Thermogravimetric analysis: A tool to evaluate the ability of mixtures in consolidating waterlogged archaeological woods
Waterlogged archaeological woods ( Pinus pinaster , Ulmus cf. minor and Fagus sylvatica L.) were consolidated by using Colophony, Rosin 100, and a mixture of Poly(ethylene) glycol (PEG) 3000 and Poly(propylene) glycol (PPG) 425. The efficiency of the consolidants was estimated by determining the con...
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creator | Donato, D. I. Lazzara, G. Milioto, S. |
description | Waterlogged archaeological woods (
Pinus pinaster
,
Ulmus
cf.
minor
and
Fagus sylvatica
L.) were consolidated by using Colophony, Rosin 100, and a mixture of Poly(ethylene) glycol (PEG) 3000 and Poly(propylene) glycol (PPG) 425. The efficiency of the consolidants was estimated by determining the content entrapped into the cavity of degraded wood. For this purpose, thermogravimetry was demonstrated to be a reliable tool. In the case that the polymeric mixture was used for impregnation, it was also possible to discriminate the amount of PEG 3000 from that of PPG 425 captured by the wood capillaries. Regardless of the wood nature, all the consolidants were present in treated samples in large amount (at least 70% w/w). Thermogravimetric results were in agreement with those calculated by using the wood degradation degree and composition of the consolidant mixture. One of the advantages of using this technique consists into requiring very small amounts (a few mg) of sample against the grams necessary for the conventional experiments. |
doi_str_mv | 10.1007/s10973-010-0717-9 |
format | Article |
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Pinus pinaster
,
Ulmus
cf.
minor
and
Fagus sylvatica
L.) were consolidated by using Colophony, Rosin 100, and a mixture of Poly(ethylene) glycol (PEG) 3000 and Poly(propylene) glycol (PPG) 425. The efficiency of the consolidants was estimated by determining the content entrapped into the cavity of degraded wood. For this purpose, thermogravimetry was demonstrated to be a reliable tool. In the case that the polymeric mixture was used for impregnation, it was also possible to discriminate the amount of PEG 3000 from that of PPG 425 captured by the wood capillaries. Regardless of the wood nature, all the consolidants were present in treated samples in large amount (at least 70% w/w). Thermogravimetric results were in agreement with those calculated by using the wood degradation degree and composition of the consolidant mixture. One of the advantages of using this technique consists into requiring very small amounts (a few mg) of sample against the grams necessary for the conventional experiments.</description><identifier>ISSN: 1388-6150</identifier><identifier>EISSN: 1588-2926</identifier><identifier>EISSN: 1572-8943</identifier><identifier>DOI: 10.1007/s10973-010-0717-9</identifier><language>eng</language><publisher>Dordrecht: Springer Netherlands</publisher><subject>Analytical Chemistry ; Applied sciences ; Archaeology ; Chemistry ; Chemistry and Materials Science ; Degradation and preservation ; Exact sciences and technology ; Inorganic Chemistry ; Measurement Science and Instrumentation ; Physical Chemistry ; Polymer industry, paints, wood ; Polymer Sciences ; Wood ; Wood. Paper. Non wovens</subject><ispartof>Journal of thermal analysis and calorimetry, 2010-09, Vol.101 (3), p.1085-1091</ispartof><rights>Akadémiai Kiadó, Budapest, Hungary 2010</rights><rights>2015 INIST-CNRS</rights><rights>COPYRIGHT 2010 Springer</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c2589-35177465e5b0e6e601529bd5775793a593491fd222c399bdced7c7ef4d937b863</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10973-010-0717-9$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10973-010-0717-9$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,777,781,27905,27906,41469,42538,51300</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=23203232$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Donato, D. I.</creatorcontrib><creatorcontrib>Lazzara, G.</creatorcontrib><creatorcontrib>Milioto, S.</creatorcontrib><title>Thermogravimetric analysis: A tool to evaluate the ability of mixtures in consolidating waterlogged archaeological woods</title><title>Journal of thermal analysis and calorimetry</title><addtitle>J Therm Anal Calorim</addtitle><description>Waterlogged archaeological woods (
Pinus pinaster
,
Ulmus
cf.
minor
and
Fagus sylvatica
L.) were consolidated by using Colophony, Rosin 100, and a mixture of Poly(ethylene) glycol (PEG) 3000 and Poly(propylene) glycol (PPG) 425. The efficiency of the consolidants was estimated by determining the content entrapped into the cavity of degraded wood. For this purpose, thermogravimetry was demonstrated to be a reliable tool. In the case that the polymeric mixture was used for impregnation, it was also possible to discriminate the amount of PEG 3000 from that of PPG 425 captured by the wood capillaries. Regardless of the wood nature, all the consolidants were present in treated samples in large amount (at least 70% w/w). Thermogravimetric results were in agreement with those calculated by using the wood degradation degree and composition of the consolidant mixture. One of the advantages of using this technique consists into requiring very small amounts (a few mg) of sample against the grams necessary for the conventional experiments.</description><subject>Analytical Chemistry</subject><subject>Applied sciences</subject><subject>Archaeology</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Degradation and preservation</subject><subject>Exact sciences and technology</subject><subject>Inorganic Chemistry</subject><subject>Measurement Science and Instrumentation</subject><subject>Physical Chemistry</subject><subject>Polymer industry, paints, wood</subject><subject>Polymer Sciences</subject><subject>Wood</subject><subject>Wood. Paper. Non wovens</subject><issn>1388-6150</issn><issn>1588-2926</issn><issn>1572-8943</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2010</creationdate><recordtype>article</recordtype><recordid>eNp9kE1LAzEQhoMoWGp_gJ68ePCQmo9NsjmWorVQELSeQzabXSP7UZKt2H_vlBWhFwlMhpn3eQdehK4pmVNC1EOiRCuOCSWYKKqwPkMTKvIcM83kOfQcekkFuUSzlEJBGCVSi1xP0M32w8e2r6P9Cq0fYnC3trPNIYV0hS4q2yQ_-_2n6P3pcbt8xpuX1Xq52GDHwAJzQZXKpPCiIF56SahguiiFUkJpboXmmaZVyRhzXMPC-VI55aus1FwVueRTNB99a9t4E7qqH6J18ErfBtd3vgowX3A4pvOMEQDuTwDQDP57qO0-JbN-ez3V0lHrYp9S9JXZxdDaeDCUmGN4ZgzPQHjmGJ7RwNyNzM4mZ5sq2s6F9AcyDr5QQMdGXYJVV_toPvt9hPTSP-Y_1kp7WA</recordid><startdate>201009</startdate><enddate>201009</enddate><creator>Donato, D. I.</creator><creator>Lazzara, G.</creator><creator>Milioto, S.</creator><general>Springer Netherlands</general><general>Springer</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>ISR</scope></search><sort><creationdate>201009</creationdate><title>Thermogravimetric analysis</title><author>Donato, D. I. ; Lazzara, G. ; Milioto, S.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c2589-35177465e5b0e6e601529bd5775793a593491fd222c399bdced7c7ef4d937b863</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2010</creationdate><topic>Analytical Chemistry</topic><topic>Applied sciences</topic><topic>Archaeology</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Degradation and preservation</topic><topic>Exact sciences and technology</topic><topic>Inorganic Chemistry</topic><topic>Measurement Science and Instrumentation</topic><topic>Physical Chemistry</topic><topic>Polymer industry, paints, wood</topic><topic>Polymer Sciences</topic><topic>Wood</topic><topic>Wood. Paper. Non wovens</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Donato, D. I.</creatorcontrib><creatorcontrib>Lazzara, G.</creatorcontrib><creatorcontrib>Milioto, S.</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Gale In Context: Science</collection><jtitle>Journal of thermal analysis and calorimetry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Donato, D. I.</au><au>Lazzara, G.</au><au>Milioto, S.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Thermogravimetric analysis: A tool to evaluate the ability of mixtures in consolidating waterlogged archaeological woods</atitle><jtitle>Journal of thermal analysis and calorimetry</jtitle><stitle>J Therm Anal Calorim</stitle><date>2010-09</date><risdate>2010</risdate><volume>101</volume><issue>3</issue><spage>1085</spage><epage>1091</epage><pages>1085-1091</pages><issn>1388-6150</issn><eissn>1588-2926</eissn><eissn>1572-8943</eissn><abstract>Waterlogged archaeological woods (
Pinus pinaster
,
Ulmus
cf.
minor
and
Fagus sylvatica
L.) were consolidated by using Colophony, Rosin 100, and a mixture of Poly(ethylene) glycol (PEG) 3000 and Poly(propylene) glycol (PPG) 425. The efficiency of the consolidants was estimated by determining the content entrapped into the cavity of degraded wood. For this purpose, thermogravimetry was demonstrated to be a reliable tool. In the case that the polymeric mixture was used for impregnation, it was also possible to discriminate the amount of PEG 3000 from that of PPG 425 captured by the wood capillaries. Regardless of the wood nature, all the consolidants were present in treated samples in large amount (at least 70% w/w). Thermogravimetric results were in agreement with those calculated by using the wood degradation degree and composition of the consolidant mixture. One of the advantages of using this technique consists into requiring very small amounts (a few mg) of sample against the grams necessary for the conventional experiments.</abstract><cop>Dordrecht</cop><pub>Springer Netherlands</pub><doi>10.1007/s10973-010-0717-9</doi><tpages>7</tpages></addata></record> |
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issn | 1388-6150 1588-2926 1572-8943 |
language | eng |
recordid | cdi_gale_infotracacademiconefile_A358998420 |
source | Springer Nature - Complete Springer Journals |
subjects | Analytical Chemistry Applied sciences Archaeology Chemistry Chemistry and Materials Science Degradation and preservation Exact sciences and technology Inorganic Chemistry Measurement Science and Instrumentation Physical Chemistry Polymer industry, paints, wood Polymer Sciences Wood Wood. Paper. Non wovens |
title | Thermogravimetric analysis: A tool to evaluate the ability of mixtures in consolidating waterlogged archaeological woods |
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