Synthesis growth and characterization of l-valine nickel (II) chloride: A novel semiorganic nonlinear optical crystal
A new semi organic nonlinear optical crystal, l -valine nickel chloride has been synthesized and good optical quality single crystals were grown by slow evaporation technique. The growth conditions of the crystals are studied and the grown crystals are confirmed by powder X-ray diffraction studies....
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| Veröffentlicht in: | Journal of thermal analysis and calorimetry 2012-06, Vol.108 (3), p.887-894 |
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| container_end_page | 894 |
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| container_title | Journal of thermal analysis and calorimetry |
| container_volume | 108 |
| creator | Sangeetha, M. K. Mariappan, M. Madhurambal, G. Mojumdar, S. C. |
| description | A new semi organic nonlinear optical crystal,
l
-valine nickel chloride has been synthesized and good optical quality single crystals were grown by slow evaporation technique. The growth conditions of the crystals are studied and the grown crystals are confirmed by powder X-ray diffraction studies. The grown crystal was characterized by using powdered XRD, FT-IR, UV–Vis–NIR, EDAX, and TG–DTA. The crystalline nature and its various planes of reflections were observed by the powder XRD. The presence of various functional groups was confirmed by FT-IR spectroscopic technique. The UV–Vis–NIR spectrum indicates that the crystal has very good absorption in the entire visible and near IR region spectrum suggesting the suitability of the material for NLO applications. The decomposition temperatures and mass loss have been estimated from the thermogravimetric analysis. |
| doi_str_mv | 10.1007/s10973-012-2355-x |
| format | Article |
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l
-valine nickel chloride has been synthesized and good optical quality single crystals were grown by slow evaporation technique. The growth conditions of the crystals are studied and the grown crystals are confirmed by powder X-ray diffraction studies. The grown crystal was characterized by using powdered XRD, FT-IR, UV–Vis–NIR, EDAX, and TG–DTA. The crystalline nature and its various planes of reflections were observed by the powder XRD. The presence of various functional groups was confirmed by FT-IR spectroscopic technique. The UV–Vis–NIR spectrum indicates that the crystal has very good absorption in the entire visible and near IR region spectrum suggesting the suitability of the material for NLO applications. The decomposition temperatures and mass loss have been estimated from the thermogravimetric analysis.</description><identifier>ISSN: 1388-6150</identifier><identifier>EISSN: 1588-2926</identifier><identifier>EISSN: 1572-8943</identifier><identifier>DOI: 10.1007/s10973-012-2355-x</identifier><language>eng</language><publisher>Dordrecht: Springer Netherlands</publisher><subject>Amino acids ; Analysis ; Analytical Chemistry ; Chemical properties ; Chemistry ; Chemistry and Materials Science ; Diffraction ; Growth ; Inorganic Chemistry ; Measurement Science and Instrumentation ; Nickel ; Physical Chemistry ; Polymer Sciences ; X-rays</subject><ispartof>Journal of thermal analysis and calorimetry, 2012-06, Vol.108 (3), p.887-894</ispartof><rights>Akadémiai Kiadó, Budapest, Hungary 2012</rights><rights>COPYRIGHT 2012 Springer</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c341t-9eb5ae7bf70eaa5abf42eaea27464f50fa15b67050d838d7bb6166563f5632d93</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10973-012-2355-x$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10973-012-2355-x$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Sangeetha, M. K.</creatorcontrib><creatorcontrib>Mariappan, M.</creatorcontrib><creatorcontrib>Madhurambal, G.</creatorcontrib><creatorcontrib>Mojumdar, S. C.</creatorcontrib><title>Synthesis growth and characterization of l-valine nickel (II) chloride: A novel semiorganic nonlinear optical crystal</title><title>Journal of thermal analysis and calorimetry</title><addtitle>J Therm Anal Calorim</addtitle><description>A new semi organic nonlinear optical crystal,
l
-valine nickel chloride has been synthesized and good optical quality single crystals were grown by slow evaporation technique. The growth conditions of the crystals are studied and the grown crystals are confirmed by powder X-ray diffraction studies. The grown crystal was characterized by using powdered XRD, FT-IR, UV–Vis–NIR, EDAX, and TG–DTA. The crystalline nature and its various planes of reflections were observed by the powder XRD. The presence of various functional groups was confirmed by FT-IR spectroscopic technique. The UV–Vis–NIR spectrum indicates that the crystal has very good absorption in the entire visible and near IR region spectrum suggesting the suitability of the material for NLO applications. The decomposition temperatures and mass loss have been estimated from the thermogravimetric analysis.</description><subject>Amino acids</subject><subject>Analysis</subject><subject>Analytical Chemistry</subject><subject>Chemical properties</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Diffraction</subject><subject>Growth</subject><subject>Inorganic Chemistry</subject><subject>Measurement Science and Instrumentation</subject><subject>Nickel</subject><subject>Physical Chemistry</subject><subject>Polymer Sciences</subject><subject>X-rays</subject><issn>1388-6150</issn><issn>1588-2926</issn><issn>1572-8943</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2012</creationdate><recordtype>article</recordtype><recordid>eNp9kV1LwzAUhosoOOZ-gHcFb9xFZz6atL0cw2lhIDi9Dml70kW7RJJON3-9GfVmIBJCDuF5DofzRtE1RjOMUHbnMSoymiBMEkIZS_Zn0QizPE9IQfh5qGmoOWboMpp4rytEMOIFy4tRtFwfTL8Br33cOvvVb2JpmrjeSCfrHpz-lr22JrYq7pJP2WkDsdH1O3TxbVlOA9hZpxu4ii6U7DxMft9x9Lq8f1k8Jqunh3IxXyU1TXGfFFAxCVmlMgRSMlmplIAESbKUp4ohJTGreIYYanKaN1lVccw541SFS5qCjqOboW8rOxDaKNuHQbfa12JOWYHylDESqNkfVDgNbHVtDSgd_k-E6YkQmB72fSt33oty_XzK4oGtnfXegRIfTm-lOwiMxDEOMcQhQhziGIfYB4cMjg-sacGJN7tzJmzqH-kHWumLbg</recordid><startdate>20120601</startdate><enddate>20120601</enddate><creator>Sangeetha, M. K.</creator><creator>Mariappan, M.</creator><creator>Madhurambal, G.</creator><creator>Mojumdar, S. C.</creator><general>Springer Netherlands</general><general>Springer</general><scope>AAYXX</scope><scope>CITATION</scope><scope>ISR</scope></search><sort><creationdate>20120601</creationdate><title>Synthesis growth and characterization of l-valine nickel (II) chloride</title><author>Sangeetha, M. K. ; Mariappan, M. ; Madhurambal, G. ; Mojumdar, S. C.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c341t-9eb5ae7bf70eaa5abf42eaea27464f50fa15b67050d838d7bb6166563f5632d93</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2012</creationdate><topic>Amino acids</topic><topic>Analysis</topic><topic>Analytical Chemistry</topic><topic>Chemical properties</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Diffraction</topic><topic>Growth</topic><topic>Inorganic Chemistry</topic><topic>Measurement Science and Instrumentation</topic><topic>Nickel</topic><topic>Physical Chemistry</topic><topic>Polymer Sciences</topic><topic>X-rays</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Sangeetha, M. K.</creatorcontrib><creatorcontrib>Mariappan, M.</creatorcontrib><creatorcontrib>Madhurambal, G.</creatorcontrib><creatorcontrib>Mojumdar, S. C.</creatorcontrib><collection>CrossRef</collection><collection>Gale In Context: Science</collection><jtitle>Journal of thermal analysis and calorimetry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Sangeetha, M. K.</au><au>Mariappan, M.</au><au>Madhurambal, G.</au><au>Mojumdar, S. C.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis growth and characterization of l-valine nickel (II) chloride: A novel semiorganic nonlinear optical crystal</atitle><jtitle>Journal of thermal analysis and calorimetry</jtitle><stitle>J Therm Anal Calorim</stitle><date>2012-06-01</date><risdate>2012</risdate><volume>108</volume><issue>3</issue><spage>887</spage><epage>894</epage><pages>887-894</pages><issn>1388-6150</issn><eissn>1588-2926</eissn><eissn>1572-8943</eissn><abstract>A new semi organic nonlinear optical crystal,
l
-valine nickel chloride has been synthesized and good optical quality single crystals were grown by slow evaporation technique. The growth conditions of the crystals are studied and the grown crystals are confirmed by powder X-ray diffraction studies. The grown crystal was characterized by using powdered XRD, FT-IR, UV–Vis–NIR, EDAX, and TG–DTA. The crystalline nature and its various planes of reflections were observed by the powder XRD. The presence of various functional groups was confirmed by FT-IR spectroscopic technique. The UV–Vis–NIR spectrum indicates that the crystal has very good absorption in the entire visible and near IR region spectrum suggesting the suitability of the material for NLO applications. The decomposition temperatures and mass loss have been estimated from the thermogravimetric analysis.</abstract><cop>Dordrecht</cop><pub>Springer Netherlands</pub><doi>10.1007/s10973-012-2355-x</doi><tpages>8</tpages></addata></record> |
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| ispartof | Journal of thermal analysis and calorimetry, 2012-06, Vol.108 (3), p.887-894 |
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| subjects | Amino acids Analysis Analytical Chemistry Chemical properties Chemistry Chemistry and Materials Science Diffraction Growth Inorganic Chemistry Measurement Science and Instrumentation Nickel Physical Chemistry Polymer Sciences X-rays |
| title | Synthesis growth and characterization of l-valine nickel (II) chloride: A novel semiorganic nonlinear optical crystal |
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