Preparation, characterization, and determination of mechanical and thermal stability of natural zeolite-based foamed geopolymers
[Display omitted] •Foamed geopolymers were prepared for the first time by the alkaline activation of Ecuadorian natural zeolite.•Different amounts of Al powder and H2O2 (30% water solution) were used as foaming agents.•The compressive strength results met Ecuadorian technical standards NTE INEN 643...
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Veröffentlicht in: | Construction & building materials 2018-05, Vol.172, p.448-456 |
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creator | Lynch, José Luis Villalba Baykara, Haci Cornejo, Mauricio Soriano, Guillermo Ulloa, Néstor A. |
description | [Display omitted]
•Foamed geopolymers were prepared for the first time by the alkaline activation of Ecuadorian natural zeolite.•Different amounts of Al powder and H2O2 (30% water solution) were used as foaming agents.•The compressive strength results met Ecuadorian technical standards NTE INEN 643 and NTE INEN 638.•Potential isolation materials were prepared for construction industry.
This study is the first attempt to evaluate the effect of two foaming agents, aluminum powder and hydrogen peroxide (30 wt% water solution) on zeolite-based geopolymers and their possible use as building material according to Ecuadorian technical standards. These foamed geopolymers were prepared by alkali activation of an Ecuadorian natural zeolitic tuff and by alkali activation using NaOH (10 M), Ca(OH)2 and Na4Si5O12, with the use of two different foaming agents mentioned. In the case of aluminum powder, the experimental range was between 0.05 and 0.25 wt%; on the other hand, the percentages of hydrogen peroxide ranged from 0.5 to 4.0%. For characterization of the foamed geopolymer samples, quantitative X-ray diffraction (QXRD), thermogravimetric (TGA), Fourier transform infrared spectroscopy (FTIR), and scanning electron microscopy (SEM) techniques were used. The results of both foaming agents in zeolite-based geopolymers met Ecuadorian technical standards NTE INEN 643 and NTE INEN 638; nevertheless, the use of aluminum powder as foaming agent exhibited a better pore size distribution, suggesting a better performance. On the basis of these results, foamed geopolymers are suitable construction materials for the application of manufactured for masonry wall in houses. |
doi_str_mv | 10.1016/j.conbuildmat.2018.03.253 |
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•Foamed geopolymers were prepared for the first time by the alkaline activation of Ecuadorian natural zeolite.•Different amounts of Al powder and H2O2 (30% water solution) were used as foaming agents.•The compressive strength results met Ecuadorian technical standards NTE INEN 643 and NTE INEN 638.•Potential isolation materials were prepared for construction industry.
This study is the first attempt to evaluate the effect of two foaming agents, aluminum powder and hydrogen peroxide (30 wt% water solution) on zeolite-based geopolymers and their possible use as building material according to Ecuadorian technical standards. These foamed geopolymers were prepared by alkali activation of an Ecuadorian natural zeolitic tuff and by alkali activation using NaOH (10 M), Ca(OH)2 and Na4Si5O12, with the use of two different foaming agents mentioned. In the case of aluminum powder, the experimental range was between 0.05 and 0.25 wt%; on the other hand, the percentages of hydrogen peroxide ranged from 0.5 to 4.0%. For characterization of the foamed geopolymer samples, quantitative X-ray diffraction (QXRD), thermogravimetric (TGA), Fourier transform infrared spectroscopy (FTIR), and scanning electron microscopy (SEM) techniques were used. The results of both foaming agents in zeolite-based geopolymers met Ecuadorian technical standards NTE INEN 643 and NTE INEN 638; nevertheless, the use of aluminum powder as foaming agent exhibited a better pore size distribution, suggesting a better performance. On the basis of these results, foamed geopolymers are suitable construction materials for the application of manufactured for masonry wall in houses.</description><identifier>ISSN: 0950-0618</identifier><identifier>EISSN: 1879-0526</identifier><identifier>DOI: 10.1016/j.conbuildmat.2018.03.253</identifier><language>eng</language><publisher>Elsevier Ltd</publisher><subject>Aluminum powder ; Analysis ; Chemical properties ; Concretes ; Ecuadorian natural zeolite ; Foamed geopolymer ; Hydrogen peroxide ; Mechanical properties ; Potential Isolation materials ; Thermal properties ; Volcanic rocks ; Zeolites</subject><ispartof>Construction & building materials, 2018-05, Vol.172, p.448-456</ispartof><rights>2018 Elsevier Ltd</rights><rights>COPYRIGHT 2018 Elsevier B.V.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c463t-76690787848e9419d7650dedcefda2b6402e98c577423d797c9c62f1ff94ab5a3</citedby><cites>FETCH-LOGICAL-c463t-76690787848e9419d7650dedcefda2b6402e98c577423d797c9c62f1ff94ab5a3</cites><orcidid>0000-0002-8319-0836</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.conbuildmat.2018.03.253$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,780,784,3548,27922,27923,45993</link.rule.ids></links><search><creatorcontrib>Lynch, José Luis Villalba</creatorcontrib><creatorcontrib>Baykara, Haci</creatorcontrib><creatorcontrib>Cornejo, Mauricio</creatorcontrib><creatorcontrib>Soriano, Guillermo</creatorcontrib><creatorcontrib>Ulloa, Néstor A.</creatorcontrib><title>Preparation, characterization, and determination of mechanical and thermal stability of natural zeolite-based foamed geopolymers</title><title>Construction & building materials</title><description>[Display omitted]
•Foamed geopolymers were prepared for the first time by the alkaline activation of Ecuadorian natural zeolite.•Different amounts of Al powder and H2O2 (30% water solution) were used as foaming agents.•The compressive strength results met Ecuadorian technical standards NTE INEN 643 and NTE INEN 638.•Potential isolation materials were prepared for construction industry.
This study is the first attempt to evaluate the effect of two foaming agents, aluminum powder and hydrogen peroxide (30 wt% water solution) on zeolite-based geopolymers and their possible use as building material according to Ecuadorian technical standards. These foamed geopolymers were prepared by alkali activation of an Ecuadorian natural zeolitic tuff and by alkali activation using NaOH (10 M), Ca(OH)2 and Na4Si5O12, with the use of two different foaming agents mentioned. In the case of aluminum powder, the experimental range was between 0.05 and 0.25 wt%; on the other hand, the percentages of hydrogen peroxide ranged from 0.5 to 4.0%. For characterization of the foamed geopolymer samples, quantitative X-ray diffraction (QXRD), thermogravimetric (TGA), Fourier transform infrared spectroscopy (FTIR), and scanning electron microscopy (SEM) techniques were used. The results of both foaming agents in zeolite-based geopolymers met Ecuadorian technical standards NTE INEN 643 and NTE INEN 638; nevertheless, the use of aluminum powder as foaming agent exhibited a better pore size distribution, suggesting a better performance. On the basis of these results, foamed geopolymers are suitable construction materials for the application of manufactured for masonry wall in houses.</description><subject>Aluminum powder</subject><subject>Analysis</subject><subject>Chemical properties</subject><subject>Concretes</subject><subject>Ecuadorian natural zeolite</subject><subject>Foamed geopolymer</subject><subject>Hydrogen peroxide</subject><subject>Mechanical properties</subject><subject>Potential Isolation materials</subject><subject>Thermal properties</subject><subject>Volcanic rocks</subject><subject>Zeolites</subject><issn>0950-0618</issn><issn>1879-0526</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2018</creationdate><recordtype>article</recordtype><sourceid>N95</sourceid><recordid>eNqNksFrHCEUxiW00G3a_2FCr5mpOjM6HsPSJoVAcmjP4uhz1mVGF3ULm1P_9LjZHBLYQxH08b3f9-DJh9AVwQ3BhH3fNjr4ce9ms6jcUEyGBrcN7dsLtCIDFzXuKfuAVlj0uMaMDJ_Q55S2GGNGGV2hf48Rdiqq7IK_rvSmlDpDdE-vivKmMlCUxfkXqQq2WqCA3mk1v_TzprRLnbIa3ezy4cgUeh-L-AShSFCPKoGpbFBLeSYIuzAfFojpC_po1Zzg6-t7if78_PF7fVffP9z-Wt_c17pjba45YwLzgQ_dAKIjwnDWYwNGgzWKjqzDFMSge8472houuBaaUUusFZ0ae9Veom-nuZOaQTpvQy6rLi5pedN3tOdsIEOh6jPUBB7KLsGDdUV-xzdn-HIMLE6fNVy_MYz75DykciU3bXKa1D6l97g44TqGlCJYuYtuUfEgCZbHAMitfBMAeQyAxK0sASje9ckL5Vv_OogyaQdeg3ERdJYmuP-Y8gxVIMFK</recordid><startdate>20180530</startdate><enddate>20180530</enddate><creator>Lynch, José Luis Villalba</creator><creator>Baykara, Haci</creator><creator>Cornejo, Mauricio</creator><creator>Soriano, Guillermo</creator><creator>Ulloa, Néstor A.</creator><general>Elsevier Ltd</general><general>Elsevier B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>N95</scope><scope>XI7</scope><orcidid>https://orcid.org/0000-0002-8319-0836</orcidid></search><sort><creationdate>20180530</creationdate><title>Preparation, characterization, and determination of mechanical and thermal stability of natural zeolite-based foamed geopolymers</title><author>Lynch, José Luis Villalba ; Baykara, Haci ; Cornejo, Mauricio ; Soriano, Guillermo ; Ulloa, Néstor A.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c463t-76690787848e9419d7650dedcefda2b6402e98c577423d797c9c62f1ff94ab5a3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2018</creationdate><topic>Aluminum powder</topic><topic>Analysis</topic><topic>Chemical properties</topic><topic>Concretes</topic><topic>Ecuadorian natural zeolite</topic><topic>Foamed geopolymer</topic><topic>Hydrogen peroxide</topic><topic>Mechanical properties</topic><topic>Potential Isolation materials</topic><topic>Thermal properties</topic><topic>Volcanic rocks</topic><topic>Zeolites</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Lynch, José Luis Villalba</creatorcontrib><creatorcontrib>Baykara, Haci</creatorcontrib><creatorcontrib>Cornejo, Mauricio</creatorcontrib><creatorcontrib>Soriano, Guillermo</creatorcontrib><creatorcontrib>Ulloa, Néstor A.</creatorcontrib><collection>CrossRef</collection><collection>Gale Business: Insights</collection><collection>Business Insights: Essentials</collection><jtitle>Construction & building materials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Lynch, José Luis Villalba</au><au>Baykara, Haci</au><au>Cornejo, Mauricio</au><au>Soriano, Guillermo</au><au>Ulloa, Néstor A.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Preparation, characterization, and determination of mechanical and thermal stability of natural zeolite-based foamed geopolymers</atitle><jtitle>Construction & building materials</jtitle><date>2018-05-30</date><risdate>2018</risdate><volume>172</volume><spage>448</spage><epage>456</epage><pages>448-456</pages><issn>0950-0618</issn><eissn>1879-0526</eissn><abstract>[Display omitted]
•Foamed geopolymers were prepared for the first time by the alkaline activation of Ecuadorian natural zeolite.•Different amounts of Al powder and H2O2 (30% water solution) were used as foaming agents.•The compressive strength results met Ecuadorian technical standards NTE INEN 643 and NTE INEN 638.•Potential isolation materials were prepared for construction industry.
This study is the first attempt to evaluate the effect of two foaming agents, aluminum powder and hydrogen peroxide (30 wt% water solution) on zeolite-based geopolymers and their possible use as building material according to Ecuadorian technical standards. These foamed geopolymers were prepared by alkali activation of an Ecuadorian natural zeolitic tuff and by alkali activation using NaOH (10 M), Ca(OH)2 and Na4Si5O12, with the use of two different foaming agents mentioned. In the case of aluminum powder, the experimental range was between 0.05 and 0.25 wt%; on the other hand, the percentages of hydrogen peroxide ranged from 0.5 to 4.0%. For characterization of the foamed geopolymer samples, quantitative X-ray diffraction (QXRD), thermogravimetric (TGA), Fourier transform infrared spectroscopy (FTIR), and scanning electron microscopy (SEM) techniques were used. The results of both foaming agents in zeolite-based geopolymers met Ecuadorian technical standards NTE INEN 643 and NTE INEN 638; nevertheless, the use of aluminum powder as foaming agent exhibited a better pore size distribution, suggesting a better performance. On the basis of these results, foamed geopolymers are suitable construction materials for the application of manufactured for masonry wall in houses.</abstract><pub>Elsevier Ltd</pub><doi>10.1016/j.conbuildmat.2018.03.253</doi><tpages>9</tpages><orcidid>https://orcid.org/0000-0002-8319-0836</orcidid></addata></record> |
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subjects | Aluminum powder Analysis Chemical properties Concretes Ecuadorian natural zeolite Foamed geopolymer Hydrogen peroxide Mechanical properties Potential Isolation materials Thermal properties Volcanic rocks Zeolites |
title | Preparation, characterization, and determination of mechanical and thermal stability of natural zeolite-based foamed geopolymers |
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