical high-pressure cell, named CRISTAPRESS, has been especially designed to investigate phase transitions of complex liquids, i.e., polymers, polymer blends, nano-composites, etc. The design of the cell is based on the optical properties of morphological entities through in situ light...
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| Veröffentlicht in: | Review of scientific instruments 2014-01, Vol.85 (1), p.013906-013906 |
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| container_title | Review of scientific instruments |
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| creator | Boyer, S A E Fournier, F E J Gandin, Ch-A Haudin, J-M |
| description | An original optical high-pressure cell, named CRISTAPRESS, has been especially designed to investigate phase transitions of complex liquids, i.e., polymers, polymer blends, nano-composites, etc. The design of the cell is based on the optical properties of morphological entities through in situ light depolarizing microscopic observations. Pressure up to 200 MPa with a fine temperature control up to 300 °C can be applied. A striking advantage of this cell is the possibility to select the pressure transmitting medium that can be water, silicone oil, a fluid in the supercritical state, etc. The potential of the novel technique was demonstrated by carrying out time-resolved measurements during polymer crystallization induced by water pressure. These preliminary experimental investigations permit to discriminate the role of the barometric and thermal histories on the kinetics of polymer growth, as well as on the subsequent morphologies. It should lead to new reliable crystallization kinetics models. |
| doi_str_mv | 10.1063/1.4862473 |
| format | Article |
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Pressure up to 200 MPa with a fine temperature control up to 300 °C can be applied. A striking advantage of this cell is the possibility to select the pressure transmitting medium that can be water, silicone oil, a fluid in the supercritical state, etc. The potential of the novel technique was demonstrated by carrying out time-resolved measurements during polymer crystallization induced by water pressure. These preliminary experimental investigations permit to discriminate the role of the barometric and thermal histories on the kinetics of polymer growth, as well as on the subsequent morphologies. It should lead to new reliable crystallization kinetics models.</description><identifier>ISSN: 0034-6748</identifier><identifier>EISSN: 1089-7623</identifier><identifier>DOI: 10.1063/1.4862473</identifier><identifier>PMID: 24517781</identifier><language>eng</language><publisher>United States: American Institute of Physics</publisher><subject>Barometers ; Crystallization ; Depolarization ; Engineering Sciences ; Materials ; Morphology ; Nanocomposites ; Optical properties ; Phase transitions ; Polymer blends ; Polymer matrix composites ; Polymers ; Pressure cells ; Pressure crystallization ; Scientific apparatus & instruments ; Temperature control ; Water pressure</subject><ispartof>Review of scientific instruments, 2014-01, Vol.85 (1), p.013906-013906</ispartof><rights>2014 AIP Publishing LLC.</rights><rights>Distributed under a Creative Commons Attribution 4.0 International License</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c347t-ffb231a31c9da089668b7667964c1569f878c068cf49badd93c05a442d0802c3</citedby><cites>FETCH-LOGICAL-c347t-ffb231a31c9da089668b7667964c1569f878c068cf49badd93c05a442d0802c3</cites><orcidid>0000-0003-4052-2981 ; 0000-0002-6270-5407</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>230,314,780,784,885,4024,27923,27924,27925</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/24517781$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink><backlink>$$Uhttps://minesparis-psl.hal.science/hal-00960121$$DView record in HAL$$Hfree_for_read</backlink></links><search><creatorcontrib>Boyer, S A E</creatorcontrib><creatorcontrib>Fournier, F E J</creatorcontrib><creatorcontrib>Gandin, Ch-A</creatorcontrib><creatorcontrib>Haudin, J-M</creatorcontrib><title>CRISTAPRESS: an optical cell for structure development in high-pressure crystallization</title><title>Review of scientific instruments</title><addtitle>Rev Sci Instrum</addtitle><description>An original optical high-pressure cell, named CRISTAPRESS, has been especially designed to investigate phase transitions of complex liquids, i.e., polymers, polymer blends, nano-composites, etc. The design of the cell is based on the optical properties of morphological entities through in situ light depolarizing microscopic observations. Pressure up to 200 MPa with a fine temperature control up to 300 °C can be applied. A striking advantage of this cell is the possibility to select the pressure transmitting medium that can be water, silicone oil, a fluid in the supercritical state, etc. The potential of the novel technique was demonstrated by carrying out time-resolved measurements during polymer crystallization induced by water pressure. These preliminary experimental investigations permit to discriminate the role of the barometric and thermal histories on the kinetics of polymer growth, as well as on the subsequent morphologies. 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| fulltext | fulltext |
| identifier | ISSN: 0034-6748 |
| ispartof | Review of scientific instruments, 2014-01, Vol.85 (1), p.013906-013906 |
| issn | 0034-6748 1089-7623 |
| language | eng |
| recordid | cdi_hal_primary_oai_HAL_hal_00960121v1 |
| source | AIP Journals Complete; Alma/SFX Local Collection |
| subjects | Barometers Crystallization Depolarization Engineering Sciences Materials Morphology Nanocomposites Optical properties Phase transitions Polymer blends Polymer matrix composites Polymers Pressure cells Pressure crystallization Scientific apparatus & instruments Temperature control Water pressure |
| title | CRISTAPRESS: an optical cell for structure development in high-pressure crystallization |
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