Phenolic resins (IV). Thermal degradation of crosslinked resins in controlled atmospheres
The study involved the thermal degradation of phenolic resins in controlled atmospheres (inert and oxidizing). Its aim was to characterize volatile organic compounds (VOC) and inorganic compounds released during heat treatment. The methods used were thermogravimetry coupled with thermodesorption/gas...
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| Veröffentlicht in: | Polymers & polymer composites 2003-01, Vol.11 (5), p.345-357 |
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| container_issue | 5 |
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| container_title | Polymers & polymer composites |
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| creator | BOUAJILA, J RAFFIN, G ALAMERCERY, S WATON, H SANGLAR, C GRENIER-LOUSTALOT, M. F |
| description | The study involved the thermal degradation of phenolic resins in controlled atmospheres (inert and oxidizing). Its aim was to characterize volatile organic compounds (VOC) and inorganic compounds released during heat treatment. The methods used were thermogravimetry coupled with thermodesorption/gas chromatography/mass spectrometry (TG/TCT/GC/MS) and thermogravimetric analysis coupled with infrared (TGA/IR). At the end of the heat cycle, residues were characterized by Fourier transform infrared spectroscopy (FTIR) and nuclear magnetic resonance (solid state 13 C NMR (CP/MAS)). The data show that the synthesis conditions of the crosslinked resins, the controlled environment and the temperature of the degradation heat cycle, all affect the composition of volatile compounds and residues at the end of the cycle. The data have enabled us to propose decomposition reaction mechanisms for these resins in oxidizing and inert environments. |
| doi_str_mv | 10.1177/096739110301100501 |
| format | Article |
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Thermal degradation of crosslinked resins in controlled atmospheres</title><source>Access via SAGE</source><source>Sage Journals GOLD Open Access 2024</source><creator>BOUAJILA, J ; RAFFIN, G ; ALAMERCERY, S ; WATON, H ; SANGLAR, C ; GRENIER-LOUSTALOT, M. F</creator><creatorcontrib>BOUAJILA, J ; RAFFIN, G ; ALAMERCERY, S ; WATON, H ; SANGLAR, C ; GRENIER-LOUSTALOT, M. F</creatorcontrib><description>The study involved the thermal degradation of phenolic resins in controlled atmospheres (inert and oxidizing). Its aim was to characterize volatile organic compounds (VOC) and inorganic compounds released during heat treatment. The methods used were thermogravimetry coupled with thermodesorption/gas chromatography/mass spectrometry (TG/TCT/GC/MS) and thermogravimetric analysis coupled with infrared (TGA/IR). At the end of the heat cycle, residues were characterized by Fourier transform infrared spectroscopy (FTIR) and nuclear magnetic resonance (solid state 13 C NMR (CP/MAS)). The data show that the synthesis conditions of the crosslinked resins, the controlled environment and the temperature of the degradation heat cycle, all affect the composition of volatile compounds and residues at the end of the cycle. The data have enabled us to propose decomposition reaction mechanisms for these resins in oxidizing and inert environments.</description><identifier>ISSN: 0967-3911</identifier><identifier>EISSN: 1478-2391</identifier><identifier>DOI: 10.1177/096739110301100501</identifier><language>eng</language><publisher>Shrewsbury: Rapra Technology</publisher><subject>Analytical chemistry ; Applied sciences ; Chemical reactions and properties ; Chemical Sciences ; Degradation ; Exact sciences and technology ; Organic polymers ; Physicochemistry of polymers</subject><ispartof>Polymers & polymer composites, 2003-01, Vol.11 (5), p.345-357</ispartof><rights>2003 INIST-CNRS</rights><rights>Distributed under a Creative Commons Attribution 4.0 International License</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c340t-9f7eb2cc0e6f5a4ba24fc26f69a427a36e57d1f24bce68fec0b1310593e639013</citedby><cites>FETCH-LOGICAL-c340t-9f7eb2cc0e6f5a4ba24fc26f69a427a36e57d1f24bce68fec0b1310593e639013</cites><orcidid>0000-0002-7156-2313 ; 0000-0003-4177-2667 ; 0000-0002-2439-5145</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>230,314,780,784,885,27924,27925</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=15018609$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://hal.science/hal-00511095$$DView record in HAL$$Hfree_for_read</backlink></links><search><creatorcontrib>BOUAJILA, J</creatorcontrib><creatorcontrib>RAFFIN, G</creatorcontrib><creatorcontrib>ALAMERCERY, S</creatorcontrib><creatorcontrib>WATON, H</creatorcontrib><creatorcontrib>SANGLAR, C</creatorcontrib><creatorcontrib>GRENIER-LOUSTALOT, M. F</creatorcontrib><title>Phenolic resins (IV). Thermal degradation of crosslinked resins in controlled atmospheres</title><title>Polymers & polymer composites</title><description>The study involved the thermal degradation of phenolic resins in controlled atmospheres (inert and oxidizing). Its aim was to characterize volatile organic compounds (VOC) and inorganic compounds released during heat treatment. The methods used were thermogravimetry coupled with thermodesorption/gas chromatography/mass spectrometry (TG/TCT/GC/MS) and thermogravimetric analysis coupled with infrared (TGA/IR). At the end of the heat cycle, residues were characterized by Fourier transform infrared spectroscopy (FTIR) and nuclear magnetic resonance (solid state 13 C NMR (CP/MAS)). The data show that the synthesis conditions of the crosslinked resins, the controlled environment and the temperature of the degradation heat cycle, all affect the composition of volatile compounds and residues at the end of the cycle. The data have enabled us to propose decomposition reaction mechanisms for these resins in oxidizing and inert environments.</description><subject>Analytical chemistry</subject><subject>Applied sciences</subject><subject>Chemical reactions and properties</subject><subject>Chemical Sciences</subject><subject>Degradation</subject><subject>Exact sciences and technology</subject><subject>Organic polymers</subject><subject>Physicochemistry of polymers</subject><issn>0967-3911</issn><issn>1478-2391</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2003</creationdate><recordtype>article</recordtype><recordid>eNplkM9LwzAYhoMoOKf_gKdeFHfozI82XY5jqBsM9DAFTyVNv7ho2sykE_zvTd3Ug5d88PK8L-RB6JzgMSFFcY0FL5ggBDMcH5xjcoAGJCsmKY3xIRr0QNoTx-gkhFeMKeE8H6DnhzW0zhqVeAimDcnV4mk0TlZr8I20SQ0vXtayM65NnE6UdyFY075B_cObNlGu7byzNoaya1zYxDKEU3SkpQ1wtr9D9Hh7s5rN0-X93WI2XaaKZbhLhS6gokph4DqXWSVpphXlmguZ0UIyDnlRE02zSgGfaFC4IozgXDDgTGDChmi0211LW268aaT_LJ005Xy6LPss6ohORP7Rs5c7duPd-xZCVzYmKLBWtuC2oaSFiNIojiDdgd8_9qB_lwkue-Plf-OxdLFfl0FJq71slQl_zchMOBbsC8xwf5Y</recordid><startdate>20030101</startdate><enddate>20030101</enddate><creator>BOUAJILA, J</creator><creator>RAFFIN, G</creator><creator>ALAMERCERY, S</creator><creator>WATON, H</creator><creator>SANGLAR, C</creator><creator>GRENIER-LOUSTALOT, M. 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The data show that the synthesis conditions of the crosslinked resins, the controlled environment and the temperature of the degradation heat cycle, all affect the composition of volatile compounds and residues at the end of the cycle. The data have enabled us to propose decomposition reaction mechanisms for these resins in oxidizing and inert environments.</abstract><cop>Shrewsbury</cop><pub>Rapra Technology</pub><doi>10.1177/096739110301100501</doi><tpages>13</tpages><orcidid>https://orcid.org/0000-0002-7156-2313</orcidid><orcidid>https://orcid.org/0000-0003-4177-2667</orcidid><orcidid>https://orcid.org/0000-0002-2439-5145</orcidid></addata></record> |
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| identifier | ISSN: 0967-3911 |
| ispartof | Polymers & polymer composites, 2003-01, Vol.11 (5), p.345-357 |
| issn | 0967-3911 1478-2391 |
| language | eng |
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| source | Access via SAGE; Sage Journals GOLD Open Access 2024 |
| subjects | Analytical chemistry Applied sciences Chemical reactions and properties Chemical Sciences Degradation Exact sciences and technology Organic polymers Physicochemistry of polymers |
| title | Phenolic resins (IV). Thermal degradation of crosslinked resins in controlled atmospheres |
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