Low temperature TLP bonding of [Al.sub.2][O.sub.3]-ceramics using eutectic Au- alloys
In this study, [Al.sub.2][O.sub.3]-ceramics were joined via TLP bonding using interlayers of eutectic Au-12Ge (wt%) and Au-3Si (wt%) solder alloys, respectively, with a melting temperature of 361 and 363°C and Ni wetting layers. The Ni layers were part of a metallic multilayer coating (Ti/W/Ni) appl...
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Veröffentlicht in: | Journal of materials science 2013-10, Vol.48 (20), p.7115 |
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description | In this study, [Al.sub.2][O.sub.3]-ceramics were joined via TLP bonding using interlayers of eutectic Au-12Ge (wt%) and Au-3Si (wt%) solder alloys, respectively, with a melting temperature of 361 and 363°C and Ni wetting layers. The Ni layers were part of a metallic multilayer coating (Ti/W/Ni) applied on the ceramic surface to ensure wetting and adhesion during the joining process. For comparison, a soldering process was performed as well by changing the multilayer structure to Ti/W/Au. With respect to the different joining processes the influence of the variation in wetting layers on the interface reactions, mechanical properties and re-melting temperature was analyzed by scanning electron microscopy, shear testing, and differential scanning calorimetry. It is shown that sound joint can be produced at a joining temperature of 400°C, achieving reasonable shear strength and re-melting temperatures more than 550°C above the initial melting temperature of the filler metal. |
doi_str_mv | 10.1007/s10853-013-7526-z |
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The Ni layers were part of a metallic multilayer coating (Ti/W/Ni) applied on the ceramic surface to ensure wetting and adhesion during the joining process. For comparison, a soldering process was performed as well by changing the multilayer structure to Ti/W/Au. With respect to the different joining processes the influence of the variation in wetting layers on the interface reactions, mechanical properties and re-melting temperature was analyzed by scanning electron microscopy, shear testing, and differential scanning calorimetry. It is shown that sound joint can be produced at a joining temperature of 400°C, achieving reasonable shear strength and re-melting temperatures more than 550°C above the initial melting temperature of the filler metal.</description><identifier>ISSN: 0022-2461</identifier><identifier>EISSN: 1573-4803</identifier><identifier>DOI: 10.1007/s10853-013-7526-z</identifier><language>eng</language><publisher>Springer</publisher><subject>Alloys ; Ceramic materials ; Ceramics ; Coatings ; Mechanical properties ; Specialty metals industry</subject><ispartof>Journal of materials science, 2013-10, Vol.48 (20), p.7115</ispartof><rights>COPYRIGHT 2013 Springer</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27922,27923</link.rule.ids></links><search><creatorcontrib>Weyrich, Nico</creatorcontrib><creatorcontrib>Leinenbach, Christian</creatorcontrib><title>Low temperature TLP bonding of [Al.sub.2][O.sub.3]-ceramics using eutectic Au- alloys</title><title>Journal of materials science</title><description>In this study, [Al.sub.2][O.sub.3]-ceramics were joined via TLP bonding using interlayers of eutectic Au-12Ge (wt%) and Au-3Si (wt%) solder alloys, respectively, with a melting temperature of 361 and 363°C and Ni wetting layers. The Ni layers were part of a metallic multilayer coating (Ti/W/Ni) applied on the ceramic surface to ensure wetting and adhesion during the joining process. For comparison, a soldering process was performed as well by changing the multilayer structure to Ti/W/Au. With respect to the different joining processes the influence of the variation in wetting layers on the interface reactions, mechanical properties and re-melting temperature was analyzed by scanning electron microscopy, shear testing, and differential scanning calorimetry. It is shown that sound joint can be produced at a joining temperature of 400°C, achieving reasonable shear strength and re-melting temperatures more than 550°C above the initial melting temperature of the filler metal.</description><subject>Alloys</subject><subject>Ceramic materials</subject><subject>Ceramics</subject><subject>Coatings</subject><subject>Mechanical properties</subject><subject>Specialty metals industry</subject><issn>0022-2461</issn><issn>1573-4803</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2013</creationdate><recordtype>article</recordtype><recordid>eNpVjstKw0AUhgdRsFYfwN1sXUw8c8tMl6GoLQQqWlellLklRNJEOhO8PL3xslDO4j_8fN_hIHRJIaMA6jpS0JIToJwoyXLycYQmVCpOhAZ-jCYAjBEmcnqKzmJ8BgCpGJ2gp7J_xSnsX8LBpOEQ8Lq8x7bvfNPVuK_wpmizONiMbTer74VviRvZfeMiHuIXFYYUXGocLgaCTdv27_EcnVSmjeHiN6dofXuzni9IubpbzouS1IpLIjwo64SmXldacGWZkTy3QeWVt_mMV9IHqYIVwhhltHcgnKfaS0HBSD_jU5T9nK1NG3ZNV_XpYNw4Poz_9V2omrEvuJCguGByFK7-CSOTwluqzRDjbvn48Jf9BFMEY74</recordid><startdate>20131015</startdate><enddate>20131015</enddate><creator>Weyrich, Nico</creator><creator>Leinenbach, Christian</creator><general>Springer</general><scope>ISR</scope></search><sort><creationdate>20131015</creationdate><title>Low temperature TLP bonding of [Al.sub.2][O.sub.3]-ceramics using eutectic Au- alloys</title><author>Weyrich, Nico ; Leinenbach, Christian</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-g735-4d07bc481d8f8437b2a536be76fdb693f5de57eb44aa7a8dc04cd18d5410a5d93</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2013</creationdate><topic>Alloys</topic><topic>Ceramic materials</topic><topic>Ceramics</topic><topic>Coatings</topic><topic>Mechanical properties</topic><topic>Specialty metals industry</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Weyrich, Nico</creatorcontrib><creatorcontrib>Leinenbach, Christian</creatorcontrib><collection>Gale In Context: Science</collection><jtitle>Journal of materials science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Weyrich, Nico</au><au>Leinenbach, Christian</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Low temperature TLP bonding of [Al.sub.2][O.sub.3]-ceramics using eutectic Au- alloys</atitle><jtitle>Journal of materials science</jtitle><date>2013-10-15</date><risdate>2013</risdate><volume>48</volume><issue>20</issue><spage>7115</spage><pages>7115-</pages><issn>0022-2461</issn><eissn>1573-4803</eissn><abstract>In this study, [Al.sub.2][O.sub.3]-ceramics were joined via TLP bonding using interlayers of eutectic Au-12Ge (wt%) and Au-3Si (wt%) solder alloys, respectively, with a melting temperature of 361 and 363°C and Ni wetting layers. The Ni layers were part of a metallic multilayer coating (Ti/W/Ni) applied on the ceramic surface to ensure wetting and adhesion during the joining process. For comparison, a soldering process was performed as well by changing the multilayer structure to Ti/W/Au. With respect to the different joining processes the influence of the variation in wetting layers on the interface reactions, mechanical properties and re-melting temperature was analyzed by scanning electron microscopy, shear testing, and differential scanning calorimetry. It is shown that sound joint can be produced at a joining temperature of 400°C, achieving reasonable shear strength and re-melting temperatures more than 550°C above the initial melting temperature of the filler metal.</abstract><pub>Springer</pub><doi>10.1007/s10853-013-7526-z</doi><tpages>10</tpages></addata></record> |
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subjects | Alloys Ceramic materials Ceramics Coatings Mechanical properties Specialty metals industry |
title | Low temperature TLP bonding of [Al.sub.2][O.sub.3]-ceramics using eutectic Au- alloys |
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