Amorphous and partially crystallized metallic glasses: An indentation study
The plastic behaviour of amorphous, partially and totally crystallized Zr 41.25Ti 13.75Cu 12.5Ni 10Be 22.5 (at.%) Vitreloy1 samples is investigated using self similar instrumented indentation. Residual imprints are imaged using atomic force microscopy (AFM). Young's modulus and hardness are est...
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| Veröffentlicht in: | Materials science & engineering. A, Structural materials : properties, microstructure and processing Structural materials : properties, microstructure and processing, 2008-06, Vol.483 (SI), p.652-655 |
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| container_title | Materials science & engineering. A, Structural materials : properties, microstructure and processing |
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| creator | Charleux, L. Gravier, S. Verdier, M. Fivel, M. Blandin, J.J. |
| description | The plastic behaviour of amorphous, partially and totally crystallized Zr
41.25Ti
13.75Cu
12.5Ni
10Be
22.5 (at.%) Vitreloy1 samples is investigated using self similar instrumented indentation. Residual imprints are imaged using atomic force microscopy (AFM). Young's modulus and hardness are estimated using the value of the contact area derived from AFM imaging. Compressive tests and three point bending ultrasonic measurements are performed to probe the macroscopic properties. Despite a significant change in the shape of the imprint during the loading, we show that the amorphous alloy does not exhibit any size effect. Both for the amorphous and for the partially crystallized samples, the values of the Young modulus and the yield stress obtained by nanoindentation are consistent with those obtained by the macroscopic procedure. Inversely, the full crystallization samples display high brittleness on compressive tests while no cracking but only an increasing yield stress are observed using indentation. It is concluded that indentation is a well-suited test to probe the mechanical properties of the bulk metallic glasses. |
| doi_str_mv | 10.1016/j.msea.2006.12.180 |
| format | Article |
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41.25Ti
13.75Cu
12.5Ni
10Be
22.5 (at.%) Vitreloy1 samples is investigated using self similar instrumented indentation. Residual imprints are imaged using atomic force microscopy (AFM). Young's modulus and hardness are estimated using the value of the contact area derived from AFM imaging. Compressive tests and three point bending ultrasonic measurements are performed to probe the macroscopic properties. Despite a significant change in the shape of the imprint during the loading, we show that the amorphous alloy does not exhibit any size effect. Both for the amorphous and for the partially crystallized samples, the values of the Young modulus and the yield stress obtained by nanoindentation are consistent with those obtained by the macroscopic procedure. Inversely, the full crystallization samples display high brittleness on compressive tests while no cracking but only an increasing yield stress are observed using indentation. It is concluded that indentation is a well-suited test to probe the mechanical properties of the bulk metallic glasses.</description><identifier>ISSN: 0921-5093</identifier><identifier>EISSN: 1873-4936</identifier><identifier>DOI: 10.1016/j.msea.2006.12.180</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>Bulk metallic glasses ; Condensed matter: structure, mechanical and thermal properties ; Deformation and plasticity (including yield, ductility, and superplasticity) ; Engineering Sciences ; Exact sciences and technology ; Fracture stress ; Indentation ; Materials ; Mechanical and acoustical properties of condensed matter ; Mechanical properties of solids ; Mechanics ; Physics ; Shear bands ; Yield stress</subject><ispartof>Materials science & engineering. A, Structural materials : properties, microstructure and processing, 2008-06, Vol.483 (SI), p.652-655</ispartof><rights>2007 Elsevier B.V.</rights><rights>2008 INIST-CNRS</rights><rights>Distributed under a Creative Commons Attribution 4.0 International License</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c395t-63f291aeb5950c2e56826581bf773574d9efa255e1b5a15a83a5b0a405ce6b2f3</citedby><cites>FETCH-LOGICAL-c395t-63f291aeb5950c2e56826581bf773574d9efa255e1b5a15a83a5b0a405ce6b2f3</cites><orcidid>0000-0003-0563-2675 ; 0000-0003-3533-2438</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.msea.2006.12.180$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>230,309,310,314,780,784,789,790,885,3550,23930,23931,25140,27924,27925,45995</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=20375582$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://hal.science/hal-00935239$$DView record in HAL$$Hfree_for_read</backlink></links><search><creatorcontrib>Charleux, L.</creatorcontrib><creatorcontrib>Gravier, S.</creatorcontrib><creatorcontrib>Verdier, M.</creatorcontrib><creatorcontrib>Fivel, M.</creatorcontrib><creatorcontrib>Blandin, J.J.</creatorcontrib><title>Amorphous and partially crystallized metallic glasses: An indentation study</title><title>Materials science & engineering. A, Structural materials : properties, microstructure and processing</title><description>The plastic behaviour of amorphous, partially and totally crystallized Zr
41.25Ti
13.75Cu
12.5Ni
10Be
22.5 (at.%) Vitreloy1 samples is investigated using self similar instrumented indentation. Residual imprints are imaged using atomic force microscopy (AFM). Young's modulus and hardness are estimated using the value of the contact area derived from AFM imaging. Compressive tests and three point bending ultrasonic measurements are performed to probe the macroscopic properties. Despite a significant change in the shape of the imprint during the loading, we show that the amorphous alloy does not exhibit any size effect. Both for the amorphous and for the partially crystallized samples, the values of the Young modulus and the yield stress obtained by nanoindentation are consistent with those obtained by the macroscopic procedure. Inversely, the full crystallization samples display high brittleness on compressive tests while no cracking but only an increasing yield stress are observed using indentation. It is concluded that indentation is a well-suited test to probe the mechanical properties of the bulk metallic glasses.</description><subject>Bulk metallic glasses</subject><subject>Condensed matter: structure, mechanical and thermal properties</subject><subject>Deformation and plasticity (including yield, ductility, and superplasticity)</subject><subject>Engineering Sciences</subject><subject>Exact sciences and technology</subject><subject>Fracture stress</subject><subject>Indentation</subject><subject>Materials</subject><subject>Mechanical and acoustical properties of condensed matter</subject><subject>Mechanical properties of solids</subject><subject>Mechanics</subject><subject>Physics</subject><subject>Shear bands</subject><subject>Yield stress</subject><issn>0921-5093</issn><issn>1873-4936</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2008</creationdate><recordtype>article</recordtype><recordid>eNp9kE1P3DAQhq2qSF2gf6CnXFqJQ8LYXicx6mWFWkCsxAXO1sSZFK_ysXiySMuvr7eLOPbkkfXMOzOPEN8kFBJkebkpBiYsFEBZSFXIGj6JhawrnS-tLj-LBVglcwNWfxGnzBsAkEswC3G_Gqa4fZ52nOHYZluMc8C-32c-7nlOVXijNhvoX-mzPz0yE19lqzELY0vjjHOYxoznXbs_Fycd9kxf398z8fT71-P1bb5-uLm7Xq1zr62Z81J3ykqkxlgDXpEpa1WaWjZdVWlTLVtLHSpjSDYGpcFao2kA07qeykZ1-kxcHHOfsXfbGAaMezdhcLertTv8QbrTKG1fZWJ_HNltnF52xLMbAnvqexwpHe20BmVUaROojqCPE3Ok7iNZgjs4dht3cOwOjp1ULjlOTd_f05E99l3E0Qf-6FSgK2NqlbifR46SltdA0bEPNHpqQyQ_u3YK_xvzF6JVkao</recordid><startdate>20080615</startdate><enddate>20080615</enddate><creator>Charleux, L.</creator><creator>Gravier, S.</creator><creator>Verdier, M.</creator><creator>Fivel, M.</creator><creator>Blandin, J.J.</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>1XC</scope><orcidid>https://orcid.org/0000-0003-0563-2675</orcidid><orcidid>https://orcid.org/0000-0003-3533-2438</orcidid></search><sort><creationdate>20080615</creationdate><title>Amorphous and partially crystallized metallic glasses: An indentation study</title><author>Charleux, L. ; Gravier, S. ; Verdier, M. ; Fivel, M. ; Blandin, J.J.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c395t-63f291aeb5950c2e56826581bf773574d9efa255e1b5a15a83a5b0a405ce6b2f3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2008</creationdate><topic>Bulk metallic glasses</topic><topic>Condensed matter: structure, mechanical and thermal properties</topic><topic>Deformation and plasticity (including yield, ductility, and superplasticity)</topic><topic>Engineering Sciences</topic><topic>Exact sciences and technology</topic><topic>Fracture stress</topic><topic>Indentation</topic><topic>Materials</topic><topic>Mechanical and acoustical properties of condensed matter</topic><topic>Mechanical properties of solids</topic><topic>Mechanics</topic><topic>Physics</topic><topic>Shear bands</topic><topic>Yield stress</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Charleux, L.</creatorcontrib><creatorcontrib>Gravier, S.</creatorcontrib><creatorcontrib>Verdier, M.</creatorcontrib><creatorcontrib>Fivel, M.</creatorcontrib><creatorcontrib>Blandin, J.J.</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Hyper Article en Ligne (HAL)</collection><jtitle>Materials science & engineering. A, Structural materials : properties, microstructure and processing</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Charleux, L.</au><au>Gravier, S.</au><au>Verdier, M.</au><au>Fivel, M.</au><au>Blandin, J.J.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Amorphous and partially crystallized metallic glasses: An indentation study</atitle><jtitle>Materials science & engineering. A, Structural materials : properties, microstructure and processing</jtitle><date>2008-06-15</date><risdate>2008</risdate><volume>483</volume><issue>SI</issue><spage>652</spage><epage>655</epage><pages>652-655</pages><issn>0921-5093</issn><eissn>1873-4936</eissn><abstract>The plastic behaviour of amorphous, partially and totally crystallized Zr
41.25Ti
13.75Cu
12.5Ni
10Be
22.5 (at.%) Vitreloy1 samples is investigated using self similar instrumented indentation. Residual imprints are imaged using atomic force microscopy (AFM). Young's modulus and hardness are estimated using the value of the contact area derived from AFM imaging. Compressive tests and three point bending ultrasonic measurements are performed to probe the macroscopic properties. Despite a significant change in the shape of the imprint during the loading, we show that the amorphous alloy does not exhibit any size effect. Both for the amorphous and for the partially crystallized samples, the values of the Young modulus and the yield stress obtained by nanoindentation are consistent with those obtained by the macroscopic procedure. Inversely, the full crystallization samples display high brittleness on compressive tests while no cracking but only an increasing yield stress are observed using indentation. It is concluded that indentation is a well-suited test to probe the mechanical properties of the bulk metallic glasses.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><doi>10.1016/j.msea.2006.12.180</doi><tpages>4</tpages><orcidid>https://orcid.org/0000-0003-0563-2675</orcidid><orcidid>https://orcid.org/0000-0003-3533-2438</orcidid></addata></record> |
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| ispartof | Materials science & engineering. A, Structural materials : properties, microstructure and processing, 2008-06, Vol.483 (SI), p.652-655 |
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| language | eng |
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| source | Elsevier ScienceDirect Journals Complete |
| subjects | Bulk metallic glasses Condensed matter: structure, mechanical and thermal properties Deformation and plasticity (including yield, ductility, and superplasticity) Engineering Sciences Exact sciences and technology Fracture stress Indentation Materials Mechanical and acoustical properties of condensed matter Mechanical properties of solids Mechanics Physics Shear bands Yield stress |
| title | Amorphous and partially crystallized metallic glasses: An indentation study |
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