Influence of process parameters on the microstructure of laser printed NdFeB alloys
•Comprehensive characterization of Laser Printed 3D NdFeB magnets.•Correlation between laser parameters and solidification microstructure.•Identification of relevant crystallographic phases.•Improvement of magnetic properties by post fabrication heat treatments.•3D-printed NdFeB magnets (13.3 at.% R...
Gespeichert in:
| Veröffentlicht in: | Journal of magnetism and magnetic materials 2023-03, Vol.570, p.170503, Article 170503 |
|---|---|
| Hauptverfasser: | , , , , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | |
|---|---|
| container_issue | |
| container_start_page | 170503 |
| container_title | Journal of magnetism and magnetic materials |
| container_volume | 570 |
| creator | Caniou, Romain Rado, Cyril Gaillard, Gilles-Charles Tosoni, Olivier Flament, Camille Garandet, Jean-Paul |
| description | •Comprehensive characterization of Laser Printed 3D NdFeB magnets.•Correlation between laser parameters and solidification microstructure.•Identification of relevant crystallographic phases.•Improvement of magnetic properties by post fabrication heat treatments.•3D-printed NdFeB magnets (13.3 at.% RE) with HcJ = 551 kA/m and Br = 0.55 T.
In this study, a methodology, based on the realization of single-track beads to the elaboration of 3D parts, was implemented in order to understand the microstructure of the laser printed NdFeB permanent magnets. An homemade powder was used, and the microstructures of the elaborated samples were characterized. For 3D parts measurement of the magnetic properties with various heat treatments were also carried out. The results demonstrate the effect of the laser parameters on the microstructure, especially on iron nucleation and on the transition from columnar to equiaxed growth. After an optimized heat treatment, the printed magnets exhibit a coercivity HcJ = 551 kA/m, a remanence Br = 0.55 T and an energy product (BH)max = 38 kJ.m−3. |
| doi_str_mv | 10.1016/j.jmmm.2023.170503 |
| format | Article |
| fullrecord | <record><control><sourceid>hal_cross</sourceid><recordid>TN_cdi_hal_primary_oai_HAL_cea_04176850v1</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><els_id>S030488532300152X</els_id><sourcerecordid>oai_HAL_cea_04176850v1</sourcerecordid><originalsourceid>FETCH-LOGICAL-c285t-a00be5a28ccd5e6bce4ef14f456c96672d435d6def6dceab781b0199bbbc7d7a3</originalsourceid><addsrcrecordid>eNp9kD1PwzAURS0EEqXwB5i8MiQ8J47tSiylorRSBQMwW479oibKR2WnlfrvSQhiZHrLPVfvHkLuGcQMmHis4qppmjiBJI2ZhAzSCzJjSqYRl0JckhmkwCOlsvSa3IRQAQDjSszIx7Yt6iO2FmlX0IPvLIZAD8abBnv0gXYt7fdIm9L6LvT-aPuj_8nWJqAfiLLt0dE3t8Znauq6O4dbclWYOuDd752Tr_XL52oT7d5ft6vlLrKJyvrIAOSYmURZ6zIUuUWOBeMFz4RdCCETx9PMCYeFcBZNLhXLgS0WeZ5b6aRJ5-Rh6t2bWg-PNMafdWdKvVnu9EBo4EwKlcGJDdlkyo4zgsfiD2CgR4W60qNCPSrUk8IBepogHFacSvQ62HJ05UqPtteuK__DvwG35HuU</addsrcrecordid><sourcetype>Open Access Repository</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype></control><display><type>article</type><title>Influence of process parameters on the microstructure of laser printed NdFeB alloys</title><source>Elsevier ScienceDirect Journals Complete - AutoHoldings</source><creator>Caniou, Romain ; Rado, Cyril ; Gaillard, Gilles-Charles ; Tosoni, Olivier ; Flament, Camille ; Garandet, Jean-Paul</creator><creatorcontrib>Caniou, Romain ; Rado, Cyril ; Gaillard, Gilles-Charles ; Tosoni, Olivier ; Flament, Camille ; Garandet, Jean-Paul</creatorcontrib><description>•Comprehensive characterization of Laser Printed 3D NdFeB magnets.•Correlation between laser parameters and solidification microstructure.•Identification of relevant crystallographic phases.•Improvement of magnetic properties by post fabrication heat treatments.•3D-printed NdFeB magnets (13.3 at.% RE) with HcJ = 551 kA/m and Br = 0.55 T.
In this study, a methodology, based on the realization of single-track beads to the elaboration of 3D parts, was implemented in order to understand the microstructure of the laser printed NdFeB permanent magnets. An homemade powder was used, and the microstructures of the elaborated samples were characterized. For 3D parts measurement of the magnetic properties with various heat treatments were also carried out. The results demonstrate the effect of the laser parameters on the microstructure, especially on iron nucleation and on the transition from columnar to equiaxed growth. After an optimized heat treatment, the printed magnets exhibit a coercivity HcJ = 551 kA/m, a remanence Br = 0.55 T and an energy product (BH)max = 38 kJ.m−3.</description><identifier>ISSN: 0304-8853</identifier><identifier>EISSN: 1873-4766</identifier><identifier>DOI: 10.1016/j.jmmm.2023.170503</identifier><language>eng</language><publisher>Elsevier B.V</publisher><subject>Additive manufacturing ; Chemical Sciences ; Crystallographic phases ; Heat treatments ; Material chemistry ; NdFeB permanent magnets ; Solidification microstructure</subject><ispartof>Journal of magnetism and magnetic materials, 2023-03, Vol.570, p.170503, Article 170503</ispartof><rights>2023 Elsevier B.V.</rights><rights>Distributed under a Creative Commons Attribution 4.0 International License</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c285t-a00be5a28ccd5e6bce4ef14f456c96672d435d6def6dceab781b0199bbbc7d7a3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.jmmm.2023.170503$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>230,314,780,784,885,3550,27924,27925,45995</link.rule.ids><backlink>$$Uhttps://cea.hal.science/cea-04176850$$DView record in HAL$$Hfree_for_read</backlink></links><search><creatorcontrib>Caniou, Romain</creatorcontrib><creatorcontrib>Rado, Cyril</creatorcontrib><creatorcontrib>Gaillard, Gilles-Charles</creatorcontrib><creatorcontrib>Tosoni, Olivier</creatorcontrib><creatorcontrib>Flament, Camille</creatorcontrib><creatorcontrib>Garandet, Jean-Paul</creatorcontrib><title>Influence of process parameters on the microstructure of laser printed NdFeB alloys</title><title>Journal of magnetism and magnetic materials</title><description>•Comprehensive characterization of Laser Printed 3D NdFeB magnets.•Correlation between laser parameters and solidification microstructure.•Identification of relevant crystallographic phases.•Improvement of magnetic properties by post fabrication heat treatments.•3D-printed NdFeB magnets (13.3 at.% RE) with HcJ = 551 kA/m and Br = 0.55 T.
In this study, a methodology, based on the realization of single-track beads to the elaboration of 3D parts, was implemented in order to understand the microstructure of the laser printed NdFeB permanent magnets. An homemade powder was used, and the microstructures of the elaborated samples were characterized. For 3D parts measurement of the magnetic properties with various heat treatments were also carried out. The results demonstrate the effect of the laser parameters on the microstructure, especially on iron nucleation and on the transition from columnar to equiaxed growth. After an optimized heat treatment, the printed magnets exhibit a coercivity HcJ = 551 kA/m, a remanence Br = 0.55 T and an energy product (BH)max = 38 kJ.m−3.</description><subject>Additive manufacturing</subject><subject>Chemical Sciences</subject><subject>Crystallographic phases</subject><subject>Heat treatments</subject><subject>Material chemistry</subject><subject>NdFeB permanent magnets</subject><subject>Solidification microstructure</subject><issn>0304-8853</issn><issn>1873-4766</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><recordid>eNp9kD1PwzAURS0EEqXwB5i8MiQ8J47tSiylorRSBQMwW479oibKR2WnlfrvSQhiZHrLPVfvHkLuGcQMmHis4qppmjiBJI2ZhAzSCzJjSqYRl0JckhmkwCOlsvSa3IRQAQDjSszIx7Yt6iO2FmlX0IPvLIZAD8abBnv0gXYt7fdIm9L6LvT-aPuj_8nWJqAfiLLt0dE3t8Znauq6O4dbclWYOuDd752Tr_XL52oT7d5ft6vlLrKJyvrIAOSYmURZ6zIUuUWOBeMFz4RdCCETx9PMCYeFcBZNLhXLgS0WeZ5b6aRJ5-Rh6t2bWg-PNMafdWdKvVnu9EBo4EwKlcGJDdlkyo4zgsfiD2CgR4W60qNCPSrUk8IBepogHFacSvQ62HJ05UqPtteuK__DvwG35HuU</recordid><startdate>20230315</startdate><enddate>20230315</enddate><creator>Caniou, Romain</creator><creator>Rado, Cyril</creator><creator>Gaillard, Gilles-Charles</creator><creator>Tosoni, Olivier</creator><creator>Flament, Camille</creator><creator>Garandet, Jean-Paul</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>AAYXX</scope><scope>CITATION</scope><scope>1XC</scope><scope>VOOES</scope></search><sort><creationdate>20230315</creationdate><title>Influence of process parameters on the microstructure of laser printed NdFeB alloys</title><author>Caniou, Romain ; Rado, Cyril ; Gaillard, Gilles-Charles ; Tosoni, Olivier ; Flament, Camille ; Garandet, Jean-Paul</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c285t-a00be5a28ccd5e6bce4ef14f456c96672d435d6def6dceab781b0199bbbc7d7a3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2023</creationdate><topic>Additive manufacturing</topic><topic>Chemical Sciences</topic><topic>Crystallographic phases</topic><topic>Heat treatments</topic><topic>Material chemistry</topic><topic>NdFeB permanent magnets</topic><topic>Solidification microstructure</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Caniou, Romain</creatorcontrib><creatorcontrib>Rado, Cyril</creatorcontrib><creatorcontrib>Gaillard, Gilles-Charles</creatorcontrib><creatorcontrib>Tosoni, Olivier</creatorcontrib><creatorcontrib>Flament, Camille</creatorcontrib><creatorcontrib>Garandet, Jean-Paul</creatorcontrib><collection>CrossRef</collection><collection>Hyper Article en Ligne (HAL)</collection><collection>Hyper Article en Ligne (HAL) (Open Access)</collection><jtitle>Journal of magnetism and magnetic materials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Caniou, Romain</au><au>Rado, Cyril</au><au>Gaillard, Gilles-Charles</au><au>Tosoni, Olivier</au><au>Flament, Camille</au><au>Garandet, Jean-Paul</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Influence of process parameters on the microstructure of laser printed NdFeB alloys</atitle><jtitle>Journal of magnetism and magnetic materials</jtitle><date>2023-03-15</date><risdate>2023</risdate><volume>570</volume><spage>170503</spage><pages>170503-</pages><artnum>170503</artnum><issn>0304-8853</issn><eissn>1873-4766</eissn><abstract>•Comprehensive characterization of Laser Printed 3D NdFeB magnets.•Correlation between laser parameters and solidification microstructure.•Identification of relevant crystallographic phases.•Improvement of magnetic properties by post fabrication heat treatments.•3D-printed NdFeB magnets (13.3 at.% RE) with HcJ = 551 kA/m and Br = 0.55 T.
In this study, a methodology, based on the realization of single-track beads to the elaboration of 3D parts, was implemented in order to understand the microstructure of the laser printed NdFeB permanent magnets. An homemade powder was used, and the microstructures of the elaborated samples were characterized. For 3D parts measurement of the magnetic properties with various heat treatments were also carried out. The results demonstrate the effect of the laser parameters on the microstructure, especially on iron nucleation and on the transition from columnar to equiaxed growth. After an optimized heat treatment, the printed magnets exhibit a coercivity HcJ = 551 kA/m, a remanence Br = 0.55 T and an energy product (BH)max = 38 kJ.m−3.</abstract><pub>Elsevier B.V</pub><doi>10.1016/j.jmmm.2023.170503</doi><oa>free_for_read</oa></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0304-8853 |
| ispartof | Journal of magnetism and magnetic materials, 2023-03, Vol.570, p.170503, Article 170503 |
| issn | 0304-8853 1873-4766 |
| language | eng |
| recordid | cdi_hal_primary_oai_HAL_cea_04176850v1 |
| source | Elsevier ScienceDirect Journals Complete - AutoHoldings |
| subjects | Additive manufacturing Chemical Sciences Crystallographic phases Heat treatments Material chemistry NdFeB permanent magnets Solidification microstructure |
| title | Influence of process parameters on the microstructure of laser printed NdFeB alloys |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-08T03%3A57%3A11IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-hal_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Influence%20of%20process%20parameters%20on%20the%20microstructure%20of%20laser%20printed%20NdFeB%20alloys&rft.jtitle=Journal%20of%20magnetism%20and%20magnetic%20materials&rft.au=Caniou,%20Romain&rft.date=2023-03-15&rft.volume=570&rft.spage=170503&rft.pages=170503-&rft.artnum=170503&rft.issn=0304-8853&rft.eissn=1873-4766&rft_id=info:doi/10.1016/j.jmmm.2023.170503&rft_dat=%3Chal_cross%3Eoai_HAL_cea_04176850v1%3C/hal_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_id=info:pmid/&rft_els_id=S030488532300152X&rfr_iscdi=true |