X-ray and synchrotron investigations of heterogeneous systems based on multiwalled carbon nanotubes
This paper presents the results of a complex investigation of heterogeneous systems based on multiwalled carbon nanotubes with the outer surfaces covered by iron oxide (Fe 3 O 4 ) nanocoatings deposited using iron pentacarbonyl as a precursor. Investigations were performed by the methods of electron...
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| Veröffentlicht in: | Physics of the solid state 2015, Vol.57 (1), p.197-204 |
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| container_title | Physics of the solid state |
| container_volume | 57 |
| creator | Sivkov, V. N. Ob”edkov, A. M. Petrova, O. V. Nekipelov, S. V. Kremlev, K. V. Kaverin, B. S. Semenov, N. M. Gusev, S. A. |
| description | This paper presents the results of a complex investigation of heterogeneous systems based on multiwalled carbon nanotubes with the outer surfaces covered by iron oxide (Fe
3
O
4
) nanocoatings deposited using iron pentacarbonyl as a precursor. Investigations were performed by the methods of electron microscopy, X-ray diffractometry, and ultrasoft X-ray spectroscopy with synchrotron radiation. It was established that the formed thin coatings are continuous and nonuniform in thickness. It was shown that good adhesion of iron oxide on the multiwalled carbon nanotube surface is provided by the formation of epoxy and double carbon-oxygen bonds; in this case, the outer graphene layer of nanotubes is not destroyed and retains the hexagonal structure. |
| doi_str_mv | 10.1134/S1063783415010291 |
| format | Article |
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3
O
4
) nanocoatings deposited using iron pentacarbonyl as a precursor. Investigations were performed by the methods of electron microscopy, X-ray diffractometry, and ultrasoft X-ray spectroscopy with synchrotron radiation. It was established that the formed thin coatings are continuous and nonuniform in thickness. It was shown that good adhesion of iron oxide on the multiwalled carbon nanotube surface is provided by the formation of epoxy and double carbon-oxygen bonds; in this case, the outer graphene layer of nanotubes is not destroyed and retains the hexagonal structure.</description><identifier>ISSN: 1063-7834</identifier><identifier>EISSN: 1090-6460</identifier><identifier>DOI: 10.1134/S1063783415010291</identifier><language>eng</language><publisher>Moscow: Pleiades Publishing</publisher><subject>Coatings ; Coatings industry ; Electron microscopy ; Epoxy resins ; Ferric oxide ; Fullerenes ; Graphene ; Investigations ; Iron compounds ; Nanotubes ; Particle accelerators ; Physics ; Physics and Astronomy ; Radiation, Background ; Solid State Physics</subject><ispartof>Physics of the solid state, 2015, Vol.57 (1), p.197-204</ispartof><rights>Pleiades Publishing, Ltd. 2015</rights><rights>COPYRIGHT 2015 Springer</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c361t-2fdc6a98a684facbf1b1bba9a1d3159834b1b202212817e200da36fa4dc973fd3</citedby><cites>FETCH-LOGICAL-c361t-2fdc6a98a684facbf1b1bba9a1d3159834b1b202212817e200da36fa4dc973fd3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1134/S1063783415010291$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1134/S1063783415010291$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Sivkov, V. N.</creatorcontrib><creatorcontrib>Ob”edkov, A. M.</creatorcontrib><creatorcontrib>Petrova, O. V.</creatorcontrib><creatorcontrib>Nekipelov, S. V.</creatorcontrib><creatorcontrib>Kremlev, K. V.</creatorcontrib><creatorcontrib>Kaverin, B. S.</creatorcontrib><creatorcontrib>Semenov, N. M.</creatorcontrib><creatorcontrib>Gusev, S. A.</creatorcontrib><title>X-ray and synchrotron investigations of heterogeneous systems based on multiwalled carbon nanotubes</title><title>Physics of the solid state</title><addtitle>Phys. Solid State</addtitle><description>This paper presents the results of a complex investigation of heterogeneous systems based on multiwalled carbon nanotubes with the outer surfaces covered by iron oxide (Fe
3
O
4
) nanocoatings deposited using iron pentacarbonyl as a precursor. Investigations were performed by the methods of electron microscopy, X-ray diffractometry, and ultrasoft X-ray spectroscopy with synchrotron radiation. It was established that the formed thin coatings are continuous and nonuniform in thickness. It was shown that good adhesion of iron oxide on the multiwalled carbon nanotube surface is provided by the formation of epoxy and double carbon-oxygen bonds; in this case, the outer graphene layer of nanotubes is not destroyed and retains the hexagonal structure.</description><subject>Coatings</subject><subject>Coatings industry</subject><subject>Electron microscopy</subject><subject>Epoxy resins</subject><subject>Ferric oxide</subject><subject>Fullerenes</subject><subject>Graphene</subject><subject>Investigations</subject><subject>Iron compounds</subject><subject>Nanotubes</subject><subject>Particle accelerators</subject><subject>Physics</subject><subject>Physics and Astronomy</subject><subject>Radiation, Background</subject><subject>Solid State Physics</subject><issn>1063-7834</issn><issn>1090-6460</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2015</creationdate><recordtype>article</recordtype><recordid>eNp9kUtLAzEQgIMoWKs_wNtePWzNJNt9HEvxURAEq-Btmc0m25TdRJKs2n9vSr0UQXJIZvJ9wyRDyDXQGQDPbtdAc16UPIM5BcoqOCEToBVN8yynp_tzztP9_Tm58H5LKQDMqwkR76nDXYKmTfzOiI2zwVmTaPMpfdAdBm2NT6xKNjJIZztppB19ZH2Qg08a9LJNojCMfdBf2PcxFOiamDJobBgb6S_JmcLey6vffUre7u9el4_p0_PDarl4SgXPIaRMtSLHqsS8zBSKRkEDTYMVQstjr7H3GDPKGLASCskobZHnCrNWVAVXLZ-S2aFuh72stVHxLSjiauWghTVS6ZhfZLSYs5JxiMLNkRCZIL9Dh6P39Wr9cszCgRXOeu-kqj-cHtDtaqD1fgT1nxFEhx0cH1nTSVdv7ehM_IN_pB9s4omY</recordid><startdate>2015</startdate><enddate>2015</enddate><creator>Sivkov, V. N.</creator><creator>Ob”edkov, A. M.</creator><creator>Petrova, O. V.</creator><creator>Nekipelov, S. V.</creator><creator>Kremlev, K. V.</creator><creator>Kaverin, B. S.</creator><creator>Semenov, N. M.</creator><creator>Gusev, S. A.</creator><general>Pleiades Publishing</general><general>Springer</general><scope>AAYXX</scope><scope>CITATION</scope><scope>ISR</scope></search><sort><creationdate>2015</creationdate><title>X-ray and synchrotron investigations of heterogeneous systems based on multiwalled carbon nanotubes</title><author>Sivkov, V. N. ; Ob”edkov, A. M. ; Petrova, O. V. ; Nekipelov, S. V. ; Kremlev, K. V. ; Kaverin, B. S. ; Semenov, N. M. ; Gusev, S. A.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c361t-2fdc6a98a684facbf1b1bba9a1d3159834b1b202212817e200da36fa4dc973fd3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2015</creationdate><topic>Coatings</topic><topic>Coatings industry</topic><topic>Electron microscopy</topic><topic>Epoxy resins</topic><topic>Ferric oxide</topic><topic>Fullerenes</topic><topic>Graphene</topic><topic>Investigations</topic><topic>Iron compounds</topic><topic>Nanotubes</topic><topic>Particle accelerators</topic><topic>Physics</topic><topic>Physics and Astronomy</topic><topic>Radiation, Background</topic><topic>Solid State Physics</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Sivkov, V. N.</creatorcontrib><creatorcontrib>Ob”edkov, A. M.</creatorcontrib><creatorcontrib>Petrova, O. V.</creatorcontrib><creatorcontrib>Nekipelov, S. V.</creatorcontrib><creatorcontrib>Kremlev, K. V.</creatorcontrib><creatorcontrib>Kaverin, B. S.</creatorcontrib><creatorcontrib>Semenov, N. M.</creatorcontrib><creatorcontrib>Gusev, S. A.</creatorcontrib><collection>CrossRef</collection><collection>Gale In Context: Science</collection><jtitle>Physics of the solid state</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Sivkov, V. N.</au><au>Ob”edkov, A. M.</au><au>Petrova, O. V.</au><au>Nekipelov, S. V.</au><au>Kremlev, K. V.</au><au>Kaverin, B. S.</au><au>Semenov, N. M.</au><au>Gusev, S. A.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>X-ray and synchrotron investigations of heterogeneous systems based on multiwalled carbon nanotubes</atitle><jtitle>Physics of the solid state</jtitle><stitle>Phys. Solid State</stitle><date>2015</date><risdate>2015</risdate><volume>57</volume><issue>1</issue><spage>197</spage><epage>204</epage><pages>197-204</pages><issn>1063-7834</issn><eissn>1090-6460</eissn><abstract>This paper presents the results of a complex investigation of heterogeneous systems based on multiwalled carbon nanotubes with the outer surfaces covered by iron oxide (Fe
3
O
4
) nanocoatings deposited using iron pentacarbonyl as a precursor. Investigations were performed by the methods of electron microscopy, X-ray diffractometry, and ultrasoft X-ray spectroscopy with synchrotron radiation. It was established that the formed thin coatings are continuous and nonuniform in thickness. It was shown that good adhesion of iron oxide on the multiwalled carbon nanotube surface is provided by the formation of epoxy and double carbon-oxygen bonds; in this case, the outer graphene layer of nanotubes is not destroyed and retains the hexagonal structure.</abstract><cop>Moscow</cop><pub>Pleiades Publishing</pub><doi>10.1134/S1063783415010291</doi><tpages>8</tpages></addata></record> |
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| ispartof | Physics of the solid state, 2015, Vol.57 (1), p.197-204 |
| issn | 1063-7834 1090-6460 |
| language | eng |
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| source | SpringerLink Journals - AutoHoldings |
| subjects | Coatings Coatings industry Electron microscopy Epoxy resins Ferric oxide Fullerenes Graphene Investigations Iron compounds Nanotubes Particle accelerators Physics Physics and Astronomy Radiation, Background Solid State Physics |
| title | X-ray and synchrotron investigations of heterogeneous systems based on multiwalled carbon nanotubes |
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