A Novel Approach for Fabricating LaMN[O.sub.3] Thin Films Using Combined Microwave Combustion and Pulsed Electron Deposition Techniques
LaMn[O.sub.3] (LMO) nanopowder was synthesized by the microwave combustion method using glycine and nitrate salts of La and Mn as precursors. The as-prepared LMO powder was pressed at high pressure and annealed at 1000[degrees]C for 8 hours to make a target for thin film deposition. The structural a...
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| Veröffentlicht in: | Journal of chemistry 2019-03, Vol.2019 |
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| container_title | Journal of chemistry |
| container_volume | 2019 |
| creator | Tran, Thi Ha Tang, Thi Trung Anh Pham, Nguyen Hai Bach, Thanh Cong Sai, Cong Doanh Nguyen, Quang Hoa Le, Van Vu Nguyen, Hoang Nam Doan, Quoc Khoa Nguyen, Trong Tam Le, Viet Bau Ho, Khac Hieu Nguyen, Viet Tuyen |
| description | LaMn[O.sub.3] (LMO) nanopowder was synthesized by the microwave combustion method using glycine and nitrate salts of La and Mn as precursors. The as-prepared LMO powder was pressed at high pressure and annealed at 1000[degrees]C for 8 hours to make a target for thin film deposition. The structural and elemental analysis was obtained by X-ray diffraction (XRD) and energy dispersive X-ray spectroscopy (EDS). Thin films of LMO were fabricated using pulsed electron deposition (PED) at room temperature. The effects of discharge voltage and oxygen/argon flux ratio on the produced thin films were studied. The study shows that stoichiometry and structure of the target was preserved well in the thin films prepared with a discharge voltage from 14 to 15 kV, while the oxygen/ nitrogen flux ratio did not show a clear effect on the quality of thin films. |
| doi_str_mv | 10.1155/2019/3568185 |
| format | Article |
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The as-prepared LMO powder was pressed at high pressure and annealed at 1000[degrees]C for 8 hours to make a target for thin film deposition. The structural and elemental analysis was obtained by X-ray diffraction (XRD) and energy dispersive X-ray spectroscopy (EDS). Thin films of LMO were fabricated using pulsed electron deposition (PED) at room temperature. The effects of discharge voltage and oxygen/argon flux ratio on the produced thin films were studied. The study shows that stoichiometry and structure of the target was preserved well in the thin films prepared with a discharge voltage from 14 to 15 kV, while the oxygen/ nitrogen flux ratio did not show a clear effect on the quality of thin films.</description><identifier>ISSN: 2090-9063</identifier><identifier>DOI: 10.1155/2019/3568185</identifier><language>eng</language><publisher>John Wiley & Sons, Inc</publisher><subject>Analysis ; Combustion ; Dielectric films ; Diffraction ; Glycine ; Methods ; Thin films ; X-ray spectroscopy ; X-rays</subject><ispartof>Journal of chemistry, 2019-03, Vol.2019</ispartof><rights>COPYRIGHT 2019 John Wiley & Sons, Inc.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,864,27924,27925</link.rule.ids></links><search><creatorcontrib>Tran, Thi Ha</creatorcontrib><creatorcontrib>Tang, Thi Trung Anh</creatorcontrib><creatorcontrib>Pham, Nguyen Hai</creatorcontrib><creatorcontrib>Bach, Thanh Cong</creatorcontrib><creatorcontrib>Sai, Cong Doanh</creatorcontrib><creatorcontrib>Nguyen, Quang Hoa</creatorcontrib><creatorcontrib>Le, Van Vu</creatorcontrib><creatorcontrib>Nguyen, Hoang Nam</creatorcontrib><creatorcontrib>Doan, Quoc Khoa</creatorcontrib><creatorcontrib>Nguyen, Trong Tam</creatorcontrib><creatorcontrib>Le, Viet Bau</creatorcontrib><creatorcontrib>Ho, Khac Hieu</creatorcontrib><creatorcontrib>Nguyen, Viet Tuyen</creatorcontrib><title>A Novel Approach for Fabricating LaMN[O.sub.3] Thin Films Using Combined Microwave Combustion and Pulsed Electron Deposition Techniques</title><title>Journal of chemistry</title><description>LaMn[O.sub.3] (LMO) nanopowder was synthesized by the microwave combustion method using glycine and nitrate salts of La and Mn as precursors. The as-prepared LMO powder was pressed at high pressure and annealed at 1000[degrees]C for 8 hours to make a target for thin film deposition. The structural and elemental analysis was obtained by X-ray diffraction (XRD) and energy dispersive X-ray spectroscopy (EDS). Thin films of LMO were fabricated using pulsed electron deposition (PED) at room temperature. The effects of discharge voltage and oxygen/argon flux ratio on the produced thin films were studied. The study shows that stoichiometry and structure of the target was preserved well in the thin films prepared with a discharge voltage from 14 to 15 kV, while the oxygen/ nitrogen flux ratio did not show a clear effect on the quality of thin films.</description><subject>Analysis</subject><subject>Combustion</subject><subject>Dielectric films</subject><subject>Diffraction</subject><subject>Glycine</subject><subject>Methods</subject><subject>Thin films</subject><subject>X-ray spectroscopy</subject><subject>X-rays</subject><issn>2090-9063</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2019</creationdate><recordtype>article</recordtype><sourceid/><recordid>eNptj7FOwzAQhj2ARFW68QCWmJM6duw4Y1RaQGoLQ5gQqhzn3BoldonT8gi8NmlhYOBuOOn7_jvpELpJSJwknE8pSfIp40Imkl-gESU5iXIi2BWahPBOhpKScZqN0FeB1_4IDS72-84rvcPGd3ihqs5q1Vu3xUu1Wr8-xeFQxewNlzvr8MI2bcAv4aRnvq2sgxqvrO78pzrCGR1Cb73DytX4-dCEwc8b0H03sDvY-2DPugS9c_bjAOEaXRo15Ca_c4zKxbycPUTLp_vHWbGMtiLjUWpS4DQHLfLMUADIRMpqnlJZV7WsBBOiSoiSmaSKMJEzoYyQw-daVyw1nI3R7c_ZrWpgY53xfad0a4PeFIIynjEuT6n4n9TQNbRWewfGDvzPwjeZv3D2</recordid><startdate>20190331</startdate><enddate>20190331</enddate><creator>Tran, Thi Ha</creator><creator>Tang, Thi Trung Anh</creator><creator>Pham, Nguyen Hai</creator><creator>Bach, Thanh Cong</creator><creator>Sai, Cong Doanh</creator><creator>Nguyen, Quang Hoa</creator><creator>Le, Van Vu</creator><creator>Nguyen, Hoang Nam</creator><creator>Doan, Quoc Khoa</creator><creator>Nguyen, Trong Tam</creator><creator>Le, Viet Bau</creator><creator>Ho, Khac Hieu</creator><creator>Nguyen, Viet Tuyen</creator><general>John Wiley & Sons, Inc</general><scope/></search><sort><creationdate>20190331</creationdate><title>A Novel Approach for Fabricating LaMN[O.sub.3] Thin Films Using Combined Microwave Combustion and Pulsed Electron Deposition Techniques</title><author>Tran, Thi Ha ; Tang, Thi Trung Anh ; Pham, Nguyen Hai ; Bach, Thanh Cong ; Sai, Cong Doanh ; Nguyen, Quang Hoa ; Le, Van Vu ; Nguyen, Hoang Nam ; Doan, Quoc Khoa ; Nguyen, Trong Tam ; Le, Viet Bau ; Ho, Khac Hieu ; Nguyen, Viet Tuyen</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-g675-4f4e529ec697f2eee7643d5428dbd8b6366b10a8782a036936af68906ccb34f53</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2019</creationdate><topic>Analysis</topic><topic>Combustion</topic><topic>Dielectric films</topic><topic>Diffraction</topic><topic>Glycine</topic><topic>Methods</topic><topic>Thin films</topic><topic>X-ray spectroscopy</topic><topic>X-rays</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Tran, Thi Ha</creatorcontrib><creatorcontrib>Tang, Thi Trung Anh</creatorcontrib><creatorcontrib>Pham, Nguyen Hai</creatorcontrib><creatorcontrib>Bach, Thanh Cong</creatorcontrib><creatorcontrib>Sai, Cong Doanh</creatorcontrib><creatorcontrib>Nguyen, Quang Hoa</creatorcontrib><creatorcontrib>Le, Van Vu</creatorcontrib><creatorcontrib>Nguyen, Hoang Nam</creatorcontrib><creatorcontrib>Doan, Quoc Khoa</creatorcontrib><creatorcontrib>Nguyen, Trong Tam</creatorcontrib><creatorcontrib>Le, Viet Bau</creatorcontrib><creatorcontrib>Ho, Khac Hieu</creatorcontrib><creatorcontrib>Nguyen, Viet Tuyen</creatorcontrib><jtitle>Journal of chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Tran, Thi Ha</au><au>Tang, Thi Trung Anh</au><au>Pham, Nguyen Hai</au><au>Bach, Thanh Cong</au><au>Sai, Cong Doanh</au><au>Nguyen, Quang Hoa</au><au>Le, Van Vu</au><au>Nguyen, Hoang Nam</au><au>Doan, Quoc Khoa</au><au>Nguyen, Trong Tam</au><au>Le, Viet Bau</au><au>Ho, Khac Hieu</au><au>Nguyen, Viet Tuyen</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>A Novel Approach for Fabricating LaMN[O.sub.3] Thin Films Using Combined Microwave Combustion and Pulsed Electron Deposition Techniques</atitle><jtitle>Journal of chemistry</jtitle><date>2019-03-31</date><risdate>2019</risdate><volume>2019</volume><issn>2090-9063</issn><abstract>LaMn[O.sub.3] (LMO) nanopowder was synthesized by the microwave combustion method using glycine and nitrate salts of La and Mn as precursors. The as-prepared LMO powder was pressed at high pressure and annealed at 1000[degrees]C for 8 hours to make a target for thin film deposition. The structural and elemental analysis was obtained by X-ray diffraction (XRD) and energy dispersive X-ray spectroscopy (EDS). Thin films of LMO were fabricated using pulsed electron deposition (PED) at room temperature. The effects of discharge voltage and oxygen/argon flux ratio on the produced thin films were studied. The study shows that stoichiometry and structure of the target was preserved well in the thin films prepared with a discharge voltage from 14 to 15 kV, while the oxygen/ nitrogen flux ratio did not show a clear effect on the quality of thin films.</abstract><pub>John Wiley & Sons, Inc</pub><doi>10.1155/2019/3568185</doi></addata></record> |
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| source | DOAJ Directory of Open Access Journals; Wiley Online Library Open Access; EZB-FREE-00999 freely available EZB journals; Alma/SFX Local Collection; Free Full-Text Journals in Chemistry |
| subjects | Analysis Combustion Dielectric films Diffraction Glycine Methods Thin films X-ray spectroscopy X-rays |
| title | A Novel Approach for Fabricating LaMN[O.sub.3] Thin Films Using Combined Microwave Combustion and Pulsed Electron Deposition Techniques |
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