Differential pulse anodic stripping voltammetric determination of traces of tin using a glassy carbon electrode modified with bismuth and a film of poly(bromophenol blue)
We report on an anodic stripping voltammetric method for the determination of tin using a glassy carbon electrode modified with bismuth and poly(bromophenol blue). After an accumulation time of 60 s at −1.20 V (vs. SCE), the response of the electrode to tin in 1.0 M HCl is linear in the concentratio...
Gespeichert in:
| Veröffentlicht in: | Mikrochimica acta (1966) 2012-06, Vol.177 (3-4), p.365-372 |
|---|---|
| Hauptverfasser: | , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | 372 |
|---|---|
| container_issue | 3-4 |
| container_start_page | 365 |
| container_title | Mikrochimica acta (1966) |
| container_volume | 177 |
| creator | Yang, Gongjun Wang, Yujuan Qi, Fen |
| description | We report on an anodic stripping voltammetric method for the determination of tin using a glassy carbon electrode modified with bismuth and poly(bromophenol blue). After an accumulation time of 60 s at −1.20 V (vs. SCE), the response of the electrode to tin in 1.0 M HCl is linear in the concentration ranges from 20 nM to 1.0 μM, and from 1.0 μM to 20 μM, with a detection limit of 7.0 nM (at an SNR of 3) and with relative standard deviations in the order of 3.0–3.8%. The method was validated by comparing the results with those obtained by AAS and successfully applied to the determination of tin in canned food.
Figure
Differential pulse stripping voltammetric responses of Sn
2+
at Bi/Poly(BPB)/GCE in 1.0 M HCl . Sn
2+
concentration (μM): 0.020, 0.10, 0.30, 0.50, 0.70, 1.0, 3.0, 5.0, 7.0, 10.0 and 20.0. Inset: Differential pulse stripping voltammograms of circle portion at low Sn
2+
concentration are zoomed in. |
| doi_str_mv | 10.1007/s00604-012-0790-9 |
| format | Article |
| fullrecord | <record><control><sourceid>gale_cross</sourceid><recordid>TN_cdi_gale_infotracacademiconefile_A715063131</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><galeid>A715063131</galeid><sourcerecordid>A715063131</sourcerecordid><originalsourceid>FETCH-LOGICAL-c357t-40ffebaddc27b6b3121a5ed26392bbb6330ef8d4b8d10795ccf47b2f62c565cb3</originalsourceid><addsrcrecordid>eNp9kcuO1DAQRS0EEk3DB7DzBgkWGfxInM5yNAzMSCOxgbXlR7nHIz8iOwH1L_GVOASxRLUoy65zVdcXobeUXFFCxo-VEEH6jlDWkXEi3fQMHWjPRTeQkT9HB0KY6LgY2Uv0qtYnQugoWH9Avz5556BAWrwKeF5DBaxStt7guhQ_zz6d8Y8cFhUjtAuDLSxQok9q8Tnh7PBSlIH65-QTXutGKHwOqtYLNqroNgYBzFKyBRybtvNg8U-_PGLta1xbV8k2xvkQN505h8t7XXLM8yOkHLAOK3x4jV441fZ787cf0ffPt99u7rqHr1_ub64fOsOHcel60gxpZa1hoxaaU0bVAJYJPjGtteCcgDvZXp8sbV81GOP6UTMnmBnEYDQ_oqtd96wCSJ9c3hy2shC9yQnamiCvRzoQwWmrI6I7YEqutYCTc_FRlYukRG7pyD0d2dKRWzpyasy7nZlVNSq4opLx9R_IholNrD-1ObbP1faUzlDkU15Lav7_I_4bd0CkJQ</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype></control><display><type>article</type><title>Differential pulse anodic stripping voltammetric determination of traces of tin using a glassy carbon electrode modified with bismuth and a film of poly(bromophenol blue)</title><source>SpringerLink Journals</source><creator>Yang, Gongjun ; Wang, Yujuan ; Qi, Fen</creator><creatorcontrib>Yang, Gongjun ; Wang, Yujuan ; Qi, Fen</creatorcontrib><description>We report on an anodic stripping voltammetric method for the determination of tin using a glassy carbon electrode modified with bismuth and poly(bromophenol blue). After an accumulation time of 60 s at −1.20 V (vs. SCE), the response of the electrode to tin in 1.0 M HCl is linear in the concentration ranges from 20 nM to 1.0 μM, and from 1.0 μM to 20 μM, with a detection limit of 7.0 nM (at an SNR of 3) and with relative standard deviations in the order of 3.0–3.8%. The method was validated by comparing the results with those obtained by AAS and successfully applied to the determination of tin in canned food.
Figure
Differential pulse stripping voltammetric responses of Sn
2+
at Bi/Poly(BPB)/GCE in 1.0 M HCl . Sn
2+
concentration (μM): 0.020, 0.10, 0.30, 0.50, 0.70, 1.0, 3.0, 5.0, 7.0, 10.0 and 20.0. Inset: Differential pulse stripping voltammograms of circle portion at low Sn
2+
concentration are zoomed in.</description><identifier>ISSN: 0026-3672</identifier><identifier>EISSN: 1436-5073</identifier><identifier>DOI: 10.1007/s00604-012-0790-9</identifier><identifier>CODEN: MIACAQ</identifier><language>eng</language><publisher>Vienna: Springer Vienna</publisher><subject>Analytical Chemistry ; Characterization and Evaluation of Materials ; Chemistry ; Chemistry and Materials Science ; Electrochemical methods ; Exact sciences and technology ; Microengineering ; Nanochemistry ; Nanotechnology ; Original Paper ; Phenols ; Spectrometric and optical methods</subject><ispartof>Mikrochimica acta (1966), 2012-06, Vol.177 (3-4), p.365-372</ispartof><rights>Springer-Verlag 2012</rights><rights>2015 INIST-CNRS</rights><rights>COPYRIGHT 2012 Springer</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c357t-40ffebaddc27b6b3121a5ed26392bbb6330ef8d4b8d10795ccf47b2f62c565cb3</citedby><cites>FETCH-LOGICAL-c357t-40ffebaddc27b6b3121a5ed26392bbb6330ef8d4b8d10795ccf47b2f62c565cb3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s00604-012-0790-9$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s00604-012-0790-9$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=25929248$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Yang, Gongjun</creatorcontrib><creatorcontrib>Wang, Yujuan</creatorcontrib><creatorcontrib>Qi, Fen</creatorcontrib><title>Differential pulse anodic stripping voltammetric determination of traces of tin using a glassy carbon electrode modified with bismuth and a film of poly(bromophenol blue)</title><title>Mikrochimica acta (1966)</title><addtitle>Microchim Acta</addtitle><description>We report on an anodic stripping voltammetric method for the determination of tin using a glassy carbon electrode modified with bismuth and poly(bromophenol blue). After an accumulation time of 60 s at −1.20 V (vs. SCE), the response of the electrode to tin in 1.0 M HCl is linear in the concentration ranges from 20 nM to 1.0 μM, and from 1.0 μM to 20 μM, with a detection limit of 7.0 nM (at an SNR of 3) and with relative standard deviations in the order of 3.0–3.8%. The method was validated by comparing the results with those obtained by AAS and successfully applied to the determination of tin in canned food.
Figure
Differential pulse stripping voltammetric responses of Sn
2+
at Bi/Poly(BPB)/GCE in 1.0 M HCl . Sn
2+
concentration (μM): 0.020, 0.10, 0.30, 0.50, 0.70, 1.0, 3.0, 5.0, 7.0, 10.0 and 20.0. Inset: Differential pulse stripping voltammograms of circle portion at low Sn
2+
concentration are zoomed in.</description><subject>Analytical Chemistry</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Electrochemical methods</subject><subject>Exact sciences and technology</subject><subject>Microengineering</subject><subject>Nanochemistry</subject><subject>Nanotechnology</subject><subject>Original Paper</subject><subject>Phenols</subject><subject>Spectrometric and optical methods</subject><issn>0026-3672</issn><issn>1436-5073</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2012</creationdate><recordtype>article</recordtype><recordid>eNp9kcuO1DAQRS0EEk3DB7DzBgkWGfxInM5yNAzMSCOxgbXlR7nHIz8iOwH1L_GVOASxRLUoy65zVdcXobeUXFFCxo-VEEH6jlDWkXEi3fQMHWjPRTeQkT9HB0KY6LgY2Uv0qtYnQugoWH9Avz5556BAWrwKeF5DBaxStt7guhQ_zz6d8Y8cFhUjtAuDLSxQok9q8Tnh7PBSlIH65-QTXutGKHwOqtYLNqroNgYBzFKyBRybtvNg8U-_PGLta1xbV8k2xvkQN505h8t7XXLM8yOkHLAOK3x4jV441fZ787cf0ffPt99u7rqHr1_ub64fOsOHcel60gxpZa1hoxaaU0bVAJYJPjGtteCcgDvZXp8sbV81GOP6UTMnmBnEYDQ_oqtd96wCSJ9c3hy2shC9yQnamiCvRzoQwWmrI6I7YEqutYCTc_FRlYukRG7pyD0d2dKRWzpyasy7nZlVNSq4opLx9R_IholNrD-1ObbP1faUzlDkU15Lav7_I_4bd0CkJQ</recordid><startdate>20120601</startdate><enddate>20120601</enddate><creator>Yang, Gongjun</creator><creator>Wang, Yujuan</creator><creator>Qi, Fen</creator><general>Springer Vienna</general><general>Springer</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20120601</creationdate><title>Differential pulse anodic stripping voltammetric determination of traces of tin using a glassy carbon electrode modified with bismuth and a film of poly(bromophenol blue)</title><author>Yang, Gongjun ; Wang, Yujuan ; Qi, Fen</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c357t-40ffebaddc27b6b3121a5ed26392bbb6330ef8d4b8d10795ccf47b2f62c565cb3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2012</creationdate><topic>Analytical Chemistry</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Electrochemical methods</topic><topic>Exact sciences and technology</topic><topic>Microengineering</topic><topic>Nanochemistry</topic><topic>Nanotechnology</topic><topic>Original Paper</topic><topic>Phenols</topic><topic>Spectrometric and optical methods</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Yang, Gongjun</creatorcontrib><creatorcontrib>Wang, Yujuan</creatorcontrib><creatorcontrib>Qi, Fen</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><jtitle>Mikrochimica acta (1966)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Yang, Gongjun</au><au>Wang, Yujuan</au><au>Qi, Fen</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Differential pulse anodic stripping voltammetric determination of traces of tin using a glassy carbon electrode modified with bismuth and a film of poly(bromophenol blue)</atitle><jtitle>Mikrochimica acta (1966)</jtitle><stitle>Microchim Acta</stitle><date>2012-06-01</date><risdate>2012</risdate><volume>177</volume><issue>3-4</issue><spage>365</spage><epage>372</epage><pages>365-372</pages><issn>0026-3672</issn><eissn>1436-5073</eissn><coden>MIACAQ</coden><abstract>We report on an anodic stripping voltammetric method for the determination of tin using a glassy carbon electrode modified with bismuth and poly(bromophenol blue). After an accumulation time of 60 s at −1.20 V (vs. SCE), the response of the electrode to tin in 1.0 M HCl is linear in the concentration ranges from 20 nM to 1.0 μM, and from 1.0 μM to 20 μM, with a detection limit of 7.0 nM (at an SNR of 3) and with relative standard deviations in the order of 3.0–3.8%. The method was validated by comparing the results with those obtained by AAS and successfully applied to the determination of tin in canned food.
Figure
Differential pulse stripping voltammetric responses of Sn
2+
at Bi/Poly(BPB)/GCE in 1.0 M HCl . Sn
2+
concentration (μM): 0.020, 0.10, 0.30, 0.50, 0.70, 1.0, 3.0, 5.0, 7.0, 10.0 and 20.0. Inset: Differential pulse stripping voltammograms of circle portion at low Sn
2+
concentration are zoomed in.</abstract><cop>Vienna</cop><pub>Springer Vienna</pub><doi>10.1007/s00604-012-0790-9</doi><tpages>8</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0026-3672 |
| ispartof | Mikrochimica acta (1966), 2012-06, Vol.177 (3-4), p.365-372 |
| issn | 0026-3672 1436-5073 |
| language | eng |
| recordid | cdi_gale_infotracacademiconefile_A715063131 |
| source | SpringerLink Journals |
| subjects | Analytical Chemistry Characterization and Evaluation of Materials Chemistry Chemistry and Materials Science Electrochemical methods Exact sciences and technology Microengineering Nanochemistry Nanotechnology Original Paper Phenols Spectrometric and optical methods |
| title | Differential pulse anodic stripping voltammetric determination of traces of tin using a glassy carbon electrode modified with bismuth and a film of poly(bromophenol blue) |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-02-13T10%3A04%3A33IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-gale_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Differential%20pulse%20anodic%20stripping%20voltammetric%20determination%20of%20traces%20of%20tin%20using%20a%20glassy%20carbon%20electrode%20modified%20with%20bismuth%20and%20a%20film%20of%20poly(bromophenol%20blue)&rft.jtitle=Mikrochimica%20acta%20(1966)&rft.au=Yang,%20Gongjun&rft.date=2012-06-01&rft.volume=177&rft.issue=3-4&rft.spage=365&rft.epage=372&rft.pages=365-372&rft.issn=0026-3672&rft.eissn=1436-5073&rft.coden=MIACAQ&rft_id=info:doi/10.1007/s00604-012-0790-9&rft_dat=%3Cgale_cross%3EA715063131%3C/gale_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_id=info:pmid/&rft_galeid=A715063131&rfr_iscdi=true |