Syntheses and characterization of different zinc(II) oxide nano-structures from direct thermal decomposition of 1D coordination polymers
Three zinc(II) nitrite coordination polymers, [Zn(4-bpdb)(NO 2) 2] n ( 1), {[Zn (3-bpdb) (NO 2)]·0.5H 2O} n ( 2) and [Zn(3-bpdh)(NO 2) 2] n ( 3), 4-bpdb = 1,4-bis(4-pyridyl)-2,3-diaza-1,3-butadiene, 3-bpdb = 1,4-bis(3-pyridyl)-2,3-diaza-1,3-butadiene and 3-bpdh = 2,5-bis(3-pyridyl)-3,4-diaza-2,4-hex...
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| Veröffentlicht in: | Polyhedron 2010-02, Vol.29 (2), p.801-806 |
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| creator | Bigdeli, Fahime Morsali, Ali Retailleau, Pascal |
| description | Three zinc(II) nitrite coordination polymers, [Zn(4-bpdb)(NO
2)
2]
n
(
1), {[Zn (3-bpdb) (NO
2)]·0.5H
2O}
n
(
2) and [Zn(3-bpdh)(NO
2)
2]
n
(
3), 4-bpdb
=
1,4-bis(4-pyridyl)-2,3-diaza-1,3-butadiene, 3-bpdb
=
1,4-bis(3-pyridyl)-2,3-diaza-1,3-butadiene and 3-bpdh
=
2,5-bis(3-pyridyl)-3,4-diaza-2,4-hexadiene} were prepared and characterized by elemental analyses and IR spectroscopy. Compound
3 was structurally characterized by single-crystal X-ray diffraction and is one-dimensional polymer with coordination environments of distorted octahedral, ZnN
2O
4.
Three zinc(II) nitrite coordination polymers, [Zn(4-bpdb)(NO
2)
2]
n
(
1), {[Zn(3-bpdb)(NO
2)]·0.5H
2O}
n
(
2) and [Zn(3-bpdh)(NO
2)
2]
n
(
3), 4-bpdb = 1,4-bis(4-pyridyl)-2,3-diaza-1,3-butadiene, 3-bpdb
=
1,4-bis(3-pyridyl)-2,3-diaza-1,3-butadiene and 3-bpdh
=
2,5-bis(3-pyridyl)-3,4-diaza-2,4-hexadiene} were prepared and characterized by elemental analyses and IR spectroscopy. Compound
3 was structurally characterized by single-crystal X-ray diffraction and is one-dimensional polymer with coordination environments of distorted octahedral, ZnN
2O
4. The thermal stabilities of compounds
1–3 were studied by thermal gravimetric (TG) and differential thermal analyses (DTA). Direct calcination of the compounds
1–3 at 600
°C under air atmospheres yields different morphologies of nano-sized ZnO. |
| doi_str_mv | 10.1016/j.poly.2009.10.027 |
| format | Article |
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2)
2]
n
(
1), {[Zn (3-bpdb) (NO
2)]·0.5H
2O}
n
(
2) and [Zn(3-bpdh)(NO
2)
2]
n
(
3), 4-bpdb
=
1,4-bis(4-pyridyl)-2,3-diaza-1,3-butadiene, 3-bpdb
=
1,4-bis(3-pyridyl)-2,3-diaza-1,3-butadiene and 3-bpdh
=
2,5-bis(3-pyridyl)-3,4-diaza-2,4-hexadiene} were prepared and characterized by elemental analyses and IR spectroscopy. Compound
3 was structurally characterized by single-crystal X-ray diffraction and is one-dimensional polymer with coordination environments of distorted octahedral, ZnN
2O
4.
Three zinc(II) nitrite coordination polymers, [Zn(4-bpdb)(NO
2)
2]
n
(
1), {[Zn(3-bpdb)(NO
2)]·0.5H
2O}
n
(
2) and [Zn(3-bpdh)(NO
2)
2]
n
(
3), 4-bpdb = 1,4-bis(4-pyridyl)-2,3-diaza-1,3-butadiene, 3-bpdb
=
1,4-bis(3-pyridyl)-2,3-diaza-1,3-butadiene and 3-bpdh
=
2,5-bis(3-pyridyl)-3,4-diaza-2,4-hexadiene} were prepared and characterized by elemental analyses and IR spectroscopy. Compound
3 was structurally characterized by single-crystal X-ray diffraction and is one-dimensional polymer with coordination environments of distorted octahedral, ZnN
2O
4. The thermal stabilities of compounds
1–3 were studied by thermal gravimetric (TG) and differential thermal analyses (DTA). Direct calcination of the compounds
1–3 at 600
°C under air atmospheres yields different morphologies of nano-sized ZnO.</description><identifier>ISSN: 0277-5387</identifier><identifier>EISSN: 0277-5387</identifier><identifier>DOI: 10.1016/j.poly.2009.10.027</identifier><language>eng</language><publisher>Elsevier Ltd</publisher><subject>Chemical Sciences ; Coordination polymer ; Nano-structure ; Organic chemistry ; Zinc(II) nitrite ; Zinc(II) oxide</subject><ispartof>Polyhedron, 2010-02, Vol.29 (2), p.801-806</ispartof><rights>2009 Elsevier Ltd</rights><rights>Distributed under a Creative Commons Attribution 4.0 International License</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c334t-73e7516785f03c9330388aebcc08b4a8592e60a3f2d07b04941d683a1beeae813</citedby><cites>FETCH-LOGICAL-c334t-73e7516785f03c9330388aebcc08b4a8592e60a3f2d07b04941d683a1beeae813</cites><orcidid>0000-0003-3995-519X</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.poly.2009.10.027$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>230,314,776,780,881,3536,27903,27904,45974</link.rule.ids><backlink>$$Uhttps://hal.science/hal-00466334$$DView record in HAL$$Hfree_for_read</backlink></links><search><creatorcontrib>Bigdeli, Fahime</creatorcontrib><creatorcontrib>Morsali, Ali</creatorcontrib><creatorcontrib>Retailleau, Pascal</creatorcontrib><title>Syntheses and characterization of different zinc(II) oxide nano-structures from direct thermal decomposition of 1D coordination polymers</title><title>Polyhedron</title><description>Three zinc(II) nitrite coordination polymers, [Zn(4-bpdb)(NO
2)
2]
n
(
1), {[Zn (3-bpdb) (NO
2)]·0.5H
2O}
n
(
2) and [Zn(3-bpdh)(NO
2)
2]
n
(
3), 4-bpdb
=
1,4-bis(4-pyridyl)-2,3-diaza-1,3-butadiene, 3-bpdb
=
1,4-bis(3-pyridyl)-2,3-diaza-1,3-butadiene and 3-bpdh
=
2,5-bis(3-pyridyl)-3,4-diaza-2,4-hexadiene} were prepared and characterized by elemental analyses and IR spectroscopy. Compound
3 was structurally characterized by single-crystal X-ray diffraction and is one-dimensional polymer with coordination environments of distorted octahedral, ZnN
2O
4.
Three zinc(II) nitrite coordination polymers, [Zn(4-bpdb)(NO
2)
2]
n
(
1), {[Zn(3-bpdb)(NO
2)]·0.5H
2O}
n
(
2) and [Zn(3-bpdh)(NO
2)
2]
n
(
3), 4-bpdb = 1,4-bis(4-pyridyl)-2,3-diaza-1,3-butadiene, 3-bpdb
=
1,4-bis(3-pyridyl)-2,3-diaza-1,3-butadiene and 3-bpdh
=
2,5-bis(3-pyridyl)-3,4-diaza-2,4-hexadiene} were prepared and characterized by elemental analyses and IR spectroscopy. Compound
3 was structurally characterized by single-crystal X-ray diffraction and is one-dimensional polymer with coordination environments of distorted octahedral, ZnN
2O
4. The thermal stabilities of compounds
1–3 were studied by thermal gravimetric (TG) and differential thermal analyses (DTA). Direct calcination of the compounds
1–3 at 600
°C under air atmospheres yields different morphologies of nano-sized ZnO.</description><subject>Chemical Sciences</subject><subject>Coordination polymer</subject><subject>Nano-structure</subject><subject>Organic chemistry</subject><subject>Zinc(II) nitrite</subject><subject>Zinc(II) oxide</subject><issn>0277-5387</issn><issn>0277-5387</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2010</creationdate><recordtype>article</recordtype><recordid>eNp9kL1OwzAUhS0EEqXwAkwe6ZBgx_lxJJaKv1aqxADMluPcqK4Su7LTivYJeGwcBRATi20dne_c64PQNSUxJTS_3cRb2x7ihJAyCDFJihM0CWcRZYwXp3_e5-jC-w0JUErZBH2-Hky_Bg8eS1NjtZZOqh6cPspeW4Ntg2vdNODA9PiojbpZLmfYfugasJHGRr53O9XvXAhonO2C24Hqcch0nWxxDcp2W-v1Txp9wMpaV2szDhj27sD5S3TWyNbD1fc9Re9Pj2_3i2j18ry8n68ixVjaRwWDIqN5wbOGMFUyRhjnEiqlCK9SybMygZxI1iQ1KSqSlimtc84krQAkcMqmaDbmrmUrtk530h2ElVos5isxaISkeR5m7QdvMnqVs947aH4BSsTQu9iIYX8x9D5ooeUA3Y0QhF_sNTjhlQajYGxG1Fb_h38Bx5qOnA</recordid><startdate>20100201</startdate><enddate>20100201</enddate><creator>Bigdeli, Fahime</creator><creator>Morsali, Ali</creator><creator>Retailleau, Pascal</creator><general>Elsevier Ltd</general><general>Elsevier</general><scope>AAYXX</scope><scope>CITATION</scope><scope>1XC</scope><orcidid>https://orcid.org/0000-0003-3995-519X</orcidid></search><sort><creationdate>20100201</creationdate><title>Syntheses and characterization of different zinc(II) oxide nano-structures from direct thermal decomposition of 1D coordination polymers</title><author>Bigdeli, Fahime ; Morsali, Ali ; Retailleau, Pascal</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c334t-73e7516785f03c9330388aebcc08b4a8592e60a3f2d07b04941d683a1beeae813</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2010</creationdate><topic>Chemical Sciences</topic><topic>Coordination polymer</topic><topic>Nano-structure</topic><topic>Organic chemistry</topic><topic>Zinc(II) nitrite</topic><topic>Zinc(II) oxide</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Bigdeli, Fahime</creatorcontrib><creatorcontrib>Morsali, Ali</creatorcontrib><creatorcontrib>Retailleau, Pascal</creatorcontrib><collection>CrossRef</collection><collection>Hyper Article en Ligne (HAL)</collection><jtitle>Polyhedron</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Bigdeli, Fahime</au><au>Morsali, Ali</au><au>Retailleau, Pascal</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Syntheses and characterization of different zinc(II) oxide nano-structures from direct thermal decomposition of 1D coordination polymers</atitle><jtitle>Polyhedron</jtitle><date>2010-02-01</date><risdate>2010</risdate><volume>29</volume><issue>2</issue><spage>801</spage><epage>806</epage><pages>801-806</pages><issn>0277-5387</issn><eissn>0277-5387</eissn><abstract>Three zinc(II) nitrite coordination polymers, [Zn(4-bpdb)(NO
2)
2]
n
(
1), {[Zn (3-bpdb) (NO
2)]·0.5H
2O}
n
(
2) and [Zn(3-bpdh)(NO
2)
2]
n
(
3), 4-bpdb
=
1,4-bis(4-pyridyl)-2,3-diaza-1,3-butadiene, 3-bpdb
=
1,4-bis(3-pyridyl)-2,3-diaza-1,3-butadiene and 3-bpdh
=
2,5-bis(3-pyridyl)-3,4-diaza-2,4-hexadiene} were prepared and characterized by elemental analyses and IR spectroscopy. Compound
3 was structurally characterized by single-crystal X-ray diffraction and is one-dimensional polymer with coordination environments of distorted octahedral, ZnN
2O
4.
Three zinc(II) nitrite coordination polymers, [Zn(4-bpdb)(NO
2)
2]
n
(
1), {[Zn(3-bpdb)(NO
2)]·0.5H
2O}
n
(
2) and [Zn(3-bpdh)(NO
2)
2]
n
(
3), 4-bpdb = 1,4-bis(4-pyridyl)-2,3-diaza-1,3-butadiene, 3-bpdb
=
1,4-bis(3-pyridyl)-2,3-diaza-1,3-butadiene and 3-bpdh
=
2,5-bis(3-pyridyl)-3,4-diaza-2,4-hexadiene} were prepared and characterized by elemental analyses and IR spectroscopy. Compound
3 was structurally characterized by single-crystal X-ray diffraction and is one-dimensional polymer with coordination environments of distorted octahedral, ZnN
2O
4. The thermal stabilities of compounds
1–3 were studied by thermal gravimetric (TG) and differential thermal analyses (DTA). Direct calcination of the compounds
1–3 at 600
°C under air atmospheres yields different morphologies of nano-sized ZnO.</abstract><pub>Elsevier Ltd</pub><doi>10.1016/j.poly.2009.10.027</doi><tpages>6</tpages><orcidid>https://orcid.org/0000-0003-3995-519X</orcidid></addata></record> |
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| ispartof | Polyhedron, 2010-02, Vol.29 (2), p.801-806 |
| issn | 0277-5387 0277-5387 |
| language | eng |
| recordid | cdi_hal_primary_oai_HAL_hal_00466334v1 |
| source | Elsevier ScienceDirect Journals |
| subjects | Chemical Sciences Coordination polymer Nano-structure Organic chemistry Zinc(II) nitrite Zinc(II) oxide |
| title | Syntheses and characterization of different zinc(II) oxide nano-structures from direct thermal decomposition of 1D coordination polymers |
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