TiO.sub.2@ZnO nanocomposite: bifunctional material for solid phase extraction of U and photocatalytic degradation of organic contaminant
A bifunctional TiO.sub.2@ZnO nanorods hybrid material was synthesized via one-step hydrothermal synthesis and studied as an adsorbent for SPE of U(VI) and Th(IV) and as a photocatalyst for the photocatalytic removal of methylene blue (MB). The formation of TiO.sub.2@ZnO hybrid composite was confirme...
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Veröffentlicht in: | Journal of radioanalytical and nuclear chemistry 2023-10, Vol.332 (10), p.3879 |
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container_title | Journal of radioanalytical and nuclear chemistry |
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creator | Aydin, Funda Yilmaz, Erkan Demirkiran, Gülay Erbas, Zeliha Vurucuel, Merve Soylak, Mustafa |
description | A bifunctional TiO.sub.2@ZnO nanorods hybrid material was synthesized via one-step hydrothermal synthesis and studied as an adsorbent for SPE of U(VI) and Th(IV) and as a photocatalyst for the photocatalytic removal of methylene blue (MB). The formation of TiO.sub.2@ZnO hybrid composite was confirmed by XRD, Raman, SEM, SEM-EDX and SEM-Mapping analysis. After determining the optimum values of the analytical parameters affecting the recovery of the analytes, the developed TiO.sub.2@ZnO hybrid NPs-SPE method was applied to natural waters with a high recovery efficiency (94-97%). The accuracy of the method was also verified by using CRM-TMDA 62.2 and TM-25.3 standards. Photocatalytic properties of the fabricated nanocomposite were investigated by degrading of MB under UV light. The results indicated that the synthesized TiO.sub.2@ZnO material can be used as a promising adsorbent/photocatalyst candidate for the adsorption of U(VI) and Th(IV) analytes in waters as well as the photocatalysis degradation of MB dyestuff. |
doi_str_mv | 10.1007/s10967-023-09082-1 |
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The formation of TiO.sub.2@ZnO hybrid composite was confirmed by XRD, Raman, SEM, SEM-EDX and SEM-Mapping analysis. After determining the optimum values of the analytical parameters affecting the recovery of the analytes, the developed TiO.sub.2@ZnO hybrid NPs-SPE method was applied to natural waters with a high recovery efficiency (94-97%). The accuracy of the method was also verified by using CRM-TMDA 62.2 and TM-25.3 standards. Photocatalytic properties of the fabricated nanocomposite were investigated by degrading of MB under UV light. The results indicated that the synthesized TiO.sub.2@ZnO material can be used as a promising adsorbent/photocatalyst candidate for the adsorption of U(VI) and Th(IV) analytes in waters as well as the photocatalysis degradation of MB dyestuff.</description><identifier>ISSN: 0236-5731</identifier><identifier>DOI: 10.1007/s10967-023-09082-1</identifier><language>eng</language><publisher>Springer</publisher><subject>Adsorption ; Analysis ; Methylene blue ; Zinc oxide</subject><ispartof>Journal of radioanalytical and nuclear chemistry, 2023-10, Vol.332 (10), p.3879</ispartof><rights>COPYRIGHT 2023 Springer</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27924,27925</link.rule.ids></links><search><creatorcontrib>Aydin, Funda</creatorcontrib><creatorcontrib>Yilmaz, Erkan</creatorcontrib><creatorcontrib>Demirkiran, Gülay</creatorcontrib><creatorcontrib>Erbas, Zeliha</creatorcontrib><creatorcontrib>Vurucuel, Merve</creatorcontrib><creatorcontrib>Soylak, Mustafa</creatorcontrib><title>TiO.sub.2@ZnO nanocomposite: bifunctional material for solid phase extraction of U and photocatalytic degradation of organic contaminant</title><title>Journal of radioanalytical and nuclear chemistry</title><description>A bifunctional TiO.sub.2@ZnO nanorods hybrid material was synthesized via one-step hydrothermal synthesis and studied as an adsorbent for SPE of U(VI) and Th(IV) and as a photocatalyst for the photocatalytic removal of methylene blue (MB). The formation of TiO.sub.2@ZnO hybrid composite was confirmed by XRD, Raman, SEM, SEM-EDX and SEM-Mapping analysis. After determining the optimum values of the analytical parameters affecting the recovery of the analytes, the developed TiO.sub.2@ZnO hybrid NPs-SPE method was applied to natural waters with a high recovery efficiency (94-97%). The accuracy of the method was also verified by using CRM-TMDA 62.2 and TM-25.3 standards. Photocatalytic properties of the fabricated nanocomposite were investigated by degrading of MB under UV light. The results indicated that the synthesized TiO.sub.2@ZnO material can be used as a promising adsorbent/photocatalyst candidate for the adsorption of U(VI) and Th(IV) analytes in waters as well as the photocatalysis degradation of MB dyestuff.</description><subject>Adsorption</subject><subject>Analysis</subject><subject>Methylene blue</subject><subject>Zinc oxide</subject><issn>0236-5731</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><sourceid/><recordid>eNptjk1PwzAMhnMAiTH4A5wicW5xki5pOTFNfEmTdhkXLpObjxHUJlOTSfAP-Nl0fEgckA-2Xz-2X0IuGJQMQF0lBo1UBXBRQAM1L9gRmYydLGZKsBNymtIrADR1LSbkY-1XZdq3Jb95DisaMEQd-11MPttr2nq3Dzr7GLCjPWY7-LFwcaApdt7Q3QsmS-1bHvCLotHRJ4rhMIk5aszYvWevqbHbAQ3-MnHYYhhlHUPG3o9f8xk5dtgle_6Tp2R9d7tePBTL1f3jYr4stlJBoYBpqVtn3KwRSrpaa6cq5VqwEhXohhvFHHe8ZbqyRtTguGiNrSqBTlgrpuTy--wWO7vxwcWD994nvZkrWQvJZwpGqvyHGsPY3o-mrfOj_mfhE74WdTY</recordid><startdate>20231001</startdate><enddate>20231001</enddate><creator>Aydin, Funda</creator><creator>Yilmaz, Erkan</creator><creator>Demirkiran, Gülay</creator><creator>Erbas, Zeliha</creator><creator>Vurucuel, Merve</creator><creator>Soylak, Mustafa</creator><general>Springer</general><scope/></search><sort><creationdate>20231001</creationdate><title>TiO.sub.2@ZnO nanocomposite: bifunctional material for solid phase extraction of U and photocatalytic degradation of organic contaminant</title><author>Aydin, Funda ; Yilmaz, Erkan ; Demirkiran, Gülay ; Erbas, Zeliha ; Vurucuel, Merve ; Soylak, Mustafa</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-g670-701c6cbfdf59376f8ccf747fb0e6a70c92d71f2f2b1c4ed380f23bde443af3ee3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2023</creationdate><topic>Adsorption</topic><topic>Analysis</topic><topic>Methylene blue</topic><topic>Zinc oxide</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Aydin, Funda</creatorcontrib><creatorcontrib>Yilmaz, Erkan</creatorcontrib><creatorcontrib>Demirkiran, Gülay</creatorcontrib><creatorcontrib>Erbas, Zeliha</creatorcontrib><creatorcontrib>Vurucuel, Merve</creatorcontrib><creatorcontrib>Soylak, Mustafa</creatorcontrib><jtitle>Journal of radioanalytical and nuclear chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Aydin, Funda</au><au>Yilmaz, Erkan</au><au>Demirkiran, Gülay</au><au>Erbas, Zeliha</au><au>Vurucuel, Merve</au><au>Soylak, Mustafa</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>TiO.sub.2@ZnO nanocomposite: bifunctional material for solid phase extraction of U and photocatalytic degradation of organic contaminant</atitle><jtitle>Journal of radioanalytical and nuclear chemistry</jtitle><date>2023-10-01</date><risdate>2023</risdate><volume>332</volume><issue>10</issue><spage>3879</spage><pages>3879-</pages><issn>0236-5731</issn><abstract>A bifunctional TiO.sub.2@ZnO nanorods hybrid material was synthesized via one-step hydrothermal synthesis and studied as an adsorbent for SPE of U(VI) and Th(IV) and as a photocatalyst for the photocatalytic removal of methylene blue (MB). The formation of TiO.sub.2@ZnO hybrid composite was confirmed by XRD, Raman, SEM, SEM-EDX and SEM-Mapping analysis. After determining the optimum values of the analytical parameters affecting the recovery of the analytes, the developed TiO.sub.2@ZnO hybrid NPs-SPE method was applied to natural waters with a high recovery efficiency (94-97%). The accuracy of the method was also verified by using CRM-TMDA 62.2 and TM-25.3 standards. Photocatalytic properties of the fabricated nanocomposite were investigated by degrading of MB under UV light. The results indicated that the synthesized TiO.sub.2@ZnO material can be used as a promising adsorbent/photocatalyst candidate for the adsorption of U(VI) and Th(IV) analytes in waters as well as the photocatalysis degradation of MB dyestuff.</abstract><pub>Springer</pub><doi>10.1007/s10967-023-09082-1</doi></addata></record> |
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subjects | Adsorption Analysis Methylene blue Zinc oxide |
title | TiO.sub.2@ZnO nanocomposite: bifunctional material for solid phase extraction of U and photocatalytic degradation of organic contaminant |
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