Structural and Morphological Studies of V[sub.2]O[sub.5]/MWCNTs and ZrO[sub.2]/MWCNTs Composites as Photocatalysts
The present study outlines the synthesis of transition metal oxide- (TMO-) multiwall carbon nanotubes- (MWCNTs-) based composites for photocatalytic application. MWCNTs were functionalized/purified by treating with H[sub.2]SO[sub.4] and HNO[sub.3] to improve their dispersion in water. The TMOs (ZrO[...
Gespeichert in:
Veröffentlicht in: | Journal of chemistry 2021-05, Vol.2021 |
---|---|
Hauptverfasser: | , , , , , |
Format: | Artikel |
Sprache: | eng |
Schlagworte: | |
Online-Zugang: | Volltext |
Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
container_end_page | |
---|---|
container_issue | |
container_start_page | |
container_title | Journal of chemistry |
container_volume | 2021 |
creator | Iqbal, Sajid Bokhari, Tanveer Hussain Latif, Shoomaila Imran, Muhammad Javaid, Ayesha Mitu, Liviu |
description | The present study outlines the synthesis of transition metal oxide- (TMO-) multiwall carbon nanotubes- (MWCNTs-) based composites for photocatalytic application. MWCNTs were functionalized/purified by treating with H[sub.2]SO[sub.4] and HNO[sub.3] to improve their dispersion in water. The TMOs (ZrO[sub.2], V[sub.2]O[sub.5]) were decorated on MWCNTs by the hydrothermal method to yield V[sub.2]O[sub.5]/MWCNTs and ZrO[sub.2]/MWCNTs composites. Subsequently, these composites were characterized for their structural/morphological studies by Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD), and scanning electron microscopy (SEM). Photocatalytic activities of TMO/MWCNTs composites were investigated by degradation phenomenon of methylene blue (MB) dye in aqueous solution. It was observed that the prepared composites best performed in the presence of H[sub.2]O[sub.2] under ultraviolet irradiation. The maximum observed degradation efficiencies for ZrO[sub.2]/MWCNTs and V[sub.2]O[sub.5]/MWCNTs were 49% and 96%, respectively. |
doi_str_mv | 10.1155/2021/9922726 |
format | Article |
fullrecord | <record><control><sourceid>gale</sourceid><recordid>TN_cdi_gale_infotracmisc_A814734188</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><galeid>A814734188</galeid><sourcerecordid>A814734188</sourcerecordid><originalsourceid>FETCH-LOGICAL-g678-4e3d1341321d858d72354b5568b2cc78263a96cd6494bda412536c9bd387de3b3</originalsourceid><addsrcrecordid>eNptkEtLAzEUhbNQsNTu_AEDrqedvJNlGXxBa4UOCkopmSQzjUybMsks_PeGWsGF9y4OfPeeszgA3MBiCiGlM1QgOJMSIY7YBRihQha5LBi-ApMQPos0QmCK-Aj069gPOg696jJ1MNnS98ed73zrdCLrOBhnQ-ab7PUjDPUUbVYnpZvZ8q18rsLJ9N6vztdfWvr90QcXk1eF7GXno9cqqu4rxHANLhvVBTs56xhU93dV-ZgvVg9P5XyRt4yLnFhsICYQI2gEFYYjTElNKRM10poLxLCSTBtGJKmNIhBRzLSsDRbcWFzjMbj9iW1VZ7fu0PjYK713QW_nAhKeslMJYzD95yutsXun_cE2LvE_hm8h2miS</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype></control><display><type>article</type><title>Structural and Morphological Studies of V[sub.2]O[sub.5]/MWCNTs and ZrO[sub.2]/MWCNTs Composites as Photocatalysts</title><source>DOAJ Directory of Open Access Journals</source><source>EZB-FREE-00999 freely available EZB journals</source><source>Wiley Online Library (Open Access Collection)</source><source>Alma/SFX Local Collection</source><source>Free Full-Text Journals in Chemistry</source><creator>Iqbal, Sajid ; Bokhari, Tanveer Hussain ; Latif, Shoomaila ; Imran, Muhammad ; Javaid, Ayesha ; Mitu, Liviu</creator><creatorcontrib>Iqbal, Sajid ; Bokhari, Tanveer Hussain ; Latif, Shoomaila ; Imran, Muhammad ; Javaid, Ayesha ; Mitu, Liviu</creatorcontrib><description>The present study outlines the synthesis of transition metal oxide- (TMO-) multiwall carbon nanotubes- (MWCNTs-) based composites for photocatalytic application. MWCNTs were functionalized/purified by treating with H[sub.2]SO[sub.4] and HNO[sub.3] to improve their dispersion in water. The TMOs (ZrO[sub.2], V[sub.2]O[sub.5]) were decorated on MWCNTs by the hydrothermal method to yield V[sub.2]O[sub.5]/MWCNTs and ZrO[sub.2]/MWCNTs composites. Subsequently, these composites were characterized for their structural/morphological studies by Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD), and scanning electron microscopy (SEM). Photocatalytic activities of TMO/MWCNTs composites were investigated by degradation phenomenon of methylene blue (MB) dye in aqueous solution. It was observed that the prepared composites best performed in the presence of H[sub.2]O[sub.2] under ultraviolet irradiation. The maximum observed degradation efficiencies for ZrO[sub.2]/MWCNTs and V[sub.2]O[sub.5]/MWCNTs were 49% and 96%, respectively.</description><identifier>ISSN: 2090-9063</identifier><identifier>DOI: 10.1155/2021/9922726</identifier><language>eng</language><publisher>John Wiley & Sons, Inc</publisher><subject>Diffraction ; Infrared spectroscopy ; Methylene blue ; Nanotubes ; Transition metal compounds ; X-rays</subject><ispartof>Journal of chemistry, 2021-05, Vol.2021</ispartof><rights>COPYRIGHT 2021 John Wiley & Sons, Inc.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,864,27924,27925</link.rule.ids></links><search><creatorcontrib>Iqbal, Sajid</creatorcontrib><creatorcontrib>Bokhari, Tanveer Hussain</creatorcontrib><creatorcontrib>Latif, Shoomaila</creatorcontrib><creatorcontrib>Imran, Muhammad</creatorcontrib><creatorcontrib>Javaid, Ayesha</creatorcontrib><creatorcontrib>Mitu, Liviu</creatorcontrib><title>Structural and Morphological Studies of V[sub.2]O[sub.5]/MWCNTs and ZrO[sub.2]/MWCNTs Composites as Photocatalysts</title><title>Journal of chemistry</title><description>The present study outlines the synthesis of transition metal oxide- (TMO-) multiwall carbon nanotubes- (MWCNTs-) based composites for photocatalytic application. MWCNTs were functionalized/purified by treating with H[sub.2]SO[sub.4] and HNO[sub.3] to improve their dispersion in water. The TMOs (ZrO[sub.2], V[sub.2]O[sub.5]) were decorated on MWCNTs by the hydrothermal method to yield V[sub.2]O[sub.5]/MWCNTs and ZrO[sub.2]/MWCNTs composites. Subsequently, these composites were characterized for their structural/morphological studies by Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD), and scanning electron microscopy (SEM). Photocatalytic activities of TMO/MWCNTs composites were investigated by degradation phenomenon of methylene blue (MB) dye in aqueous solution. It was observed that the prepared composites best performed in the presence of H[sub.2]O[sub.2] under ultraviolet irradiation. The maximum observed degradation efficiencies for ZrO[sub.2]/MWCNTs and V[sub.2]O[sub.5]/MWCNTs were 49% and 96%, respectively.</description><subject>Diffraction</subject><subject>Infrared spectroscopy</subject><subject>Methylene blue</subject><subject>Nanotubes</subject><subject>Transition metal compounds</subject><subject>X-rays</subject><issn>2090-9063</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2021</creationdate><recordtype>article</recordtype><sourceid/><recordid>eNptkEtLAzEUhbNQsNTu_AEDrqedvJNlGXxBa4UOCkopmSQzjUybMsks_PeGWsGF9y4OfPeeszgA3MBiCiGlM1QgOJMSIY7YBRihQha5LBi-ApMQPos0QmCK-Aj069gPOg696jJ1MNnS98ed73zrdCLrOBhnQ-ab7PUjDPUUbVYnpZvZ8q18rsLJ9N6vztdfWvr90QcXk1eF7GXno9cqqu4rxHANLhvVBTs56xhU93dV-ZgvVg9P5XyRt4yLnFhsICYQI2gEFYYjTElNKRM10poLxLCSTBtGJKmNIhBRzLSsDRbcWFzjMbj9iW1VZ7fu0PjYK713QW_nAhKeslMJYzD95yutsXun_cE2LvE_hm8h2miS</recordid><startdate>20210518</startdate><enddate>20210518</enddate><creator>Iqbal, Sajid</creator><creator>Bokhari, Tanveer Hussain</creator><creator>Latif, Shoomaila</creator><creator>Imran, Muhammad</creator><creator>Javaid, Ayesha</creator><creator>Mitu, Liviu</creator><general>John Wiley & Sons, Inc</general><scope/></search><sort><creationdate>20210518</creationdate><title>Structural and Morphological Studies of V[sub.2]O[sub.5]/MWCNTs and ZrO[sub.2]/MWCNTs Composites as Photocatalysts</title><author>Iqbal, Sajid ; Bokhari, Tanveer Hussain ; Latif, Shoomaila ; Imran, Muhammad ; Javaid, Ayesha ; Mitu, Liviu</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-g678-4e3d1341321d858d72354b5568b2cc78263a96cd6494bda412536c9bd387de3b3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2021</creationdate><topic>Diffraction</topic><topic>Infrared spectroscopy</topic><topic>Methylene blue</topic><topic>Nanotubes</topic><topic>Transition metal compounds</topic><topic>X-rays</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Iqbal, Sajid</creatorcontrib><creatorcontrib>Bokhari, Tanveer Hussain</creatorcontrib><creatorcontrib>Latif, Shoomaila</creatorcontrib><creatorcontrib>Imran, Muhammad</creatorcontrib><creatorcontrib>Javaid, Ayesha</creatorcontrib><creatorcontrib>Mitu, Liviu</creatorcontrib><jtitle>Journal of chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Iqbal, Sajid</au><au>Bokhari, Tanveer Hussain</au><au>Latif, Shoomaila</au><au>Imran, Muhammad</au><au>Javaid, Ayesha</au><au>Mitu, Liviu</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Structural and Morphological Studies of V[sub.2]O[sub.5]/MWCNTs and ZrO[sub.2]/MWCNTs Composites as Photocatalysts</atitle><jtitle>Journal of chemistry</jtitle><date>2021-05-18</date><risdate>2021</risdate><volume>2021</volume><issn>2090-9063</issn><abstract>The present study outlines the synthesis of transition metal oxide- (TMO-) multiwall carbon nanotubes- (MWCNTs-) based composites for photocatalytic application. MWCNTs were functionalized/purified by treating with H[sub.2]SO[sub.4] and HNO[sub.3] to improve their dispersion in water. The TMOs (ZrO[sub.2], V[sub.2]O[sub.5]) were decorated on MWCNTs by the hydrothermal method to yield V[sub.2]O[sub.5]/MWCNTs and ZrO[sub.2]/MWCNTs composites. Subsequently, these composites were characterized for their structural/morphological studies by Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD), and scanning electron microscopy (SEM). Photocatalytic activities of TMO/MWCNTs composites were investigated by degradation phenomenon of methylene blue (MB) dye in aqueous solution. It was observed that the prepared composites best performed in the presence of H[sub.2]O[sub.2] under ultraviolet irradiation. The maximum observed degradation efficiencies for ZrO[sub.2]/MWCNTs and V[sub.2]O[sub.5]/MWCNTs were 49% and 96%, respectively.</abstract><pub>John Wiley & Sons, Inc</pub><doi>10.1155/2021/9922726</doi></addata></record> |
fulltext | fulltext |
identifier | ISSN: 2090-9063 |
ispartof | Journal of chemistry, 2021-05, Vol.2021 |
issn | 2090-9063 |
language | eng |
recordid | cdi_gale_infotracmisc_A814734188 |
source | DOAJ Directory of Open Access Journals; EZB-FREE-00999 freely available EZB journals; Wiley Online Library (Open Access Collection); Alma/SFX Local Collection; Free Full-Text Journals in Chemistry |
subjects | Diffraction Infrared spectroscopy Methylene blue Nanotubes Transition metal compounds X-rays |
title | Structural and Morphological Studies of V[sub.2]O[sub.5]/MWCNTs and ZrO[sub.2]/MWCNTs Composites as Photocatalysts |
url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2024-12-29T15%3A08%3A12IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-gale&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Structural%20and%20Morphological%20Studies%20of%20V%5Bsub.2%5DO%5Bsub.5%5D/MWCNTs%20and%20ZrO%5Bsub.2%5D/MWCNTs%20Composites%20as%20Photocatalysts&rft.jtitle=Journal%20of%20chemistry&rft.au=Iqbal,%20Sajid&rft.date=2021-05-18&rft.volume=2021&rft.issn=2090-9063&rft_id=info:doi/10.1155/2021/9922726&rft_dat=%3Cgale%3EA814734188%3C/gale%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_id=info:pmid/&rft_galeid=A814734188&rfr_iscdi=true |